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NASA NTRS1988

Bismaleimide-vinylpolystyrylpyridine graphite composites

Flammability, thermal, and selected mechanical properties of composites fabricated with epoxy and other thermally stable resin matrices are described. Properties which were measured included limiting-oxygen index, smoke evolution, thermal degradation products, total-heat release, heat-release rates, mass loss, flame spread, ignition resistance, thermogravimetric analysis and selected mechanical properties. This paper describes the properties of eight different graphite composite panels fabricated using four different resin matrices and two types of graphite reinforcement. The resin matrices included: XU71775/H795, a blend of vinylpolystyrylpyridine and bismaleimide; H795, a bismaleimide; Cycom 6162, a phenolic; and PSP 6022M, a polystyrylpyridine. The graphite fiber used was AS-4 in the form of either tape or fabric. The properties of these composites were compared with epoxy composites. It was determined that the blend of vinylpolystyrylpyridine and bismaleimide (XU71775/H795) with the graphite tape was the optimum design giving the lowest heat release rate.

Kourtides, D. A.↗

NASA NTRS2004

Analysis of Composite Skin-Stiffener Debond Specimens Using a Shell/3D Modeling Technique and Submodeling

The application of a shell/3D modeling technique for the simulation of skin/stringer debond in a specimen subjected to tension and three-point bending was studied. The global structure was modeled with shell elements. A local three-dimensional model, extending to about three specimen thicknesses on either side of the delamination front was used to model the details of the damaged section. Computed total strain energy release rates and mixed-mode ratios obtained from shell/3D simulations were in good agreement with results obtained from full solid models. The good correlation of the results demonstrated the effectiveness of the shell/3D modeling technique for the investigation of skin/stiffener separation due to delamination in the adherents. In addition, the application of the submodeling technique for the simulation of skin/stringer debond was also studied. Global models made of shell elements and solid elements were studied. Solid elements were used for local submodels, which extended between three and six specimen thicknesses on either side of the delamination front to model the details of the damaged section. Computed total strain energy release rates and mixed-mode ratios obtained from the simulations using the submodeling technique were not in agreement with results obtained from full solid models.

OBrien, T. Kevin↗

NASA NTRS1987

Review of thermal properties of graphite composite materials

Flammability, thermal, and selected mechanical properties of composites fabricated with epoxy and other thermally stable resin matrices are described. Properties which were measured included limiting-oxygen index, smoke evolution, thermal degradation products, total-heat release, heat-release rates, mass loss, flame spread, ignition resistance, thermogravimetric analysis, and selected mechanical properties. The properties of 8 different graphite composite panels fabricated using four different resin matrices and two types of graphite reinforcement are described. The resin matrices included: XU71775/H795, a blend of vinyl polystyryl pyridine and bismaleimide; H795, a bismaleimide; Cycom 6162, a phenolic; and PSP 6022M, a polystyryl pyridine. The graphite fiber used was AS-4 in the form of either tape or fabric. The properties of these composites were compared with epoxy composites. It was determined that the blend of vinyl polystyryl pyridine and bismaleimide (XU71775/H795) with the graphite tape was the optimum design giving the lowest heat release rate.

Kourtides, D. A.↗

NASA NTRS1988

Fracture toughness computational simulation of general delaminations in fiber composites

A procedure is described to computationally simulate composite laminate fracture toughness in terms of strain energy release rate. It is also used to evaluate the degradation in laminate structural integrity in terms of displacements, loss in stiffness, loss in vibration frequencies and loss in buckling resistance. Specific laminates are selected for detail studies in order to demonstrate the generality of the procedure. These laminates had center delaminations, off-center delaminations, and pocket delaminations (center and off-center) at the free-edge and center delaminations at the interior. The laminates had two different thicknesses and were made from three different materials. The results obtained are presented in graphical form to illustrate the effects of delamination on the laminate structural integrity and on the laminate strain energy release rate (composite fracture toughness).

Wilt, T. E.↗

NASA NTRS1988

Fracture toughness computational simulation of general delaminations in fiber composites

A procedure is described to computationally simulate composite laminate fracture toughness in terms of strain energy release rate (SERR). It is also used to evaluate the degradation in laminate structural integrity in terms of displacements, loss in stiffness, loss in vibration frequencies and loss in buckling resistance. Specific laminates are selected for detail studies in order to demonstrate the generality of the procedure. These laminates had center delaminations, off-center delaminations, and pocket delaminations (center and off-center) at the free-edge and center delaminations at the interior. The laminates had two different thicknesses and were made from three different materials. The results obtained are presented in graphical form to illustrate the effects of delamination on the laminate structural integrity and on the laminate strain energy release rate (composite fracture toughness).

Murthy, P. L. N.↗

NASA NTRS1999

Fracture Mechanics of Thin, Cracked Plates Under Tension, Bending and Out-of-Plane Shear Loading

Cracks in the skin of aircraft fuselages or other shell structures can be subjected to very complex stress states, resulting in mixed-mode fracture conditions. For example, a crack running along a stringer in a pressurized fuselage will be subject to the usual in-plane tension stresses (Mode-I) along with out-of-plane tearing stresses (Mode-III like). Crack growth and initiation in this case is correlated not only with the tensile or Mode-I stress intensity factor, K(sub I), but depends on a combination of parameters and on the history of crack growth. The stresses at the tip of a crack in a plate or shell are typically described in terms of either the small deflection Kirchhoff plate theory. However, real applications involve large deflections. We show, using the von-Karman theory, that the crack tip stress field derived on the basis of the small deflection theory is still valid for large deflections. We then give examples demonstrating the exact calculation of energy release rates and stress intensity factors for cracked plates loaded to large deflections. The crack tip fields calculated using the plate theories are an approximation to the actual three dimensional fields. Using three dimensional finite element analyses we have explored the relationship between the three dimensional elasticity theory and two dimensional plate theory results. The results show that for out-of-plane shear loading the three dimensional and Kirchhoff theory results coincide at distance greater than h/2 from the crack tip, where h/2 is the plate thickness. Inside this region, the distribution of stresses through the thickness can be very different from the plate theory predictions. We have also explored how the energy release rate varies as a function of crack length to plate thickness using the different theories. This is important in the implementation of fracture prediction methods using finite element analysis. Our experiments show that under certain conditions, during fatigue crack growth, the presence of out-of-plane shear loads induces a great deal of contact and friction on the crack surfaces, dramatically reducing crack growth rate. A series of experiments and a proposed computational approach for accounting for the friction is discussed.

Zehnder, Alan T.↗

NASA NTRS1999

A Shell/3D Modeling Technique for Delaminations in Composite Laminates

A shell/3D modeling technique was developed for which a local solid finite element model is used only in the immediate vicinity of the delamination front. The goal was to combine the accuracy of the full three-dimensional solution with the computational efficiency of a plate or shell finite element model. Multi-point constraints provide a kinematically compatible interface between the local 3D model and the global structural model which has been meshed with plate or shell finite elements. For simple double cantilever beam (DCB), end notched flexure (ENF), and single leg bending (SLB) specimens, mixed mode energy release rate distributions were computed across the width from nonlinear finite element analyses using the virtual crack closure technique. The analyses served to test the accuracy of the shell/3D technique for the pure mode I case (DCB), mode II case (ENF) and a mixed mode I/II case (SLB). Specimens with a unidirectional layup where the delamination is located between two 0 plies, as well as a multidirectional layup where the delamination is located between two non-zero degree plies, were simulated. For a local 3D model extending to a minimum of about three specimen thicknesses in front of and behind the delamination front, the results were in good agreement with mixed mode strain energy release rates obtained from computations where the entire specimen had been modeled with solid elements. For large built-up composite structures modeled with plate elements, the shell/3D modeling technique offers a great potential, since only a relatively small section in the vicinity of the delamination front needs to be modeled with solid elements.

Krueger, Ronald↗

NASA NTRS2017

Constitutive Modeling of the Facesheet to Core Interface in Honeycomb Sandwich Panels Subject to Mode I Delamination

A new cohesive zone traction-separation law, which includes the effects of fiber bridging, has been developed, implemented with a finite element (FE) model, and applied to simulate the delamination between the facesheet and core of a composite honeycomb sandwich panel. The proposed traction-separation law includes a standard initial cohesive component, which accounts for the initial interfacial stiffness and energy release rate, along with a new component to account for the fiber bridging contribution to the delamination process. Single cantilever beam tests on aluminum honeycomb sandwich panels with carbon fiber reinforced polymer facesheets were used to characterize and evaluate the new formulation and its finite element implementation. These tests, designed to evaluate the mode I toughness of the facesheet to core interface, exhibited significant fiber bridging and large crack process zones, giving rise to a concave downward concave upward pre-peak shape in the load-displacement curve. Unlike standard cohesive formulations, the proposed formulation captures this observed shape, and its results have been shown to be in excellent quantitative agreement with experimental load-displacement and apparent critical energy release rate results, representative of a payload fairing structure, as well as local strain fields measured with digital image correlation.

composites↗

NASA NTRS2001

Crack Turning Mechanics of Composite Wing Skin Panels

The safety of future composite wing skin integral stiffener panels requires a full understanding of failure mechanisms of these damage tolerance critical structures under both in-plane and bending loads. Of primary interest is to derive mathematical models using fracture mechanics in anisotropic cracked plate structures, to assess the crack turning mechanisms, and thereby to enhance the residual strength in the integral stiffener composite structures. The use of fracture mechanics to assess the failure behavior in a cracked structure requires the identification of critical fracture parameters which govern the severity of stress and deformation field ahead of the flaw, and which can be evaluated using information obtained from the flaw tip. In the three-year grant, the crack-tip fields under plane deformation, crack-tip fields for anisotropic plates and anisotropic shells have been obtained. In addition, methods for determining the stress intensity factors, energy release rate, and the T-stresses have been proposed and verified. The research accomplishments can be summarized as follows: (1) Under plane deformation in anisotropic solids, the asymptotic crack-tip fields have been obtained using Stroh formalism; (2) The T-stress and the coefficient of the second term for sigma(sub y), g(sub 32), have been obtained using path-independent integral, the J-integral and Betti's reciprocal theorem together with auxiliary fields; (3) With experimental data performed by NASA, analyses indicated that the mode-I critical stress intensity factor K(sub Q) provides a satisfactory characterization of fracture initiation for a given laminate thickness, provided the failure is fiber-dominated and crack extends in a self-similar manner; (4) The high constraint specimens, especially for CT specimens, due to large T-stress and large magnitude of negative g(sub 32) term may be expected to inhibit the crack extension in the same plane and promote crack turning; (5) Crack turning out of crack plane in generally anisotropic solids under plane deformation has been studied; (6) The role of T-stress and the higher-order term of sigma(sub y) on the crack turning and stability of the kinked crack has been quantified; (7) Asymptotic crack-tip fields including the effect of transverse shear deformation (Reissner plate theory) in an anisotropic plate under bending, twisting moments, and transverse shear loads has been presented; (8) The expression of the path-independent J-integral in terms of the generalized stress and strain has been derived; (9) Asymptotic crack-tip fields including the effect of transverse shear deformation (Reissner shallow shell theory) in a general anisotropic shell has been developed; (10) The Stroh formalism was used to characterize the crack tip fields in shells up to the second term and the energy release rate was expressed in a very compact form.

Yuan, F. G.↗

NASA NTRS1994

Separation of crack extension modes in composite delamination problems

This work concerns fracture mechanics modeling of composite delamination problems. In order to predict delamination resistance, an applied stress intensity factor, K, or energy release rate, G, must be compared to a mode-dependent critical value of K or G from experiment. In the interfacial fracture analysis of most applications and some tests, the mode of crack extension is not uniquely defined. It is instead a function of distance from the crack tip due to the oscillating singularity existing at the tip. In this work, a consistent method is presented of extracting crack extension modes in such cases. In particular, use of the virtual crack closure technique (VCCT) to extract modes of crack extension is studied for cases of a crack along the interface between two in-plane orthotropic materials. Modes of crack extension extracted from oscillatory analyses using VCCT are a function of the virtual crack extension length, delta. Most existing efforts to obtain delta-independent modes of crack extension involve changing the analysis in order to eliminate its oscillatory nature. One such method involves changing one or more properties of the layers to make the oscillatory exponent parameter, epsilon, equal zero. Standardized application of this method would require consistent criteria for identifying which properties can be altered without changing the physical aspects of the problem. Another method involves inserting a thin homogeneous layer (typically referred to as a resin interlayer) along the interface and placing the crack within it. The drawbacks of this method are that it requires increased modeling effort and introduces the thickness of the interlayer as an additional length parameter. The approach presented here does not attempt to alter the interfacial fracture analysis to eliminate its oscillatory behavior. Instead, the argument is made that the oscillatory behavior is non-physical and that if its effects were separated from VCCT quantities, then consistent, delta-independent modes of crack extension could be defined. Knowledge of the near-tip fields in a planar orthotropic material interfacial fracture analysis is used to determine the explicit delta dependence of VCCT parameters. Once this delta dependence is determined, energy release rates are defined with this delta dependence factored out. This modified VCCT method is applied to results from two finite element test cases. It is shown that, as predicted, delta-independent modes of crack extension result. The modified VCCT approach shows potential as a consistent method of extracting crack extension modes. It uses the same information from a finite element analysis (i.e., nodal forces and displacements) as the traditional VCCT method does. The A-independent modes extracted using the modified VCCT approach can also be used as guides to test the convergence of finite element solutions.

Beuth, Jack L.↗

NASA NTRS1994

Rate constants for the reactions of OH with CH3Cl, CH2Cl2, CHCl3, and CH3Br

Rate constants for the reactions of OH with CH3Cl, CH2Cl2, CHCl3, and CH3Br have been measured by a relative rate technique in which the reaction rate of each compound was compared to that of HFC-152a (CH3CHF2) and (for CH2Cl2) HFC-161 (CH3CH2F). Using absolute rate constants for HFC-152a and HFC-161, which we have determined relative to those for CH4, CH3CCl3, and C2H6, temperature dependent rate constants of both compounds were derived. The derived rate constant for CH3Br is in good agreement with recent absolute measurements. However, for the chloromethanes all the rate constants are lower at atmospheric temperatures than previously reported, especially for CH2Cl2 where the present rate constant is about a factor of 1.6 below the JPL 92-20 value. The new rate constant appears to resolve a discrepancy between the observed atmospheric concentrations and those calculated from the previous rate constant and estimated release rates.

Hsu, K.-J.↗

NASA NTRS1985

Seafloor hydrothermal activity and spreading rates - The Eocene carbon dioxide greenhouse revisited

A suggestion has been made that enhanced rates of hydrothermal activity during the Eocene could have caused a global warming by adding calcium to the ocean and pumping CO2 into the atmosphere (Owen and Rea, 1984). This phenomenon was purported to be consistent with the predictions of the CO2 geochemical cycle model of Berner, Lasaga and Garrels (1983) (henceforth BLAG). In fact, however, the BLAG model predicts only a weak connection between hydrothermal activity and atmospheric CO2 levels. By contrast, it predicts a strong correlation between seafloor spreading rates and pCO2, since the release rate of CO2 from carbonate metamorphism is assumed to be proportional to the mean spreading rate. The Eocene warming can be conveniently explained if the BLAG model is extended by assuming that the rate of carbonate metamorphism is also proportional to the total length of the midocean ridges from which the spreading originates.

Kasting, J. F.↗

NASA NTRS1985

Seafloor hydrothermal activity and spreading rates: the Eocene carbon dioxide greenhouse revisted

A suggestion has been made that enhanced rates of hydrothermal activity during the Eocene could have caused a global warming by adding calcium to the ocean and pumping CO2 into the atmosphere (Owen and Rea, 1984). This phenomenon was purported to be consistent with the predictions of the CO2 geochemical cycle model of Berner, Lasaga and Garrels (1983) (henceforth BLAG). In fact, however, the BLAG model predicts only a weak connection between hydrothermal activity and atmospheric CO2 levels. By contrast, it predicts a strong correlation between seafloor spreading rates and pCO2, since the release rate of CO2 from carbonate metamorphism is assumed to be proportional to the mean spreading rate. The Ecocene warming can be conveniently explained if the BLAG model is extended by assuming that the rate of carbonate metamorphism is also proportional to the total length of the midocean ridges from which the spreading originates.

Seawater/chemistry↗

NASA NTRS1995

Cationic influences upon synaptic transmission at the hair cell-afferent fiber synapse of the frog

The concentrations of inorganic cations (K+, Na+, and Ca2+) bathing the isolated frog labyrinth were varied in order to assess their role in influencing and mediating synaptic transmission at the hair cell-afferent fiber synapse. Experiments employed intracellular recordings of synaptic activity from VIIIth nerve afferents. Recordings were digitized continuously at 50 kHz, and excitatory postsynaptic potentials were detected and parameters quantified by computer algorithms. Particular attention was focused on cationic effects upon excitatory postsynaptic potential frequency of occurrence and excitatory postsynaptic potential amplitude, in order to discriminate between pre- and postsynaptic actions. Because the small size of afferents preclude long term stable recordings, alterations in cationic concentrations were applied transiently and their peak effects on synaptic activity were assessed. Increases in extracellular K+ concentration of a few millimolar produced a large increase in the frequency of occurrence of excitatory postsynaptic potentials with little change in amplitude, indicating that release of transmitter from the hair cell is tightly coupled to its membrane potential. Increasing extracellular Na+ concentration resulted in an increase in excitatory postsynaptic potential amplitude with no significant change in excitatory postsynaptic potential frequency of occurrence, suggesting that the transmitter-gated subsynaptic channel conducts Na+ ions. Decreases in extracellular Ca2+ concentration had little effect upon excitatory postsynaptic potential frequency, but increased excitatory postsynaptic potential frequency and amplitude. These findings suggest that at higher concentrations Ca2+ act presynaptically to prevent transmitter release and postsynaptically to prevent Na+ influx during the generation of the excitatory postsynaptic potential. The influences of these ions on synaptic activity at this synapse are remarkably similar to those reported at the vertebrate neuromuscular junction. The major differences between these two synapses are the neurotransmitters and the higher resting release rate and higher sensitivity of release to increased K+ concentrations of the hair cells over that of motor nerve terminals. These differences reflect the functional roles of the two synapses: the motor nerve terminal response in an all-or-nothing signal consequent from action potential invasion, while the hair cell releases transmitter in a graded fashion, proportionate to the extent of stereocilial deflection. Despite these differences between the two junctions, the similar actions of these elemental cations upon synaptic function at each implies that these ions may participate similarly in the operations of other synapses, independent of the neurotransmitter type.(ABSTRACT TRUNCATED AT 400 WORDS).

NASA Discipline Neuroscience↗

NASA NTRS2008

Measurement of Fire Radiative Energy from Space and Implications for Fire-Disaster Monitoring and Smoke Emissions Modeling

Measurement of fire radiative energy (FRE) release rate or power (FRP) from satellite provides a vital mechanism for distinguishing different strengths of fires. Analysis of 1-km resolution fire data, acquired globally by the MODerate-resolution Imaging Spectro-radiometer (MODIS) sensor aboard the Terra and Aqua satellites from 2000 to 2006, showed instantaneous FRP values ranging between 0.02 MW and 1866 MW, to which simple thresholds can be applied to categorize fires by strength, in a similar fashion as the strengths of earthquakes and hurricanes. Analysis of regional mean FRP per unit area of land (FRP flux) shows that at peak fire season in certain regions, fires can be responsible for up to 0.2 W/m2 at peak time of day. When considered as the active fire contribution to the direct surface radiative forcing (RF) in the different fire regions, this order of magnitude of FRF fluxes is non negligible. It has been determined experimentally that the amount of FRE released by a fire over the course of its duration is directly proportional to the amount of biomass consumed by it. Furthermore, at the satellite observation scale, the rate of release of FRE (i.e. FRP) is proportional to the rate of biomass consumption, and that of emission of smoke particulates and eventually also other smoke constituents. Therefore, current research efforts are geared toward deriving simple parameterizations that will facilitate direct input of FRP measurements in models, not only to improve the accuracy of burned-biomass and smoke emissions estimations, but also to reduce the hitherto practiced heavy reliance on multiple indirect parameters with indeterminate uncertainties.

Ichoku, Charles↗

NASA NTRS1973

Role of pressure transients in the detection and identification of lunar surface gas sources.

The dynamic behavior of neutral gases emitted from lunar surface sources is investigated. Pressure transients to be expected from several types of possible lunar surface sources are constructed. An approximate method is developed to estimate the source-sensor separation distance and the amount of effluent release. The case for which the source location and effluent molecular weight can be determined from ancillary data is discussed. It is shown that, if such data are available, pressure transients detected by either Apollo lunar surface experiment package ion spectrometers or cold cathode gages can be used to determine the release rate and the total amount of effluent release from the source.

Hall, F. G.↗

NASA NTRS1984

Cyclic debonding of adhesively bonded composites

To analyze the fatigue behavior of a simple composite-to-composite bonded joint, a combined experimental and analytical study of the cracked-lap-shear specimen subjected to constant-amplitude cyclic loading was undertaken. Two bonded systems were studied: T300/5208 graphite/epoxy adherends bonded with adhesives EC 3445 and with FM-300. For each bonded system, two specimen geometries were tested: (1) a strap adherend of 16 plies bonded to a lap adherend of 8 plies, and (2) a strap adherend of 8 plies bonded to a lap adherend of 16 plies. In all specimens tested, the fatigue failure was in the form of cyclic debonding with some 0 deg fiber pull-off from the strap adherend. The debond always grew in the region of adhesive that had the highest mode I (peel) loading and that region was close to the adhesive-strap interface. Furthermore, the measured cyclic debond growth rates correlated well with total strain energy release rates G(T) as well as with its components G(I) (peel) and G(II) (shear) for the mixed-mode loading in the present study.

Mall, S.↗

NASA NTRS2001

Studies of Ice Nucleating Aerosol Particles in Arctic Cloud Systems

The focus of this research is to improve the understanding of ice nucleating aerosol particles (IN) and the role they play in ice formation in Arctic clouds. IN are important for global climate issues in a variety of ways. The primary effect is their role in determining the phase (liquid or solid) of cloud particles. The microscale impact is on cloud particle size, growth rate, shape, fall speed, concentration, radiative properties, and scavenging of gases and aerosols. On a larger scale, ice formation affects the development of precipitation (rate, amount, type, and distribution), latent heat release (rate and altitude), ambient humidity, the persistence of clouds, and cloud albedo. The overall goals of our FIRE 3 research are to characterize the concentrations and variability of Arctic IN during the winter-spring transition, to compare IN measurements with ice concentrations in Arctic clouds, and to examine selected IN samples for particle morphology and chemical there are distinguishable chemical signatures. The results can be combined with other measurements of aerosols, gaseous species, and cloud characteristics in order to understand the processes that determine the phase and concentration of cloud particles.

Rogers, David C.↗