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NASA NTRS2004

PETI-298 Prepared by Microwave Synthesis: Neat Resin and Composite Properties

PETI-298 is a high temperature/high performance matrix resin that is processable into composites by resin transfer molding (RTM), resin infusion and vacuum assisted RTM techniques. It is typically synthesized in a polar aprotic solvent from the reaction of an aromatic anhydride and a combination of diamines and endcapped with phenylethynylphthalic anhydride. Microwave synthesis of PETI-298 was investigated as a means to eliminate solvent and decrease reaction time. The monomers were manually mixed and placed in a microwave oven for various times to determine optimum reaction conditions. The synthetic process was subsequently scaled-up to 330g. Three batches were synthesized and combined to give 1 kg of material that was characterized for thermal and rheological properties and compared to PETI-298 prepared by the classic solution based synthetic method. The microwave synthesized PETI-298 was subsequently used to fabricate flat laminates on T650 carbon fabric by RTM. The composite panels were analyzed and mechanical properties determined and compared with those fabricated from PETI-298 prepared by the classic solution method. The microwave synthesis process and characterization of neat resin and carbon fiber reinforced composites fabricated by RTM will be presented. KEY WORDS: Resin Transfer Molding, High Temperature Polymers, Phenylethynyl Terminated Imides, Microwave Synthesis

Smith, Joseph G.↗

NASA NTRS2004

High-Temperature Probe Station Developed to Characterize Microwave Devices Through 500 C

A photograph and a block diagram of the high-temperature probe station are shown. The system consists of the ceramic heater mounted on a NASA shuttle tile insulator, a direct current power supply, a personal-computer-based data acquisition and temperature controller, microwave probes, a microscope, and a network analyzer. The ability to perform microwave tests at high temperatures is becoming necessary. There is now a need for sensors and communication circuits that can operate at 500 C and above for aircraft engine development and monitoring during flight. To address this need, researchers have fabricated devices using wide bandgap semiconductors such as SiC with targeted operating temperatures of 500 to 600 C. However, the microwave properties of these devices often change drastically with temperature, so any designs that are intended to be used in such an environment must be characterized at high temperatures. For some reliability, lifetime, and direct-current testing, the device under test can be packaged and characterized in an oven. However, for RF and microwave measurements, it is usually not possible to establish a calibrated reference plane at the device terminals within a package. In addition, the characteristics of the package would vary over a 500 C temperature range, and this would have to be accounted for when the data were analyzed. A high temperature probe station allows circuits and devices to be characterized through on wafer measurements across a broad temperature range with known reference plane. The conventional, commercially available thermal wafer-probe stations that are used to evaluate microwave devices across a controlled temperature range have a typical upper limit of 200 C. Standalone thermal heating chucks are available with an extended upper temperature range of 300 to 400 C. To effectively characterize devices at temperatures up to and surpassing 500 C, Glenn researchers developed a custom probe station. In the past, custom probe stations have been developed to test devices under other extreme environments, such as cryogenic temperatures as low as 37 K. Similarly, this custom probe station was specifically modified for high-temperature use. It allows devices to be measured quickly and flexibly, without the use of wire bonds and test fixtures. The probe station is shown making scattering parameter measurements from 1 to 50 GHz with a Hewlett-Packard 8510C Network Analyzer. There is a half-wafer of silicon directly on top of the heater to provide a uniform heated platform for our sample. A quarter wafer of silicon carbide forms the substrate for our test circuit of several transmission lines.

Downey, Alan N.↗

NASA NTRS2007

Microwave Extraction of Water from Lunar Regolith Simulant

Nearly a decade ago the DOD Clementine lunar orbital mission obtained data indicating that the permanently shaded regions at the lunar poles may have permanently frozen water in the lunar soil. Currently NASA's Robotic Lunar Exploration Program, RLEP-2, is planned to land at the lunar pole to determine if water is present. The detection and extraction of water from the permanently frozen permafrost is an important goal for NASA. Extraction of water from lunar permafrost has a high priority in the In-Situ Resource Utilization, ISRU, community for human life support and as a fuel. The use of microwave processing would permit the extraction of water without the need to dig, drill, or excavate the lunar surface. Microwave heating of regolith is potentially faster and more efficient than any other heating methods due to the very low thermal conductivity of the lunar regolith. Also, microwaves can penetrate into the soil permitting water removal from deep below the lunar surface. A cryogenic vacuum test facility was developed for evaluating the use of microwave heating and water extraction from a lunar regolith permafrost simulant. Water is obtained in a cryogenic cold trap even with soil conditions below 0 C. The results of microwave extraction of water experiments will be presented.

Ethridge, Edwin C.↗

NASA NTRS2006

Microwave Signatures of Snow on Sea Ice: Modeling

Accurate knowledge of snow-depth distribution over sea ice is critical for polar climate studies. Current snow-depth-over-sea-ice retrieval algorithms do not sufficiently account for variations in snow and ice physical properties that can affect the accuracy of retrievals. For this reason, airborne microwave observations were coordinated with ground-based measurements of snow depth and snow properties in the vicinity of Barrow, AK, in March 2003. In this paper, the effects of snowpack properties and ice conditions on microwave signatures are examined using detailed surface-based measurements and airborne observations in conjunction with a thermal microwave-emission model. A comparison of the Microwave Emission Model of Layered Snowpacks (MEMLS) simulations with detailed snowpack and ice data from stakes along the Elson Lagoon and the Beaufort Sea and ra- 'diometer data taken from low-level flights using a Polarimetric Scanning Radiometer (PSR-A) shows that MEMLS can be used to simulate snow on sea ice and is a useful tool for understanding the limitations of the snow-depth algorithm. Analysis of radiance data taken over the Elson Lagoon and the Beaufort Sea using MEMLS suggests that the radiometric differences between the two locations are due to the differences in sea-ice emissivity. Furthermore, measured brightness temperatures suggest that the current snow-depth retrieval algorithm is sufficient for areas of smooth first-year sea ice, whereas new algorithm coefficients are needed for rough first-year sea ice. Snowpack grain size and density remain an unresolved issue for snow-depth retrievals using passive-microwave radiances.

Powell, D. C.↗

NASA NTRS2004

Microwave bonding of thin film metal coated substrates

Bonding of materials such as MEMS materials is carried out using microwaves. High microwave absorbing films are placed within a microwave cavity containing other less microwave absorbing materials, and excited to cause selective heating in the skin depth of the films. This causes heating in one place more than another. This thereby minimizes unwanted heating effects during the microwave bonding process.

Barmatz, Martin B.↗

NASA NTRS2007

Recent Results of a New Microwave SQUID Multiplexer

We are developing a proof-of-concept microwave SQUID multiplexer containing four SQUIDs coupled to GHz frequency resonant circuits and fed with a single microwave readout line. The resonators are half-wave coplanar waveguide sections and are similar to the structures used for the microwave kinetic inductance detectors developed in our group. Optimal values for the interdigital gap capacitors were determined to maximize the sensitivity of the transmitted and reflected microwave signal with respect to changes in the dynamic resistance of the SQUID. The dc current-bias line for the SQUID has an in-line inductive high frequency filter to minimize coupling between the bias line and resonator. A high frequency modulation scheme is proposed to eliminate the need for individual flux biasing of the SQUIDs, which extends the dynamic range of the readout. In this scheme a common modulation signal is imposed on each SQUID and the received signal is demodulated at one and two times the modulation frequency to maintain sensitivity at any flux state. We present the recent results of the microwave SQUID multiplexer system operating at a readout frequency range of 10 - 11GHz.

superconducting quantum interference device (SQUID↗

NASA NTRS2010

GPM Microwave Imager Engineering Model Results

The Global Precipitation Measurement (GPM) Microwave Imager (GMI) Instrument is being developed by Ball Aerospace and Technology Corporation (BATC) for the GPM program at NASA Goddard. The Global Precipitation Measurement (GPM) mission is an international effort managed by the National Aeronautics and Space Administration (NASA) to improve climate, weather, and hydro-meteorological predictions through more accurate and more frequent precipitation measurements. The GPM Microwave Imager (GMI) will be used to make calibrated, radiometric measurements from space at multiple microwave frequencies and polarizations. GMI will be placed on the GPM Core Spacecraft together with the Dualfrequency Precipitation Radar (DPR). The DPR is two-frequency precipitation measurement radar, which will operate in the Ku-band and Ka-band of the microwave spectrum. The Core Spacecraft will make radiometric and radar measurements of clouds and precipitation and will be the central element ofGPM's space segment. The data products from GPM will provide information concerning global precipitation on a frequent, near-global basis to meteorologists and scientists making weather forecasts and performing research on the global energy and water cycle, precipitation, hydrology, and related disciplines. In addition, radiometric measurements from GMI and radar measurements from the DPR will be used together to develop a retrieval transfer standard for the purpose of calibrating precipitation retrieval algorithms. This calibration standard will establish a reference against which other retrieval algorithms using only microwave radiometers (and without the benefit of the DPR) on other satellites in the GPM constellation will be compared.

Newell, David↗

NASA NTRS2010

GPM Microwave Imager Design, Predicted Performance and Status

The Global Precipitation Measurement (GPM) Microwave Imager (GMI) Instrument is being developed by Ball Aerospace and Technology Corporation (BATC) for the GPM program at NASA Goddard. The Global Precipitation Measurement (GPM) mission is an international effort managed by the National Aeronautics and Space Administration (t.JASA) to improve climate, weather, and hydro-meteorological predictions through more accurate and more frequent precipitation measurements. The GPM Microwave Imager (GMI) will be used to make calibrated, radiometric measurements from space at multiple microwave frequencies and polarizations. GMI will be placed on the GPM Core Spacecraft together with the Dual-frequency Precipitation Radar (DPR). The DPR is two-frequency precipitation measurement radar, which will operate in the Ku-band and Ka-band of the microwave spectrum. The Core Spacecraft will make radiometric and radar measurements of clouds and precipitation and will be the central element of GPM's space segment. The data products from GPM will provide information concerning global precipitation on a frequent, near-global basis to meteorologists and scientists making weather forecasts and performing research on the global energy and water cycle, precipitation, hydrology, and related disciplines. In addition, radiometric measurements from GMI and radar measurements from the DPR will be used together to develop a retrieval transfer standard for the purpose of calibrating precipitation retrieval algorithms. This calibration standard will establish a reference against which other retrieval algorithms using only microwave radiometers (and without the benefit of the DPR) on other satellites in the GPM constellation will be compared.

Krimchansky, Sergey↗

NASA NTRS2009

REFAME: Rain Estimation Using Forward Adjusted-Advection of Microwave Estimates

Sensors flying on satellites provide the only practical means of estimating the precipitation that falls over the entire globe, particularly across the vast unpopulated expanses of Earth s oceans. The sensors that observe the Earth using microwave frequencies provide the best data, but currently these are mounted only on satellites flying in "low Earth orbit". Such satellites constantly move across the Earth s surface, providing snapshots of any given location every 12-36 hours. The entire constellation of low-orbit satellites numbers less than a dozen, and their orbits are not coordinated, so a location will frequently go two or more hours between snapshots. "Geosynchronous Earth orbit" (GEO) satellites continuously observe the same region of the globe, allowing them to provide very frequent pictures. For example, the "satellite movies" shown on television come from GEO satellites. However, the sensors available on GEO satellites cannot match the skill of the low-orbit microwave sensors in estimating precipitation. It is perhaps obvious that scientists should try to combine these very different kinds of data, taking advantage of the strengths of each, but this simple concept has proved to be a huge challenge. The scheme in this paper is "Lagrangian", meaning we follow the storm systems, rather than being tied to a fixed grid of boxes on the Earth s surface. Whenever a microwave snapshot occurs, we gladly use the resulting precipitation estimate. Then at all the times between the microwave snapshots we force the storm system to make a smooth transition from one snapshot s values to the next. We know that a lot more changes occur between the snapshots, but this smooth transition the best we can do with the microwave data alone. The key new contribution in this paper is that we also look at the relative variations in the GEO estimates during these in-between times and force the estimated changes in the precipitation to have similar variations. Preliminary testing shows that this approach has enough promise that it should be developed and studied.

Behrangi, Ali↗

NASA NTRS2011

Using Microwaves to Heat Lunar Soil

This slide presentation reviews the use of microwaves to heat lunar soil in order to obtain water. There appears to be large amounts of water in the lunar poles, in Martian areas in lower latitudes and some of the Moons of Jupiter. The presence of water in the south lunar polar region was demonstrated by the Lunar CRater Observation and Sensing Satellite (LCROSS) mission. Microwaves can be used to extract water from lunar soil without excavation. Using microwaves on a lunar soil simulant at least 95% of the water from the regolith permafrost simulant was extracted (2 minutes). The process is modeled using COMSOL Multiphysics Finite Element analysis microwave physics module and demonstrated usingan experiment of an microwave apparatus on a rover.

Ethridge, Edwin C.↗

NASA NTRS2005

Microwave Treatment of Prostate Cancer and Hyperplasia

Microwave ablation in the form of microwave energy applied to a heart muscle by a coaxial catheter inserted in a vein in the groin area can be used to heat and kill diseased heart cells. A microwave catheter has been developed to provide deep myocardial ablation to treat ventricular tachycardia by restoring appropriate electrical activity within the heart and eliminating irregular heartbeats. The resulting microwave catheter design, which is now being developed for commercial use in treating ventricular tachycardia, can be modified to treat prostate cancer and benign prostatic hyperplasia (BPH). Inasmuch as the occurrence of BPH is increasing currently 350,000 operations per year are performed in the United States alone to treat this condition this microwave catheter has significant commercial potential.

Arndt, G. Dickey↗

NASA NTRS2011

A First-Order Radiative Transfer Model for Microwave Radiometry of Forest Canopies at L-Band

In this study, a first-order radiative transfer (RT) model is developed to more accurately account for vegetation canopy scattering by modifying the basic Tau-Omega model (the zero-order RT solution). In order to optimally utilize microwave radiometric data in soil moisture (SM) retrievals over vegetated landscapes, a quantitative understanding of the relationship between scattering mechanisms within vegetation canopies and the microwave brightness temperature is desirable. The first-order RT model is used to investigate this relationship and to perform a physical analysis of the scattered and emitted radiation from vegetated terrain. This model is based on an iterative solution (successive orders of scattering) of the RT equations up to the first order. This formulation adds a new scattering term to the . model. The additional term represents emission by particles (vegetation components) in the vegetation layer and emission by the ground that is scattered once by particles in the layer. The model is tested against 1.4-GHz brightness temperature measurements acquired over deciduous trees by a truck-mounted microwave instrument system called ComRAD in 2007. The model predictions are in good agreement with the data, and they give quantitative understanding for the influence of first-order scattering within the canopy on the brightness temperature. The model results show that the scattering term is significant for trees and modifications are necessary to the . model when applied to dense vegetation. Numerical simulations also indicate that the scattering term has a negligible dependence on SM and is mainly a function of the incidence angle and polarization of the microwave observation. Index Terms Emission,microwave radiometry, scattering, soil, vegetation.

Kurum, Mehmet↗

NASA NTRS2011

Land Surface Microwave Emissivities Derived from AMSR-E and MODIS Measurements with Advanced Quality Control

A microwave emissivity database has been developed with data from the Advanced Microwave Scanning Radiometer-EOS (AMSR-E) and with ancillary land surface temperature (LST) data from the Moderate Resolution Imaging Spectroradiometer (MODIS) on the same Aqua spacecraft. The primary intended application of the database is to provide surface emissivity constraints in atmospheric and surface property retrieval or assimilation. An additional application is to serve as a dynamic indicator of land surface properties relevant to climate change monitoring. The precision of the emissivity data is estimated to be significantly better than in prior databases from other sensors due to the precise collocation with high-quality MODIS LST data and due to the quality control features of our data analysis system. The accuracy of the emissivities in deserts and semi-arid regions is enhanced by applying, in those regions, a version of the emissivity retrieval algorithm that accounts for the penetration of microwave radiation through dry soil with diurnally varying vertical temperature gradients. These results suggest that this penetration effect is more widespread and more significant to interpretation of passive microwave measurements than had been previously established. Emissivity coverage in areas where persistent cloudiness interferes with the availability of MODIS LST data is achieved using a classification-based method to spread emissivity data from less-cloudy areas that have similar microwave surface properties. Evaluations and analyses of the emissivity products over homogeneous snow-free areas are presented, including application to retrieval of soil temperature profiles. Spatial inhomogeneities are the largest in the vicinity of large water bodies due to the large water/land emissivity contrast and give rise to large apparent temporal variability in the retrieved emissivities when satellite footprint locations vary over time. This issue will be dealt with in the future by including a water fraction correction. Also note that current reliance on the MODIS day-night algorithm as a source of LST limits the coverage of the database in the Polar Regions. We will consider relaxing the current restriction as part of future development.

Moncet, Jean-Luc↗

NASA NTRS2011

Microwave Tissue Soldering for Immediate Wound Closure

A novel approach for the immediate sealing of traumatic wounds is under development. A portable microwave generator and handheld antenna are used to seal wounds, binding the edges of the wound together using a biodegradable protein sealant or solder. This method could be used for repairing wounds in emergency settings by restoring the wound surface to its original strength within minutes. This technique could also be utilized for surgical purposes involving solid visceral organs (i.e., liver, spleen, and kidney) that currently do not respond well to ordinary surgical procedures. A miniaturized microwave generator and a handheld antenna are used to deliver microwave energy to the protein solder, which is applied to the wound. The antenna can be of several alternative designs optimized for placement either in contact with or in proximity to the protein solder covering the wound. In either case, optimization of the design includes the matching of impedances to maximize the energy delivered to the protein solder and wound at a chosen frequency. For certain applications, an antenna could be designed that would emit power only when it is in direct contact with the wound. The optimum frequency or frequencies for a specific application would depend on the required depth of penetration of the microwave energy. In fact, a computational simulation for each specific application could be performed, which would then match the characteristics of the antenna with the protein solder and tissue to best effect wound closure. An additional area of interest with potential benefit that remains to be validated is whether microwave energy can effectively kill bacteria in and around the wound. Thus, this may be an efficient method for simultaneously sterilizing and closing wounds.

Arndt, G. Dickey↗

NASA NTRS2012

Advances in Assimilation of Satellite-Based Passive Microwave Observations for Soil-Moisture Estimation

Satellite-based microwave measurements have long shown potential to provide global information about soil moisture. The European Space Agency (ESA) Soil Moisture and Ocean Salinity (SMOS, [1]) mission as well as the future National Aeronautics and Space Administration (NASA) Soil Moisture Active and Passive (SMAP, [2]) mission measure passive microwave emission at L-band frequencies, at a relatively coarse (40 km) spatial resolution. In addition, SMAP will measure active microwave signals at a higher spatial resolution (3 km). These new L-band missions have a greater sensing depth (of -5cm) compared with past and present C- and X-band microwave sensors. ESA currently also disseminates retrievals of SMOS surface soil moisture that are derived from SMOS brightness temperature observations and ancillary data. In this research, we address two major challenges with the assimilation of recent/future satellite-based microwave measurements: (i) assimilation of soil moisture retrievals versus brightness temperatures for surface and root-zone soil moisture estimation and (ii) scale-mismatches between satellite observations, models and in situ validation data.

De Lannoy, Gabrielle J. M.↗

NASA NTRS2012

Objective Characterization of Snow Microstructure for Microwave Emission Modeling

Passive microwave (PM) measurements are sensitive to the presence and quantity of snow, a fact that has long been used to monitor snowcover from space. In order to estimate total snow water equivalent (SWE) within PM footprints (on the order of approx 100 sq km), it is prerequisite to understand snow microwave emission at the point scale and how microwave radiation integrates spatially; the former is the topic of this paper. Snow microstructure is one of the fundamental controls on the propagation of microwave radiation through snow. Our goal in this study is to evaluate the prospects for driving the Microwave Emission Model of Layered Snowpacks with objective measurements of snow specific surface area to reproduce measured brightness temperatures when forced with objective measurements of snow specific surface area (S). This eliminates the need to treat the grain size as a free-fit parameter.

Durand, Michael↗

NASA NTRS2013

Hyperspectral Microwave Atmospheric Sounder (HyMAS) Architecture and Design Accommodations

The Hyperspectral Microwave Atmospheric Sounder (HyMAS) is being developed at Lincoln Laboratories and accommodated by the Goddard Space Flight Center for a flight opportunity on a NASA research aircraft. The term "hyperspectral microwave" is used to indicate an all-weather sounding that performs equivalent to hyperspectral infrared sounders in clear air with vertical resolution of approximately 1 km. Deploying the HyMAS equipped scanhead with the existing Conical Scanning Microwave Imaging Radiometer (CoSMIR) shortens the path to a flight demonstration. Hyperspectral microwave is achieved through the use of independent RF antennas that sample the volume of the Earth s atmosphere through various levels of frequencies, thereby producing a set of dense, spaced vertical weighting functions. The simulations proposed for HyMAS 118/183-GHz system should yield surface precipitation rate and water path retrievals for small hail, soft hail, or snow pellets, snow, rainwater, etc. with accuracies comparable to those of the Advanced Technology Microwave Sounder. Further improvements in retrieval methodology (for example, polarization exploitation) are expected. The CoSMIR instrument is a packaging concept re-used on HyMAS to ease the integration features of the scanhead. The HyMAS scanhead will include an ultra-compact Intermediate Frequency Processor (IFP) module that is mounted inside the door to improve thermal management. The IFP is fabricated with materials made of Low-Temperature Co-fired Ceramic (LTCC) technology integrated with detectors, amplifiers, A/D conversion and data aggregation. The IFP will put out 52 channels of 16 bit data comprised of 4-9 channel data streams for temperature profiles and 2-8 channel streams for water vapor. With the limited volume of the existing CoSMIR scanhead and new HyMAS front end components, the HyMAS team at Goddard began preliminary layout work inside the new drum. Importing and re-using models of the shell, the scan head computer, and the slip rings developed for CoSMIR was the starting point. The next step was to modify the antenna faceplate to accommodate the dimensions of the three dual polarization Gaussian Optics Antenna (GOA) assemblies. Two mechanical concepts for the core technology, the hyperspectral IFP, were captured in a design tradeoff. Connector models considered minimum bend radii for the IFP analog connectors. Hyperspectral imaging is accomplished by strategically using a short wavelength intermediate frequency of 18-29 GHz, and thus reducing the size of components in the connection of the front end to the IFP. The SMK (2.92mm) Series connector will lay near the hinge line to minimize its flexing. The digital output of the IFP will use a Serial Peripheral Interface (SPI) that must be accommodated by the scan head computer. To make that computer more reliable, maintainable, and forward compatible with the 52 HyMAS channels, a testbed of the scan head, calibration, and archive computers and the PIC24 microprocessor that resides on the IFP is in development. The computers will be programmed using a new framework application called Interoperable Remote Component (IRC). This software allows flexibility to program computers that communicate with each other and can adapt easily to the emerging HyMAS requirements for data format, algorithms, and graphical user interface (GUI). It is expected that the CoSMIR instrument will cut over to the IRC after it is adapted on an updated CoSMIR testbed.

Hilliard, Lawrence↗

NASA NTRS2012

Wideband Agile Digital Microwave Radiometer

The objectives of this work were to take the initial steps needed to develop a field programmable gate array (FPGA)- based wideband digital radiometer backend (>500 MHz bandwidth) that will enable passive microwave observations with minimal performance degradation in a radiofrequency-interference (RFI)-rich environment. As manmade RF emissions increase over time and fill more of the microwave spectrum, microwave radiometer science applications will be increasingly impacted in a negative way, and the current generation of spaceborne microwave radiometers that use broadband analog back ends will become severely compromised or unusable over an increasing fraction of time on orbit. There is a need to develop a digital radiometer back end that, for each observation period, uses digital signal processing (DSP) algorithms to identify the maximum amount of RFI-free spectrum across the radiometer band to preserve bandwidth to minimize radiometer noise (which is inversely related to the bandwidth). Ultimately, the objective is to incorporate all processing necessary in the back end to take contaminated input spectra and produce a single output value free of manmade signals to minimize data rates for spaceborne radiometer missions. But, to meet these objectives, several intermediate processing algorithms had to be developed, and their performance characterized relative to typical brightness temperature accuracy re quirements for current and future microwave radiometer missions, including those for measuring salinity, soil moisture, and snow pack.

Gaier, Todd C.↗