Electron paramagnetic resonance in irradiated Ag sub 2 CO sub 3.
Gamma irradiated silver carbonate EPR at liquid nitrogen temperatures
Ashford, N. A.↗
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Silicon surface barrier detectors used for liquid hydrogen density measurement
Multichannel system employing a radioisotope radiation source, strontium-90, radiation detector, and a silicon surface barrier detector, measures the local density of liquid hydrogen at various levels in a storage tank. The instrument contains electronic equipment for collecting the density information, and a data handling system for processing this information.
James, D. T.↗
Radiation damage of gallium arsenide production cells
High efficiency liquid phase epitaxy (LPE) gallium arsenide cells were irradiated with 1 Mev electrons up to fluences of 1 times 10 to the 16th power cm-2. Measurements of spectral response and dark and illuminated I-V data were made at each fluence and then, using computer codes, the experimental data was fitted to gallium arsenide cell models. In this way it was possible to determine the extent of the damage, and hence damage coefficients in both the emitter and base of the cell.
Mardesich, N.↗
An intercomparison of airborne PAN measurements
Results are reported on the performance of the NASA and NCAR PAN measurement instruments during the NASA Global Tropospheric Experiment Chemical Instrumentation Test and Evaluation 2 (CITE 2) mission in August-September 1986. Both PAN instruments employ the electron-capture gas chromatography approach for detection and are calibrated using a liquid PAN standard in a diffusion tube. Details of the instrument design, experimental protocols, and CITE 2 test flights are discussed, and the results are presented in extensive tables and graphs. It is found that the NASA and NCAR instruments agreed to within about 17 parts per trillion by volume (pptv) when the PAN mixing ratio was below 100 pptv and to within about 25 percent when the mixing ratio was 100-300 pptv.
Gregory, Gerald L.↗
A gamma-ray imaging telescope based on liquid xenon
A liquid-xenon time projection chamber (TPC) is discussed in terms of its utility as an imaging telescope for high energy astrophysics. The concept exploits the efficiency of xenon as an ionization and scintillation medium for imaging astrophysical gamma-ray sources. The design fundamentally follows the approach of an ionization calorimeter functioning as a TPC dedicated to 3D tracking. A schematic diagram of the instrument is presented, and the device measures the ionization signals - resulting from gamma-ray interactions with xenon - on collection electrodes. The liquid xenon instrument permits the identification of the direction of the Compton electron and thereby determines the location of the source. The energy region of 1-30 MeV is covered by the instrument, and source localization is possible for the entire range.
Aprile, Elena↗
640 x 480 MWIR and LWIR camera system developments
The performance of a 640 x 480 PtSi, 3,5 microns (MWIR), Stirling cooled camera system with a minimum resolvable temperature of 0.03 is considered. A preliminary specification of a full-TV resolution PtSi radiometer was developed using the measured performance characteristics of the Stirling cooled camera. The radiometer is capable of imaging rapid thermal transients from 25 to 250 C with better than 1 percent temperature resolution. This performance is achieved using the electronic exposure control capability of the MOS focal plane array (FPA). A liquid nitrogen cooled camera with an eight-position filter wheel has been developed using the 640 x 480 PtSi FPA. Low thermal mass packaging for the FPA was developed for Joule-Thomson applications.
Tower, J. R.↗
Advances in cryogenic engineering. Vols. 37A & 37B - Proceedings of the 1991 Cryogenic Engineering Conference, Univ. of Alabama, Huntsville, June 11-14, 1991
The present volume on advances in cryogenic engineering discusses heat and mass transfer in helium, heat transfer in cryogenic fluids, thermoacoustic oscillations, and insulation. Attention is given to applications of superconductivity with reference to magnetic stability and coil protection, cryogenic techniques, and refrigeration for electronics and superconducting systems. Topics addressed include compressors, expanders, and pumps for liquid helium, magnetic refrigerators, pulse tube refrigerators, and cryocoolers. Also examined are properties of cryogenic fluids, cryogenic applications in transportion and space science and technology, and cryogenic instrumentation.
Fast, Ronald W.↗
X-15 conditioning and pressurization system
The cooling system for the X-15 airplane incorporates insulation partial protection against high-temperature effects plus liquid and gaseous nitrogen to control specifically environmental and equipment temperatures. Electronic-equipment cooling represents the largest load; however, other items to be considered are the pressure-suit ventilation, aerodynamic-heating effects, sensor-head cooling, and windshield antifogging. A review of various types of cooling systems indicates that an expendable, stored, cooling system is the most efficient for short-duration missions. This paper presents a description including a simplified schematic diagram of the subject system. (author)
Bouman, C P↗
The growth of zeolites A, X and mordenite in space
Zeolites are a class of crystalline aluminosilicate materials that form the backbone of the chemical process industry worldwide. They are used primarily as adsorbents and catalysts and support to a significant extent the positive balance of trade realized by the chemical industry in the United States (around $19 billion in 1991). The magnitude of their efforts can be appreciated when one realizes that since their introduction as 'cracking catalysts' in the early 1960's, they have saved the equivalent of 60 percent of the total oil production from Alaska's North Slope. Thus the performance of zeolite catalysts can have a profound effect on the U.S. economy. It is estimated that a 1 percent increase in yield of the gasoline fraction per barrel of oil would represent a savings of 22 million barrels of crude oil per year, representing a reduction of $400 million in the United States' balance of payments. Thus any activity that results in improvement in zeolite catalyst performance is of significant scientific and industrial interest. In addition, due to their 'stability,' uniformity, and, within limits, their 'engineerable' structures, zeolites are being tested as potential adsorbents to purify gases and liquids at the parts-per-billion levels needed in today's electronic, biomedical, and biotechnology industries and for the environment. Other exotic applications, such as host materials for quantum-confined semiconductor atomic arrays, are also being investigated. Because of the importance of this class of material, extensive efforts have been made to characterize their structures and to understand their nucleation and growth mechanisms, so as to be able to custom-make zeolites for a desired application. To date, both the nucleation mechanics and chemistry (such as what are the 'key' nutrients) are, as yet, still unknown for many, if not all, systems. The problem is compounded because there is usually a 'gel' phase present that is assumed to control the degree of supersaturation, and this gel undergoes a continuous 'polymerization' type reaction during nucleation and growth. Generally, for structure characterization and diffusion studies, which are useful in evaluating zeolites for improving yield in petroleum refining as well as for many of the proposed new applications (e.g., catalytic membranes, molecular electronics, chemical sensors) large zeolites (greater than 100 to 1000 times normal size) with minimum lattice defects are desired. Presently, the lack of understanding of zeolite nucleation and growth precludes the custom design of zeolites for these or other uses. It was hypothesized that the microgravity levels achieved in an orbiting spacecraft could help to isolate the possible effects of natural convection (which affects defect formation) and minimize sedimentation, which occurs since zeolites are twice as dense as the solution from which they are formed. This was expected to promote larger crystals by allowing growing crystals a longer residence time in a high-concentration nutrient field. Thus it was hypothesized that the microgravity environment of Earth orbit would allow the growth of large, more defect-free zeolite crystals in high yield.
Sacco, Albert, Jr.↗
Direct Ink Write 3D Printing of Fully Dense and Functionally Graded Liquid Metal Elastomer Foams
Liquid metal (LM) elastomer composites offer promising potential in soft robotics, wearable electronics, and human-machine interfaces. Direct ink write (DIW) 3D printing offers a versatile manufacturing technique capable of precise control over LM microstructures, yet challenges such as interfilament void formation in multilayer structures impact material performance. Here, a DIW strategy is introduced to control both LM microstructure and material architecture. Investigating three key process parameters–nozzle height, extrusion rate, and nondimensionalized nozzle velocity–it is found that nozzle height and velocity predominantly influence filament geometry. The nozzle height primarily dictates the aspect ratio of the filament and the formation of voids. A threshold print height based on filament geometry is identified; below the height, significant surface roughness occurs, and above the ink fractures, which facilitates the creation of porous structures with tunable stiffness and programmable LM microstructure. These porous architectures exhibit reduced density and enhanced thermal conductivity compared to cast samples. When used as a dielectric in a soft capacitive sensor, they display high sensitivity (gauge factor = 9.0), as permittivity increases with compressive strain. These results demonstrate the capability to simultaneously manipulate LM microstructure and geometric architecture in LM elastomer composites through precise control of print parameters, while maintaining geometric fidelity in the printed design.
Spencer Pak↗
Surface chemistry of liquid metals
The fundamental surface chemistry of the behavior of liquid metals spreading on a solid substrate is not at all well understood. Each of these questions involves knowing the details of the structure of interfaces and their dynamics. For example the structure of a monolayer of tin oxide on pure liquid tin is unknown. This is in contrast to the relatively large amount of data available on the structure of copper oxide monolayers on solid, pure copper. However, since liquid tin has a vapor pressure below 10(exp -10)torr for a reasonable temperature range above its melting point, it is possible to use the techniques of surface science to study the geometric, electronic and vibrational structures of these monolayers. In addition, certain techniques developed by surface chemists for the study of liquid systems can be applied to the ultra-high vacuum environment. In particular we have shown that light scattering spectroscopy can be used to study the surface tension tensor of these interfaces. The tin oxide layer in particular is very interesting in that the monolayer is rigid but admits of bending. Ellipsometric microscopy allows the visualization of monolayer thick films and show whether island formation occurs at various levels of dosing.
Mann, J. Adin, Jr.↗
Common path point diffraction interferometer using liquid crystal phase shifting
A common path point diffraction interferometer uses dyed, parallel nematic liquid crystals which surround an optically transparent microsphere. Coherent, collimated and polarized light is focused on the microsphere at a diameter larger than that of the microsphere. A portion of the focused light passes through the microsphere to form a spherical wavefront reference beam and the rest of the light is attenuated by the dyed liquid crystals to form an object beam. The two beams form an interferogram which is imaged by a lens onto an electronic array sensor and into a computer which determines the wavefront of the object beam. The computer phase shifts the interferogram by stepping up an AC voltage applied across the liquid crystals without affecting the reference beam.
Mercer, Carolyn R.↗
Analysis of particulates of comet nucleus samples: Possible use of olivine as indicator phase
The electron microprobe is a proven instrument for particulate analysis and modifications are possible for in situ analysis of particulates in ice at temperatures near that of liquid nitrogen. Present sample requirements allow for polished samples with 0.25 x 0.25 dimensions to be maintained in the sample chamber of a modern electron probe (CAMECA SX-50) at a temperature of -150 C; larger samples are possible but at higher temperatures as determined by thermal conductivity. The major problem is transport and insertion of samples into the instrument through vacuum interlocks. The manufacturer of the above microprobe has designed an exchange mechanism to allow storage and transport of samples previously prepared for their sample holder which attaches to their instrument allowing extraction and insertion of samples while maintaining -150 C temperature. An important test will be the capability of preparing polished surfaces of an ice-particulate sample without loss of particles and at low temperatures. While thin sections of water ice are routine, these are not examined for particulate material and are prepared at temperatures easily obtained in room-size volumes. Anticipated problems include rounding of small grains in the relatively soft ice matrix and the technical problem of dry polishing.
Steele, I. M.↗
Supercooling effects in Cu-10 wt pct Co alloys solidified at different cooling rates
Electromagnetic levitation and electron beam surface melting were employed to study the effects of supercooling and cooling rate on the solidification of Cu-10 wt pct Co alloys. Two major effects were observed in the supercooled alloys: the nucleation of a metastable copper-rich phase which contains 13 wt pct to 20 wt pct Co in samples supercooled between 105 and 150 K and liquid phase separation which occurs in samples supercooled 150 K or more. The microstructure of the electron beam melted surfaces consisted of very fine spheres which were similar to those of the sample supercooled more than 150 K but with a refined microstructure. The results indicate that a dynamic bulk supercooling of 150 K may exist in the molten pool during the solidification of electron beam melted surfaces.
Munitz, A.↗
In-Flight Validation of the Metis Visible-Light Polarimeter Coronagraph on Board Solar Orbiter
Context. The Metis coronagraph is one of the remote sensing instruments of the ESA-NASA Solar Orbiter mission. The goal for the instrument is to enable the study of the solar atmosphere and solar wind by simultaneously acquiring images of the solar corona at two different wavelengths: visible light (VL), within a band ranging from 580 nm to 640 nm, and ultraviolet light, in the HI Lyα 121.6 ± 10 nm. The visible-light channel of the coronagraph includes a polarimeter with electro-optically modulating liquid crystal variable retarders to measure the linearly polarized brightness of the K-corona and derive the electron density. Aims. In this paper, we present the first in-flight validation results of the Metis polarimetric channel together with a comparison to the on-ground calibrations. This paper seeks to validate the first use of an electro-optical device, the liquid crystal-based polarimeter, in deep space and within a hard radiation environment. Methods. We used the orientation of the K-corona’s linear polarization vector during the roll maneuvers of the Space Orbiter spacecraft for the in-flight calibration. Results. The Metis coronagraph on board the Solar Orbiter shows good agreement with the on-ground measurements. The in-flight validation confirms the expected performance of the visible-light channel polarimeter. Furthermore, a comparison between the first polarized brightness value obtained by Metis and the polarized brightness values obtained by the space-based coronagraph LASCO and the ground-based coronagraph K-Cor shows the consistency of the Metis calibrated results.
Sun: corona↗
Review of melt inclusions in lunar rocks: constraints on melt and mantle composition and magmatic processes
Mineral-hosted melt inclusions provide a window into magmatic processes and pre-eruptive liquid compositions. Because melt inclusions are small (typically < 100 µm), the study of lunar melt inclusions is enabled by advancements of microbeam instrumental techniques. In the 1970s immediately following the Apollo and Luna missions, major and minor oxide concentrations of lunar melt inclusions were measured using electron microprobes. The data were used to understand magma evolution, and they revealed the immiscibility of two silicate liquids in the late stage of lunar magma evolution. More recently, the development of secondary ion mass spectrometry as well as laser ablation–inductively coupled plasma–mass spectrometry has enabled the measurement of key volatile elements and other trace elements in lunar melt inclusions, down to about the 0.1 ppm level. The applications of these instruments have ushered in a new wave of lunar melt inclusion studies. Recent advances have gone hand in hand with improved understanding of post-entrapment loss of volatiles. These studies have provided deep insights into pre-eruptive volatiles in lunar basalts, the abundance of volatiles in the lunar mantle, the isotopic ratios of some volatile elements, and the partition of trace elements between host olivine and melt inclusions. The recent studies of lunar melt inclusions have played a critical role in establishing a new paradigm of a fairly wet Moon with about 100 ppm H2O in the bulk silicate Moon (rather than a “bone-dry” Moon) and have been instrumental in developing an improved understanding of the origin and evolution of the Moon.
Youxue Zhang↗
Ion thruster system (8-cm) cyclic endurance test
This report describes the qualification test of an Engineering-Model 5-mN-thrust 8-cm-diameter mercury ion thruster which is representative of the Ion Auxiliary Propulsion System (IAPS) thrusters. Two of these thrusters are scheduled for future flight test. The cyclic endurance test described herein was a ground-based test performed in a vacuum facility with a liquid-nitrogen-cooled cryo-surface and a frozen mercury target. The Power Electronics Unit, Beam Shield, Gimal, and Propellant Tank that were used with the thruster in the endurance test are also similar to those of the IAPS. The IAPS thruster that will undergo the longest beam-on-time during the actual space test will be subjected to 7,055 hours of beam-on-time and 2,557 cycles during the flight test. The endurance test was successfully concluded when the mercury in the IAPS Propellant Tank was consumed. At that time, 8,471 hours of beam-on-time and 599 cycles had been accumulated. Subsequent post-test-evaluation operations were performed (without breaking vacuum) which extended the test values to 652 cycles and 9,489 hours of beam-on-time. The Power Electronic Unit (PEU) and thruster were in the same vacuum chamber throughout the test. The PEU accumulated 10,268 hr of test time with high voltage applied to the operating thruster or dummy load.
Dulgeroff, C. R.↗
Actively controlled shaft seals for aerospace applications
An electronically controlled mechanical seal for use as the purge gas seal in a liquid oxygen turbo pump has been fabricated and tested under transient operating conditions. The thickness of the lubricating film is controlled by adjusting the coning of the carbon face. This is accomplished by applying a voltage to a piezoelectric actuator to which the carbon face is bonded. The seal has been operated with a closed-loop control system that utilizes either the leakage rate or the seal face temperature as the feedback. Both speed and pressure transients have been imposed on the seal. The transient tests have demonstrated that the seal is capable of maintaining low leakage rates while limiting the face temperatures.
Salant, Richard F.↗