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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 199 records · Page 11
All sourcesNASA NTRSDOE OSTI
DOE OSTI2024

The anti-aromatic dianion and aromatic tetraanion of [18]annulene

π-Conjugated macrocycles behave differently from analogous linear chains because their electronic wavefunctions resemble a quantum particle on a ring, leading to aromaticity or anti-aromaticity. [18]Annulene, (CH) 18 , is the archetypal non-benzenoid aromatic hydrocarbon. Molecules with circuits of 4 n +2 π electrons, such as [18]annulene ( n =4), are aromatic, with enhanced stability and diatropic ring currents (magnetic shielding inside the ring), whereas those with 4 n π electrons, such as the dianion of [18]annulene, are expected to be anti-aromatic and exhibit the opposite behaviour. Here we use 1 H NMR spectroscopy to re-evaluate the structure of the [18]annulene dianion. We also show that it can be reduced further to an aromatic tetraanion, which has the same shape as the dianion. The crystal structure of the tetraanion lithium salt confirms its geometry and reveals a metallocene-like sandwich, with five Li + cations intercalated between two [18]annulene tetraanions. We also report a heteroleptic sandwich, with [18]annulene and corannulene tetraanion decks.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2025

The HIBEAM instrument at the European spallation source

The European spallation source (ESS) will be the world’s brightest neutron source and will open a new intensity frontier in particle physics. The HIBEAM collaboration aims to exploit the unique potential of the ESS with a dedicated ESS instrument for particle physics which offers world-leading capability in a number of areas. The HIBEAM program includes the first search in thirty years for free neutrons converting to antineutrons and searches for sterile neutrons, ultralight axion dark matter and nonzero neutron electric charge. This paper outlines the capabilities, design, infrastructure, and scientific potential of the HIBEAM program, including its dedicated beamline, neutron optical system, magnetic shielding and control, and detectors for neutrons and antineutrons. Additionally, we discuss the long-term scientific exploitation of HIBEAM, which may include measurements of the neutron electric dipole moment and precision studies of neutron decays.

47 OTHER INSTRUMENTATION↗
DOE OSTI2022

High-Sensitivity rf Detection Using an Optically Pumped Comagnetometer Based on Natural-Abundance Rubidium with Active Ambient-Field Cancellation

To detect a specific radio-frequency (rf) magnetic field, rf optically pumped magnetometers (OPMs) require a static magnetic field to set the Larmor frequency of the atoms equal to the frequency of interest. However, unshielded and variable magnetic field environments (e.g., an rf OPM on a moving platform) pose a problem for rf OPM operation. Here, we demonstrate the use of a natural-abundance rubidium vapor to make a comagnetometer to address this challenge. Our implementation builds upon the simultaneous application of several OPM techniques within the same vapor cell. First, we use a modified implementation of an OPM variometer based on 87 Rb to detect and actively cancel unwanted external fields at frequencies ≲60 Hz using active feedback to a set of field control coils. In this experiment, we exploit this stabilized field environment to implement a high-sensitivity rf magnetometer using 85 Rb. Using this approach, we demonstrate the ability to measure rf fields with a sensitivity of approximately 9 fT Hz -1/2 inside a magnetic shield in the presence of an applied field of approximately 20 μT along three mutually orthogonal directions. This demonstration opens up a path toward completely unshielded operation of a high-sensitivity rf OPM.

47 OTHER INSTRUMENTATION↗
DOE OSTI2020

22 K superconductivity in Ba Fe 2 As 2 exposed to F 2

Several previous reports on undoped AEFe 2 As 2 (AE = alkaline earth metal) point to drops in resistivity indicative of possible superconductivity and some degree of Meissner effect in the magnetic susceptibility. Also, based on both resistivity and magnetic susceptibility measurements, controlled exposure to water vapor has been shown to induce superconductivity in AEFe 2 As 2 . In our study, BaFe 2 As 2 single crystals grown using the self-flux method showed a full resistive drop around 22 K and magnetic shielding, when exposed to fluorine gas postgrowth. Our measurements indicate electron (donor) doping via atomic substitution of F for As is concurrent with the observed superconductivity, which sheds light on the likely effect of exposure to water vapor in previous work. Like doping experiments (such as substitution of Co for Fe, P for As, or K for Ba) in AEFe 2 As 2 to date, the present work is consistent with suppression of the spin density wave transition coincident with the appearance of T c . In addition to answering the puzzle of superconductivity in undoped or water vapor exposed AEF 2 As 2 , our results also represent a fast (20 min exposure to 5% F in He) and reliable method suitable for inducing superconductivity in thin films of AEFe 2 As 2 . As a result, some supportive work on BaFe 2 As 2 exposed to Cl 2 is also presented.

36 MATERIALS SCIENCE↗
DOE OSTI2022

Magnetic Designs of New First Target Beamline Magnets for the ORNL SNS Upgrade

The Spallation Neutron Source (SNS) at ORNL currently is being upgraded from 1.0 GeV to 1.3 GeV. Several water-cooled magnets should be upgraded to transport 30% of higher beam energy. New chicane, injection/extraction septum, and Lambertson magnets were designed. Designing the magnets was a challenging task because the new magnets required good combined integrated field quality and needed to occupy the old magnets space but with about 20% greater integrated magnetic field. Additional strong requirements applied to the magnets fringe field do not disturb the circulating beam. The special field profiles had to be provided in foil areas between magnets. The analysis described here was based on OPERA3D simulations. A special technique was used for analyzing the integrated field harmonics. Initially, the particle track was simulated, and integrated field components were calculated along this track for the reference radius, which were used for the harmonics analysis. In addition, 3D field maps were provided for beam optics simulations. The final beamline analysis confirmed good beam transmission and low losses.

3d field maps↗
DOE OSTI2026

Design of a 915 MHz conduction-cooled cryomodule

High-power, compact, continuous-wave (CW) linear electron accelerators with beam energies of up to 10 MeV are being considered for possible industrial applications. Conduction-cooled, superconducting radio-frequency (SRF) technology allows operating such machines at high electrical efficiency, thereby reducing the operating cost significantly. A prototype conduction-cooled SRF cryomodule has been designed and components are currently being manufactured. The cryomodule features a two-cell, 915 MHz SRF cavity, two cryocoolers, a fundamental power coupler, two magnetic shields, a thermal shield and warm-to-cold transitions. The cryomodule has been designed to be able to provide an energy gain of 3.5 MeV to a CW electron beam with a current of 5 mA. This contribution focusses on thermal and mechanical design aspects of the cryomodule.

Ciovati, G. [Old Dominion Univ., Norfolk, VA (Unit↗
DOE OSTI2021

Pulsed Magnetic Gradiometry in Earth's Field [Poster]

We describe a novel pulsed magnetic gradiometer based on the optical interference of sidebands generated using two spatially separated alkali vapor cells. In contrast to traditional magnetic gradiometers, our approach provides a direct readout of the gradient field without the intermediate step of subtracting the outputs of two spatially separated magnetometers. Operation of the gradiometer in multiple field orientations is discussed. The noise floor is measured as low as 25$\frac{fT}{\sqrt{Hz-cm}}$ in a room without magnetic shielding.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
DOE OSTI2025

Development of Transformative Preparation Methods to Push up High Q&G Performance of FRIB Spare HWR Cryomodule Cavities

The FRIB accelerator project construction, a top priority of US nuclear science, was completed in January 2022, and is now moving to user operation. The stable and reliable operation of the accelerating cryomodules is essential in achieving/fulfilling DOE and user expectations. So far, FRIB cryomodules meet all FRIB specifications for cavity performance. However, during the lifetime of machine operation, degradation of cryomodule performance is possible, as reported in similar operating facilities (CEBAF, SNS). If cryomodule degradation is observed at FRIB, the under-performing cryomodule will require replacement/maintenance. In effort to manage operational reliability, FRIB plans to construct a 0.53 half-wave cryomodule to serve as an active spare. In a parallel effort, FRIB will also work toward increasing operational Q and gradient of spare cryomodule cavities to gain an overall performance margin to support future operational reliability. The current FRIB cavity designs have a potential to operate at gradients higher than 8 MV/m, but are currently limited by field emission (FE) and/or high field Q slope (HFQS); known issue in buffered chemical polished (BCP) treated cavities. The proposal looks to develop transformative surface preparation treatments to improve the operational gradient of spare cryomodules higher than 10 MV/m while maintaining high Q. Thus, increasing operational margin by 30 - 50%. With the goal to improve operational reliability set, the proposal will investigate multiple objectives as possible paths forward to achieve an overall increase in cavity performance and gain a better understanding of SRF limiting mechanisms. The proposal will study the application of different chemical surface treatments to 0.53 half-wave cavities, with the addition of low temperature bakes (LTB), and measure their effects on accelerating performance. Proposed chemical treatments to be explored in this proposal include conventional EP acid mixtures, as well as innovated EP and BCP acid mixtures designed to simplify processing paths in migrating FE and HFQS. The proposed transformative treatment wet N-doping also has the potential to replicate recent advancements in SRF technology relating to nitrogen doping and high Q operation without the requirement for an ultra-high vacuum annealing furnace; currently being developed at FNAL and JLAB. In parallel, high Q performance relating to flux trapping will be investigated with the installation of a second layer of magnetic shielding in the vertical test Dewar. The research objectives presented in the proposal, and their corresponding effects on cavity performance, will provide essential knowledge and future guidance to the SRF community and provide possible paths for future SRF based projects and applications.

43 PARTICLE ACCELERATORS↗
NASA NTRS1971

Nitrogen fixation studies, lead detection in living plants, and solar wind analysis

Progress is reported for research on the following: (1) magnetically shielded test facility studies; (2) electrochemistry of B10C2H12, B9CH10(-), and preparation of tumor specific boron containing materials for use in cancer therapy; (3) histochemical method for determining lead in living plant tissue; (4) diamond cementing; (5) analysis of solar wind using the washings of lunar fines; and (6) environmental engineering.

Libby, W. F.↗
NASA NTRS1972

Fusion power for space propulsion.

Principles of operation, interplanetary orbit-to-orbit mission capabilities, technical problems, and environmental safeguards are examined for thermonuclear fusion propulsion systems. Two systems examined include (1) a fusion-electric concept in which kinetic energy of charged particles from the plasma is converted into electric power (for accelerating the propellant in an electrostatic thrustor) by the van de Graaf generator principle and (2) the direct fusion rocket in which energetic plasma lost from the reactor has a suitable amount of added propellant to obtain the optimum exhaust velocity. The deuterium-tritium and the deuterium/helium-3 reactions are considered as suitable candidates, and attention is given to problems of cryogenic refrigeration systems, magnet shielding, and high-energy particle extraction and guidance.

Roth, R.↗
NASA NTRS1976

DC-to-DC conversion with voltage multipliers

Compact device uses transformerless capacitor/diode voltage multiplier. Advantages include efficiency at high power levels, increased reliability due to elimination of magnetics and associated electrical transients, no magnetic shielding requirement, and adaptability to modular or integrated circuit systems.

Harrigill, W. T., Jr.↗
NASA NTRS1976

A mechanism for inducing climatic variations through ozone destruction: Screening of galactic cosmic rays by solar and terrestrial magnetic fields

A perturbation analysis, allowing for temperature and opacity feedbacks, is developed to calculate depletions in the O3 abundance and reductions of stratospheric solar heating that result from increases in NOx concentration. A pair of perturbation coefficients give the reduction in O3 and temperature through the stratosphere for a specified NOx increase. This type of analysis illustrates the tendency for various levels to self-heal when a perturbation occurs. Physical arguments indicate that the expected sign of the climatic effect is correct, with colder surface temperatures produced by reduced magnetic shielding. In addition, four qualitative reasons are suggested for thinking that significant ozone reductions by cosmic ray influxes will lead to an increased terrestrial albedo from stratospheric condensation. In this view, long-term (approximately 10,000 years) climatic changes have resulted from secular geomagnetic variations while shorter (approximately 100 years) excursions are related to changes in solar activity.

Chamberlain, J. W.↗
NASA NTRS1976

Antenna radiation patterns in the whistler wave regime measured in a large laboratory plasma

Antenna radiation patterns of balanced electric dipoles and shielded magnetic loop antennas are obtained by measuring the relative wave amplitude with a small receiver antenna scanned around the exciter in a large uniform collisionless magnetized laboratory plasma in the whistler wave regime. The boundary effects are assumed to be negligible even for many farfield patterns. Characteristic differences are observed between electrically short and long antennas, the former exhibiting resonance cones and the latter showing dipole-like antenna patterns along the magnetic field. Resonance cones due to small electric dipoles and magnetic loops are observed in both the near zone and the far zone. A self-focusing process is revealed which produces a pencil-shaped field-aligned radiation pattern.

Stenzel, R. L.↗
NASA NTRS1976

NASA atomic hydrogen standards program - An update

Some of the design features of NASA hydrogen masers are discussed including the large hydrogen source bulb, the palladium purified, the state selector, the replaceable pumps, the small entrance stem, magnetic shields, the elongated storage bulb, the aluminum cavity, the electronics package, and the autotuner. Attention is also given to the reliability and operating life of these hydrogen atomic standards.

Reinhardt, V. S.↗
NASA NTRS1977

A mechanism for inducing climatic variations through the stratosphere - Screening of cosmic rays by solar and terrestrial magnetic fields

The ability of heliomagnetic and geomagnetic fields to bring about climatic variations of long period is examined theoretically. A chemical relationship between low-energy cosmic rays and ozone balance in the stratosphere is sought as a crucial clue to historical changes in earth climate. A perturbation analysis is developed to arrive at zone depletion and reduction of stratospheric solar heating resulting from increased NOx concentration; temperature feedback and opacity feedback are allowed for. Modulation of galactic cosmic-radiation fluxes and ozone destruction in the stratosphere, colder surface temperatures associated with reduced magnetic shielding, and redistribution with height of total ozone decrease are explored.

Chamberlain, J. W.↗