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DOE OSTI2025

Searching for MeV-mass neutrinophilic dark matter with large scale dark matter detectors

The indirect detection of dark matter (DM) through its annihilation products is one of the primary strategies for DM detection. One of the least constrained classes of models is neutrinophilic DM, because the annihilation products, weakly interacting neutrinos, are challenging to observe. Here, we consider a scenario where MeV-mass DM exclusively annihilates to the third neutrino mass eigenstate, which is predominantly of tau and muon flavor. In such a scenario, the potential detection rate of the neutrinos originating from the DM annihilation in our Galaxy in the conventional detectors would be suppressed by up to approximately two orders of magnitude. This is because the best sensitivity of such detectors for neutrinos with energies below approximately 100 MeV is for electron neutrino flavor. In this work, we highlight the potential of large-scale DM detectors in uncovering such signals in the tens of MeV range of DM masses. In addition, we discuss how coincident signals in direct detection DM experiments and upcoming neutrino detectors such as DUNE, Hyper-Kamiokande, and JUNO could provide new perspectives on the DM problem. Published by the American Physical Society 2025

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

DOE OSTI2021

Observables for recoil identification in high-definition Gas Time Projection Chambers

Directional detection of nuclear recoils is broadly desirable in nuclear and particle physics. At low recoil energies, this capability may be used to confirm the cosmological origin of a dark matter signal, to penetrate the so-called neutrino floor, or to distinguish between different neutrino sources. Gas Time Projection Chambers (TPCs) can enable directional recoil detection if the readout granularity is sufficiently high, as is the case when micro-pattern gaseous detectors (MPGDs) are utilized. A key challenge in such detectors is identifying and rejecting background electron recoil events caused by gamma rays from radioactive contaminants in the detector materials and the environment. We define new observables that can distinguish electron and nuclear recoils, even at keV-scale energies, based on the simulated ionization's topology. Here we perform a simulation study that shows these observables outperform the traditionally used discriminant, dE/dx, by up to three orders of magnitude. Furthermore, these new observables work well even at ionization energies well below 10keV and remain robust even in the regime where directionality fails.

79 ASTRONOMY AND ASTROPHYSICS↗

NASA NTRS2011

Using Supra-Arcade Downflows as Probes of Electron Acceleration During Solar Flares

Extracting information from coronal features above flares has become more reliable with the availability of increasingly higher spatial and temporal-resolution data in recent decades. We are now able to sufficiently probe the region high above long-duration flaring active regions where reconnection is expected to be continually occurring. Flows in the supra-arcade region, first observed with Yohkoh/SXT, have been theorized to be associated with newly-reconnected outflowing loops. High resolution data appears to confirm these assertions. Assuming that these flows are indeed reconnection outflows, then the detection of those directed toward the solar surface (i.e. downflowing) should be associated with particle acceleration between the current sheet and the loop footpoints rooted in the chromosphere. RHESSI observations of highly energetic particles with respect to downflow detections could potentially constrain electron acceleration models. I will discuss measurements of these supra-arcade downflows (SADs) in relation to reconnection model parameters and present preliminary findings comparing the downflow timings with high-energy RHESSI lightcurves.

Savage, Sabrina L.↗

DOE OSTI2022

Coupling Pulse Radiolysis with Nanosecond Time-Resolved Step-Scan Fourier Transform Infrared Spectroscopy: Broadband Mid-Infrared Detection of Radiolytically Generated Transients

We describe the first implementation of broadband, nanosecond time-resolved step-scan Fourier transform infrared (S 2 -FT-IR) spectroscopy at a pulse radiolysis facility. This new technique allows the rapid acquisition of nano- to microsecond time-resolved infrared (TRIR) spectra of transient species generated by pulse radiolysis of liquid samples at a pulsed electron accelerator. Wide regions of the mid-infrared can be probed in a single experiment, which often takes < 20–30 min to complete. It is therefore a powerful method for rapidly locating the IR absorptions of short-lived, radiation-induced species in solution, and for directly monitoring their subsequent reactions. Time-resolved step-scan FT-IR detection for pulse radiolysis thus complements our existing narrowband quantum cascade laser-based pulse radiolysis-TRIR detection system, which is more suitable for acquiring single-shot kinetics and narrowband TRIR spectra on small-volume samples and in strongly absorbing solvents, such as water. We have demonstrated the application of time-resolved step-scan FT-IR spectroscopy to pulse radiolysis by probing the metal carbonyl and organic carbonyl vibrations of the one-electron-reduced forms of two Re-based CO 2 reduction catalysts in acetonitrile solution. Transient IR absorption bands with amplitudes on the order of 1 × 10 −3 are easily detected on the sub-microsecond timescale using electron pulses as short as 250 ns.

(S2-FT-IR)↗

DOE OSTI2025

Mechanically flexible mid-wave infrared imagers using black phosphorus ink films

The mid-wave infrared (MWIR) spectral range (λ = 3–8 μm) enables important sensing and imaging applications, including non-invasive bioimaging, night vision, and autonomous navigation. Commercial MWIR photodetectors are limited to rigid imagers based on heteroepitaxial materials. There is an emerging need for mechanically flexible MWIR imagers to broaden their functionality and practicality. Recently, photodetectors using van der Waals (vdW) black phosphorus (BP) flakes have demonstrated highly sensitive room-temperature photodetection. Additionally, vdW materials are solution-processable, facilitating scalable processing and flexible device fabrication. In this work, we present flexible MWIR imagers consisting of photodiodes fabricated on thin plastic substrates using BP ink films. We demonstrate mechanically robust responsivity up to 2.5-mm bending radii and after 5000 bending cycles. Leveraging this flexibility, we achieve full-azimuthal imaging, detecting directional light sources with precision. These results establish a scalable approach for large-area, conformable MWIR imaging and pave the way for integration with flexible electronics.

Wijaya, Theodorus Jonathan↗

NASA NTRS1968

Monitor senses amount of contamination deposited on surfaces

Monitoring device detects and indicates directly the amount of contamination deposited on a surface. It uses an optical system in conjunction with a reliable collimated light source and associated electronics. Change in its output signal is proportional to change in the optical absorption characteristics of the sample plate surface.

Sheehy, R. N.↗

NASA NTRS1990

A mechanism for bursty radio emission in planetary magnetospheres

Bursty radio emissions are often observed from the polar magnetospheres of the earth, Jupiter, Saturn, and Uranus in addition to the smooth radio emissions commonly detected. It is shown that in plasma regimes in which the electron plasma frequency is less than the electron cyclotron frequency, anisotropic electron beams or gyrating electron beams can excite directly broadband electromagnetic radiation. The largest growth is for right-hand X-mode radiation with frequencies above the electron cyclotron frequency. This instability can produce bursty, broadband emission, consistent with some of the properties of the radiation observed from the magnetized planets.

Wong, H. K.↗

DOE OSTI2025

Exploring the Nucleon Structure via Deep Electroproduction Processes

Understanding the internal structure of the nucleon is a fundamental goal of modern physics, which aims at a comprehensive framework describing the internal dynamics of quarks and gluons. Among other structure functions, Generalized Parton Distributions (GPDs) offer a powerful framework for describing the nucleon dynamics by correlating the longitudinal momentum and the transverse position of its internal partons. Such a correlation provides a three-dimensional picture of the nucleon and enables access to fundamental properties, including the internal pressure distributions and the parton’s angular momentum contribution to the nucleon's total spin, thereby playing a central role in resolving the nucleon spin puzzle. At the Thomas Jefferson National Facility (JLab), polarized electron beam experiments allow for probing GPDs through the measurement of hard exclusive processes. Among the cleanest experimental channels, we find the electro-production of a real photon through the Deeply Virtual Compton Scattering (DVCS) mechanism. The first data-taking period of the CLAS12 program, taking place in 2018, allowed for unique DVCS Beam Spin Asymmetry (BSA) measurements in the phase space covered by a 10.6 GeV polarized electron beam impinging on an unpolarized liquid hydrogen target. Although detecting all final-state particles ensures exclusivity of the process, conservation laws indicate that it is not mandatory. I adopt an approach omitting the direct detection of the recoil proton, providing a simplified yet effective event selection strategy that boosts statistics and gives access to a larger phase space sensitive to the underlying GPD dynamics through BSA and cross section measurements. The Double DVCS (DDVCS) process promises a dedicated mapping of GPDs. Contributing to the electro-production of a lepton pair cross-section, the DDVCS reaction extends DVCS by allowing the final-state photon to be virtual, enriching the kinematic phase space and providing unique access to the internal correlations encoded by GPDs. A feasibility study is conducted to assess the potential of future DDVCS measurements at Jefferson Lab and the future Electron-Ion Collider (EIC). While Jefferson Lab will provide DDVCS measurements in the valence region through the SoLID$\mu$ and $\mu$CLAS12 experimental projects, in the long term, the EIC will provide complementary measurements in the sea region, both accessing unprecedented information about GPDs in a phase space region otherwise inaccessible. Taken together, these investigations demonstrate both the current capabilities and future opportunities for probing GPDs through exclusive processes. The experimental analysis of DVCS at CLAS12 provides precise measurements within an established framework, while the phenomenological study of DDVCS opens the door to richer and more comprehensive explorations with future detectors and facilities.

Alvarado, Juan [Université Paris-Saclay: Gif-sur-Y↗

DOE OSTI2025

Spin-dependent dark matter scattering in quasi-two-dimensional magnets

We study the prospects of detecting dark matter coupled to the spin of the electron, such that it may scatter and excite magnons—collective excitations of electronic spins. We show that materials exhibiting long-range magnetic order where the spins are coupled only along a plane may act as directional dark matter detectors. These quasi-two-dimensional materials possess anisotropic dispersion relations and structure functions which induce a sidereal modulation in the excitation rate. We calculate the expected signal rate for some candidate (anti)ferromagnets, demonstrating a possible route to the direct detection of spin-dependent dark matter in the keV to MeV mass range.

Dark matter direct detection↗

DOE OSTI2021

Trocylation of 3-quinuclidinol, a key marker for the chemical warfare agent 3-quinuclidinyl benzilate, for its enhanced detection at low levels in complex soil matrices by electron ionization gas chromatography–mass spectrometry

Detection of 3-quinuclidinol (3Q), a marker for the chemical warfare agent 3-quinuclidinyl benzilate, is very difficult by gas chromatography–mass spectrometry (GC/MS), providing low, broad signals even when analyzed in isolated form. Therefore, a method that can convert 3Q into a substrate with enhanced detectability by GC/MS would be an important tool for its analysis. 2,2,2-Trichloroethoxycarbonyl chloride (TrocCl) was used in the derivatization of 3Q in three different soils of varying composition and total organic content (Virginia type A soil, Nebraska EPA standard soil and Ottawa sand) when present at a 10 μg g -1 concentration in each. A direct derivatization protocol and one involving the pre-extraction of the analyte were evaluated for their individual efficiencies and subsequent analysis using electron ionization GC/MS. The practical derivatization of 3Q, when present at low levels (10 μg g -1 ) in three different soil matrices, was found to be rapid (1 h) and to take place smoothly at ambient temperature (and as low as 4°C). The method detection limit was determined to be 30 ng mL -1 for the Virginia type A soil, 49 ng mL -1 for the Nebraska EPA standard soil and 72 ng mL -1 for the Ottawa sand sample. An expedient and practical derivatization method for 3Q, a chemical warfare degradation product difficult to detect by GC/MS, has been realized using trichloroethyl chloroformate. The reaction provides 3Q-Troc, a derivative with better detectability than 3Q by electron ionization GC/MS such as peak sharpness and a unique mass spectrum for its unambiguous identification.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

DOE OSTI2020

Detection of uncompensated magnetization at the interface of an epitaxial antiferromagnetic insulator

We have probed directly the temperature and magnetic field dependence of pinned uncompensated magnetization at the interface of antiferromagnetic FeF 2 with Cu, using FeF 2 -Cu-Co spin valves. Electrons polarized by the Co layer are scattered by the pinned uncompensated moments at the FeF 2 -Cu interface giving rise to giant magnetoresistance. We determined the direction and magnitude of the pinned uncompensated magnetization at different magnetic fields and temperatures using the angular dependencies of resistance. The strong FeF 2 anisotropy pins the uncompensated magnetization along the easy axis independent of the cooling field orientation. Most interestingly, magnetic fields as high as 90 kOe cannot break the pinning at the FeF 2 -Cu interface. This proves that the pinned interfacial magnetization is strongly coupled to the antiferromagnetic order inside the bulk FeF 2 layer. Studies as a function of FeF2 crystalline orientation show that uncompensated spins are only detected in a spin valve with (110) crystal orientation, but not in valves containing FeF 2 (100) and FeF 2 (001). This observation is in agreement with symmetry-related considerations which predict the equilibrium boundary magnetization for the FeF 2 (110) layer.

36 MATERIALS SCIENCE↗

DOE OSTI2025

Electronic Spin Relaxation and Clustering in High-Pressure High-Temperature Synthesized Microcrystalline Diamond Particles with Reduced Nitrogen Content

The negatively charged nitrogen-vacancy (NV – ) color center in diamonds is widely studied because of numerous applications of this unique quantum system in sensing and quantum information sciences. While substitutional nitrogen is required to form the NV – centers in diamond, it also yields other paramagnetic defects─primarily the neutrally charged substitutional nitrogen centers (P1)─that decrease NV – spin coherence, which in turn degrades performance in applications. Herein, we investigate high-pressure high-temperature synthesized diamond microparticles (ca. 140–185 μm) having lower─ranging from 3 to 38 ppm─than the typical nitrogen content of type 1b diamond ( ca. 100 ppm and higher) typically used for the production of fluorescent diamond particles with NV – centers. A suite of electron paramagnetic resonance, optically detected magnetic resonance, and nuclear magnetic resonance methods are used to characterize spin properties of P1 and NV – centers in the particles. Upon decreasing the nitrogen content from 29 to 3 ppm, the ensemble NV – T 2 relaxation time increased by about 3-fold as measured directly in the Hahn Echo experiment at magnetic field of 1.2 T. Analysis of electronic relaxation of P1 centers revealed the existence of at least two distinct populations of P1 centers, consisting of fast and slower relaxing spins and allowed for an estimation of local concentrations. Even with <10 ppm nitrogen contents, the analysis indicated a highly heterogeneous distribution of P1 centers, suggesting the possibility of P1 spin clustering even at low nitrogen concentrations. The combined data demonstrate that the particles prepared from HPHT diamond with a low nitrogen content offer improved spin properties that are beneficial for NV – sensing applications.

Carbon↗

DOE OSTI2024

Scintillating Bubble Chambers for Direct Dark Matter Detection, and an Update on SBC-LAr10

The Scintillating Bubble Chamber (SBC) Collaboration aims to use the liquid-noble bubble chamber technology as a low-threshold detector for dark matter particles of 1-10 GeV/c2. The detector combines the remarkable electron recoil (ER) discrimination of the bubble chamber with the event-by-event energy resolution provided by liquid argon (LAr) scintillation, with the crucial added benefit that ER discrimination in liquid-noble bubble chambers extends to much lower thresholds than in past freon-filled bubble chambers, with the potential for quasi-background-free operation at thresholds of 100 eV in nuclear recoil (NR) energy. SBC has developed two functionally identical 10 kg detectors: SBC-LAr10 at Fermilab will calibrate low-threshold performance, while the radio-pure SBC-SNOLAB chamber will execute SBC s first deep-underground dark matter search. SBC-LAr10 at Fermilab was recently installed in the MINOS tunnel 100 meters underground, and the first bubbles are expected this fall. I will present the current status of SBC-LAr10 and describe the suite of gamma and neutron calibrations we will execute. The calibrations will confirm the physics reach of this new technology, motivating not just the SBC-SNOLAB chamber now being assembled but also future searches into the solar neutrino fog at 1 GeV/c2.

Sheng, Zhiheng↗

NASA NTRS1989

Ionization from soft electron precipitation in the auroral F region

Rocket-borne instrumentation, launched into the morning sector auroral zone from Sondre Stromfjord, Greenland, detects electron density enhancements correlated with enhancements in the flux of soft (less than 1 keV) downgoing electrons. These electron density enhancements seem most likely to have been generated by direct production of ionization at F region altitudes. Model calculations of the electron impact ionization rate, based on the measured electron spectrum, lend support to this hypothesis.

Labelle, J.↗

NASA NTRS1991

A spacecraft charging study on the SCEX 3 rocket

Instruments on the SCEX 3 rocket payload were used to study charging during electron beam emissions. The data show that electrostatic analyzers can be used to measure vehicle charging and direct beam return currents in dense plasma conditions. The data also show return current dependencies on pitch angle, beam current and beam energy. It is found that if the proper care is taken, ESAs can be used to detect charging on vehicles in low altitude orbits which are contaminated with high levels of outgassing and in dense plasma regimes. These results are particularly important for the TSS-1 electrodynamic tether program where ESAs are being used to determine Shuttle charging levels during tether employment and to look for high fluxes of directly returning electrons during electron generator operations to balance the Shuttle charging.

Mullen, E. G.↗

NASA NTRS1992

COBE anisotropy from supercluster gas

It is suggested that the microwave background anisotropy detected by the COBE DMR might be dominated not by the direct gravitational effect of primordial fluctuations in the last scattering surface, but by scattering off of moving electrons in optically thin, nearby superclusters. Hot diffuse clouds of ionized gas created during supercluster collapse produce Sunyaev-Zel'dovich and Doppler background anisotropy whose properties may closely mimic those of primordial anisotropy in current data. Strategies for and difficulties in separating the effects are discussed, based on the anisotropy spectrum, autocorrelation, correlation with galaxy catalogs, X-ray emission, and integrated spectral distortions.

Hogan, Craig J.↗

DOE OSTI2024

Scintillating Bubble Chambers for Direct Dark Matter Detection, and an Update on SBC-LAr10

Sheng, Zhiheng↗

NASA NTRS1989

Reversal electron attachment ionizer for detection of trace species

An in-line reversal electron, high-current ionizer capable of focusing a beam of electrons to a reversal region and executing a reversal of the electrons, such that the electrons possess zero kinetic energy at the point of reversal, may be used to produce both negative and positive ions. A sample gas is introduced at the point of electron reversal for low energy electron-(sample gas) molecule attachment with high efficiency. The attachment process produces negative ions from the sample gas, which includes species present in trace (minute) amounts. These ions are extracted efficiently and directed to a mass analyzer where they may be detected and identified. The generation and detection of positive ions is accomplished in a similar fashion with minimal adjustment to potentials applied to the apparatus.

Bernius, Mark T.↗