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At least 199 records · Page 11

High-Resolution Full-Field Structural Microscopy of the Voltage-Induced Filament Formation in VO 2 -Based Neuromorphic Devices

In order to make neuromorphic functions in memristive devices more efficient, information about the structural properties of filament formation at the micro- and mesoscopic scales is necessary. Despite extensive research on VO 2 , a key material due to its filament formation, local operando structural measurements remain challenging and often involve destructive specimen preparation and long rastering times, greatly limiting the scope of experimental studies. Utilizing dark-field X-ray microscopy (DFXM), a fullfield imaging modality, structural signatures of the filament formation process operando are revealed in VO 2 devices. DFXM experiments illustrate that rutile filaments contain isolated monoclinic clusters, indicating structural nonuniformity interior to the filament. The formation of the rutile phase beneath device electrodes was shown to precede filament development, followed by the formation of filament paths guided by nucleation sites within the device. Finally, a medium-term (<30 min) memory mechanism is observed in VO 2 , mediated by sites within the device gap that tend to switch at significantly lower voltages after electrical cycling, a tendency that persists through a brief thermal reset. High spatial resolution, large field-of-view, structure selectivity, and fast signal acquisition of DFXM provided insight into structural features of the filamentary channel and surrounding regions during voltage cycling.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

Correlative chemical and elemental nano-imaging of morphology and disorder at the nacre-prismatic region interface in Pinctada margaritifera

Abstract Understanding biomineralization relies on imaging chemically heterogeneous organic–inorganic interfaces across a hierarchy of spatial scales. Further, organic minority phases are often responsible for emergent inorganic structures from the atomic arrangement of different polymorphs, to nano- and micrometer crystal dimensions, up to meter size mollusk shells. The desired simultaneous chemical and elemental imaging to identify sparse organic moieties across a large field-of-view with nanometer spatial resolution has not yet been achieved. Here, we combine nanoscale secondary ion mass spectroscopy (NanoSIMS) with spectroscopic IR s -SNOM imaging for simultaneous chemical, molecular, and elemental nanoimaging. At the example of Pinctada margaritifera mollusk shells we identify and resolve ~ 50 nm interlamellar protein sheets periodically arranged in regular ~ 600 nm intervals. The striations typically appear ~ 15 µm from the nacre-prism boundary at the interface between disordered neonacre to mature nacre. Using the polymorph distinctive IR-vibrational carbonate resonance, the nacre and prismatic regions are consistently identified as aragonite ( $${\overline{\nu }}_{a}=860$$ ν ¯ a = 860 cm −1 ) and calcite ( $${\overline{\nu }}_{c}=880$$ ν ¯ c = 880 cm −1 ), respectively. We observe previously unreported morphological features including aragonite subdomains encapsulated in extensions of the prism-covering organic membrane and regions of irregular nacre tablet formation coincident with dispersed organics. We also identify a ~ 200 nm region in the incipient nacre region with less well-defined crystal structure and integrated organics. These results show with the identification of the interlamellar protein layer how correlative nano-IR chemical and NanoSIMS elemental imaging can help distinguish different models proposed for shell growth in particular, and how organic function may relate to inorganic structure in other biomineralized systems in general.

54 ENVIRONMENTAL SCIENCES↗

Billion-pixel x-ray camera (BiPC-X)

The continuing improvement in quantum efficiency (above 90% for single visible photons), reduction in noise (below 1 electron per pixel), and shrink in pixel pitch (less than 1 μm) enable billion-pixel x-ray cameras (BiPC-X) based on commercial complementary metal–oxide–semiconductor (CMOS) imaging sensors. We describe BiPC-X designs and prototype construction based on flexible tiling of commercial CMOS imaging sensors with millions of pixels. Device models are given for direct detection of low energy x rays (<10 keV) and indirect detection of higher energies using scintillators. Modified Birks’s law is proposed for light yield non-proportionality in scintillators as a function of x-ray energy. Single x-ray sensitivity and spatial resolution have been validated experimentally using a laboratory x-ray source and the Argonne Advanced Photon Source. Possible applications include wide field-of-view or large x-ray aperture measurements in high-temperature plasmas, the state-of-the-art synchrotron, x-ray free electron laser, and pulsed power facilities.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

X-ray self-emission imaging with spherically bent Bragg crystals on the Z-machine

Here, an x-ray imaging scheme using spherically bent crystals was implemented on the Z-machine to image x rays emitted by the hot, dense plasma generated by a Magnetized Liner Inertial Fusion (MagLIF) target. This diagnostic relies on a spherically bent crystal to capture x-ray emission over a narrow spectral range (<15 eV), which is established by a limiting aperture placed on the Rowland circle. The spherical crystal optic provides the necessary high-throughput and large field-of-view required to produce a bright image over the entire, one-cm length of the emitting column of a plasma. The average spatial resolution was measured and determined to be 18 µm for the highest resolution configuration. With this resolution, the radial size of the stagnation column can be accurately determined and radial structures, such as bifurcations in the column, are clearly resolved. The success of the spherical-crystal imager has motivated the implementation of a new, two-crystal configuration for identifying sources of spectral line emission using a differential imaging technique.

47 OTHER INSTRUMENTATION↗

Overionized plasma in the supernova remnant Sagittarius A East anchored by XRISM observations

Sagittarius A East is a supernova remnant with a unique surrounding environment, as it is located in the immediate vicinity of the supermassive black hole at the Galactic center, Sagittarius A$^{*}$. The X-ray emission of the remnant is suspected to show features of overionized plasma, which would require peculiar evolutionary paths. We report on the first observation of Sagittarius A East with the X-Ray Imaging and Spectroscopy Mission (XRISM). Equipped with a combination of a high-resolution microcalorimeter spectrometer and a large field-of-view CCD imager, we for the first time resolved the Fe xxv K-shell lines into fine structure lines and measured the forbidden-to-resonance intensity ratio to be $1.39 \pm 0.12$, which strongly suggests the presence of overionized plasma. We obtained a reliable constraint on the ionization temperature just before the transition into the overionization state, of $\gt\! 4\:$keV. The recombination timescale was constrained to be $\lt\! 8 \times 10^{11} \:$cm$^{-3}\:$s. The small velocity dispersion of $109 \pm 6\:$km$\:$s$^{-1}$ indicates a low Fe ion temperature $\lt\! 8\:$keV and a small expansion velocity $\lt\! 200\:$km$\:$s$^{-1}$. The high initial ionization temperature and small recombination timescale suggest that either rapid cooling of the plasma via adiabatic expansion from dense circumstellar material or intense photoionization by Sagittarius A$^{*}$ in the past may have triggered the overionization.

galaxy center↗

Binary pseudo-random array (BPRA) for inspection and calibration for cylindrical wavefront interferometry

High-accuracy metrology is vitally important in manufacturing ultra-high-quality free-form mirrors designed to manipulate X-ray light with nanometer-scale wavelengths. However, surface topography measurements are instrument dependent, and without the knowledge of how the instrument performs under the practical usage conditions, the measured data contain some degree of uncertainty. Binary Pseudo Random Array (BPRA) “white noise” artifact are effective and useful for characterizing the Instrument Transfer Function (ITF) of surface topography metrology tools and wavefront measurement instrument. BPRA artifact contains features with all spatial frequencies in the instrument bandpass with equal weight. As a result, power spectral density of the patterns has a deterministic white-noise-like character that allows direct determination of the ITF with uniform sensitivity over the entire spatial frequency range. The application examples include electron microscopes, x-ray microscopes, interferometric microscopes, and large field-of-view Fizeau Interferometers. Furthermore, we will introduce the application of BPRA method to characterizing the ITF of Cylindrical Wavefront Interferometry (CWI), by developing the BPRA artifact which matches the radius of curvature of the cylindrical wavefront. The data acquisition and analysis procedures for different applications of the ITF calibration technique developed are also discussed.

Munechika, K↗

Nuclear imaging to diagnose and correct target-driver registration at high-repetition-rate for improved reactor efficiency

Inertial Confinement Fusion produces energy from a burning plasma lasting a fraction of a nanosecond. Power plant designs based on Inertial Fusion Energy (IFE) will need to ignite targets 1-10 times a second, fired as projectiles into a chamber and delivering the driver to the target location. Driver asymmetry is known to impact ICF experiments at gain near unity and remains a candidate for primary yield degradation, and therefore fusion power plant energy output, for high-gain target designs. For a Fusion Power Plant (FPP), continuous and real-time monitoring of target performance provides an opportunity to stabilize or correct the target-driver registration. This requires x-ray and neutron imaging with a large field-of-view, sufficiently high resolution, fast analysis and to subtend a minimal solid angle. We introduce design criteria for such an imaging system that uses a coded aperture and time-gated, lens-coupled scintillators as a viable solution and outline the research steps required to field such a system. Integrating the imaging system into an IFE power plant as part of an active feedback loop could increase average power output by reducing the failure rate due to mis-aligned drivers with respect to the target.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Pioneer Venus Star Sensor

The design predictions and orbital performance verification of the solid state star scanner used in the Onboard Attitude Control of the Pioneer Venus Orbiter and Multiprobe are presented. The star sensor extended the scanner use to active despin control, and it differs from previous sensors in solid state detection, redundant electronics for reliability, larger field of view, and large dynamic spin range. The star scanner hardware and design performance based on the ability to predict all noise sources, signal magnitudes, and expected detection probability are discussed. In-flight data collected to verify sensor ground calibration are tabulated and plotted in predicted accuracy curves. It is concluded that the Pioneer Venus Star Sensor has demonstrated predictable star calibration in the range of .1 magnitude uncertainties and usable star catalogs of 100 stars with very high probabilities of detection, which were much better than expected and well within the mission requirements.

Gutshall, R. L.↗

Eye torsion and visual tilt are mediated by different binocular processes

Viewing a large, patterned field rotating about the line of sight produces two measurable effects; cyclotorsion of the eyes (torsion) and a perceived displacement of vertical and horizontal (tilt). Experiments examining binocular interaction for these effects show: (1) both effects demonstrate summation in normal individuals and thus both involve a binocular process; (2) the process for tilt is different than for torsion, since summation for torsion is spared in stereodeficient individuals while that for tilt is eliminated.

Wolfe, J. M.↗

A binocular contribution to the production of optokinetic nystagmus in normal and stereoblind subjects

Viewing a large patterned field moving in one direction produces a regular pattern of eye movements known as optokinetic nystagmus (OKN). Fox et al. (1978) showed that the mechanism producing OKN can utilize purely binocular or 'cyclopean' input. Experiments reported confirm that finding and extend it to demonstrate that the binocularity of this mechanism is not disrupted in subjects who lack stereopsis. This result indicates that there exists more than one binocular process in the visual system.

Wolfe, J. M.↗

Radiometric accuracy of the Diffuse Infrared Background Experiment (DIRBE)

The Diffuse Infrared Background Experiment (DIRBE) is a cryogenically-cooled 10-band photometer with a large field-of-view (0.886 x 0.886 sq deg) which scans by rotation of the Cosmic Background Explorer about a spin axis. In-orbit calibration requires that the DIRBE detect and measure with precision the signatures of compact sources as they transit the field-of-view. Analysis of the conceptual optical design revealed that response of the 10 bands would vary significantly as a function of source position in the field-of-view, caused by anamorphic pupil distortion and field separation. The optical design reported in this paper is the result of changes which greatly improve the response uniformity and radiometric accuracy of the DIRBE.

Howell, B. J.↗

Ideas for a future earth observing system from geosynchronous orbit

Uses for the proposed geosynchronous platform are described. The geosynchronous satellite could provide good spatial and temporal resolution, a large field-of-view, easier calibration, stereography, and data relay. The limitations of the platform are discussed. The applications of the geosynchronous platform to meteorology, earth surveying, and oceanography are examined.

Shenk, William E.↗

High accuracy image centroiding with a moving Ronchi ruling

A moving Ronchi ruling at the focal plane of a telescope has been employed to measure the relative motions of stars with great accuracy. The method has long-term stability and exceptional linearity over a relatively large field-of-view. This measurement technique may prove useful in other applications where such capabilities are required. This paper employs Fourier optics to describe the operation of the device, explore performance at very long and very short periods, and consider ruling profiles and other means of optimizing performance.

Lawrence, George N.↗

NIFTE: The Near Infrared Faint-Object Telescope Experiment

The high sensitivity of large format InSb arrays can be used to obtain deep images of the sky at 3-5 micrometers. In this spectral range cool or highly redshifted objects (e.g. brown dwarfs and protogalaxies) which are not visible at shorter wavelengths may be observed. Sensitivity at these wavelengths in ground-based observations is severly limited by the thermal flux from the telescope and from the earth's atmosphere. The Near Infrared Faint-Object Telescope Experiment (NIFTE), a 50 cm cooled rocket-borne telescope combined with large format, high performance InSb arrays, can reach a limiting flux less than 1 micro-Jy(1-sigma) over a large field-of-view in a single flight. In comparison, the Infrared Space Observatory (ISO) will require days of observation to reach a sensitivity more than one order of magnitude worse over a similar area of the sky. The deep 3-5 micrometer images obtained by the rocket-borne telescope will assist in determining the nature of faint red objects detected by ground-based telescopes at 2 micrometers, and by ISO at wavelengths longer than 5 micrometers.

Bock, James J.↗

Cloud properties inferred from 8-12 micron data

A trispectral combination of observations at 8-, 11-, and 12-micron bands is suggested for detecting cloud and cloud properties in the infrared. Atmospheric ice and water vapor absorption peak in opposite halves of the window region so that positive 8-minus-11-micron brightness temperature differences indicate cloud, while near-zero or negative differences indicate clear regions. The absorption coefficient for water increases more between 11 and 12 microns than between 8 and 11 microns, while for ice, the reverse is true. Cloud phases is determined by a scatter diagram of 8-minus-11-micron versus 11-minus-12-micron brightness temperature differences; ice cloud shows a slope greater than 1 and water cloud less than 1. The trispectral brightness temperature method was tested upon high-resolution interferometer data resulting in clear-cloud and cloud-phase delineation. Simulations using differing 8-micron bandwidths revealed no significant degradation of cloud property detection. Thus, the 8-micron bandwidth for future satellites can be selected based on the requirements of other applications, such as surface characterization studies. Application of the technique to current polar-orbiting High-Resolution Infrared Sounder (HIRS)-Advanced Very High Resolution Radiometer (AVHRR) datasets is constrained by the nonuniformity of the cloud scenes sensed within the large HIRS field of view. Analysis of MAS (MODIS Airborne Simulator) high-spatial resolution (500 m) data with all three 8-, 11-, and 12-micron bands revealed sharp delineation of differing cloud and background scenes, from which a simple automated threshold technique was developed. Cloud phase, clear-sky, and qualitative differences in cloud emissivity and cloud height were identified on a case study segment from 24 November 1991, consistent with the scene. More rigorous techniques would allow further cloud parameter clarification. The opportunities for global cloud delineation with the Moderate-Resolution Imaging Spectrometer (MODIS) appear excellent. The spectral selection, the spatial resolution, and the global coverage are all well suited for significant advances.

Strabala, Kathleen I.↗

A Snapshot of the Continuous Emission of the Active Galactic Nucleus in NGC 3783 from Gamma-Ray to Radio Wavelengths

To better understand the physical processes that produce the continuous emission in active galactic nuclei (AGN), a snapshot of the overall continuous energy distribution of NGC 3783, from gamma ray to radio wavelengths, has been obtained within the framework of the World Astronomy Days. The data collected in this campaign are from GRO, ROSAT, Voyager 2, IUE, HST, CTIO, SAAO, and the VLA. Great care has been taken in disentangling the genuine AGN continusous emission from other contributions; depending on the waveband, the latter might be (1) unrelated contaminating sources in cases where the instrument field of view is large (2) components within which the AGN is embedded, such as the stellar bulge population which accounts for a significant fraction of the optical continuum, and free-bound and FE2 blends wich contribute to the ultraviolet flux. After correction for these other contributins, the continuous emission of the isolated AGN appears to be rather flat (i.e., approximately equal energy per unit logarithmic frequency) from soft gamma ray to infrared wavelengths. At high energies (0.1 MeV to 0.1 keV), the AGN continuum can be fitted by a power law F nu approaches Nu(exp -a) with a spectral index of alpha approximately 1. At longer wavelengths, two excesses above this power law ('bumps') appear: in the ultraviolet, the classical big blue bump, which can be interpreted as thermal emission from the accretion disc surrounding a massive black hole, and in the infrared, a second bump which can be ascribed to thermal emission from dust in the vicinity of the AGN, heated by ultraviolet radiation from the central source. By fitting accretion-disk models to the observed AGN spectral energy distribution, we find values for the accretion disk innermost temperature, accretion rate, and black hole mass, with some differences that depend on whether or not we extrapolate the high energy power law up to infrared wavelengths. A fit to the IR bump above the extended alpha equals 1 power law suggests the presence of a dust component covering the region from a distance rho approximately equals 80 light days (hot grains at a temperature of approximately equals 1500 K) to rho approximately equals 60 light years (cool grains at T approximately equals 200 K). The total mass of dust is around 60 solar masses.

Alloin, D.↗

The Advanced Pair Telescope (APT) Mission Concept

We present a mission concept for the Advanced Pair Telescope (APT), a high-energy gamma-ray instrument with an order of magnitude improvement in sensitivity, 6 sr field of view, and angular resolution a factor of 3-10 times that of GLAST. With its very wide instantaneous field-of-view and large effective area, this instrument would be capable of detecting GRBs at very large redshifts, would enable a very high resolution study of SNRs and PWN, and could provide hour-scale temporal resolution of transients from many AGN and galactic sources. The APT instrument will consist of a Xe time-projection-chamber tracker that bridges the energy regime between Compton scattering and pair production and will provide an unprecedented improvement in angular resolution; a thick scintillating-fiber trackerlcalorimeter that will provide sensitivity and energy resolution to higher energies and will possess a factor of 10 improvement in geometric factor over GLAST; and an anticoincidence detector using scintillator-tiles to reject charged particles. After the anticipated 10-years of GLAST operation , the APT instrument would provide continued coverage of the critial high-energy gamma-ray band (between 30 MeV to 100 GeV), providing an essential component of broad-band multiwavelength studies of the high-energy universe.

Hunter, Stanley↗

Images and Spectral Performance of WFC3 Interference Filters

The Wide Field Camera 3 (WFC3) is a panchromatic imager that will be deployed in the Hubble Space Telescope (HST). The mission of the WFC3 is to enhance HST1s imaging capability in the ultraviolet, visible and near-infrared spectral regions. Together with a wavelength coverage spanning 2000A to 1.7 micron, the WFC3 high sensitivity, high spatial resolution, and large field-of-view provide the astronomer with an unprecedented set of tools for exploring all types of exciting astrophysical terrain and for addressing many key questions in astronomy today. The filter compliment, which includes broad, medium, and narrow band filters, naturally reflects the diversity of astronomical programs to be targeted with WFC3. The WFC3 holds 61 UVIS filters elements, 14 IR filters, and 3 dispersive elements. During ground testing, the majority of the UVIS filters were found to exhibit excellent performance consistent with or exceeding expectations; however, a subset of filters showed considerable ghost images; some with relative intensity as high as 10-15%. Replacement filters with band-defining coatings that substantially reduce these ghost images were designed and procured. A state-of-the-art characterization setup was developed to measured the intensity of ghost images, focal shift, wedge direction , transmitted uniformity and surface feature of filters that could effect uniform flat field images. We will report on this new filter characterization methods, as well as the spectral performance measurements of the in-band transmittance and blocking.

Quijada, Manuel A.↗