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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 199 records · Page 11
All sourcesNASA NTRSDOE OSTI
NASA NTRS2022

Constraints on the Optical Depth to Reionization from Balloon-borne Cosmic Microwave Background Measurements

We assess the uncertainty with which a balloon-borne experiment, nominally called Tau Surveyor (τS), can measure the optical depth to reionization σ(τ) with given realistic constraints of instrument noise and foreground emissions. Using a τS fiducial design with six frequency bands between 150 and 380 GHz, with white and uniform map noise of 7 μK arcmin, achievable with a single midlatitude flight, and including Planck's 30 and 44 GHz data, we assess the error σ(τ) obtained with three foreground models and as a function of sky fraction f sky between 40% and 54%. We carry out the analysis using both parametric and blind foreground separation techniques. We compare the σ(τ) values to those obtained with low-frequency and high-frequency versions of the experiment called τS-lf and τS-hf, which have only four and up to eight frequency bands with narrower and wider frequency coverage, respectively. We find that with τS, the lowest constraint is σ(τ) = 0.0034, obtained for one of the foreground models with f sky = 54%. σ(τ) is larger, in some cases by more than a factor of 2, for smaller sky fractions, with τS-lf, or as a function of foreground model. The τS-hf configuration does not lead to significantly tighter constraints. The exclusion of the 30 and 44 GHz data, which give information about synchrotron emission, leads to significant τ misestimates. Decreasing noise by an ambitious factor of 10, while keeping f sky = 40%, gives σ(τ) = 0.0031. The combination of σ(τ) = 0.0034, baryon acoustic oscillation data from DESI, and future cosmic microwave background B-mode lensing data from the CMB-S3/CMB-S4 experiments could give σ(∑m v ) = 17 meV.

cosmic microwave background radiation↗
DOE OSTI2022

Surrogate isotope-containing materials for emergency response training and Methods of formation and dispersal

Surrogate materials are in the form of solid particles that include surrogate isotopes, namely, short-lived isotopes selected and formed to serve as surrogates for the radioactive materials of a nuclear fallout without including isotopes that are, or that decay to, biologically or environmentally deleterious and persistent isotopes. The surrogate material may be formed using high-purity reactant material and irradiation and separation techniques that enable tailoring of the isotopes and ratios thereof included in the surrogate material, and the surrogate material may be dispersed, e.g., in a training environment, in solid form.

Carney, Kevin P.↗
DOE OSTI2023

Improving Volatile Fatty Acid Productivity of Anaerobic Digestion

Typical anaerobic digestion (AD) focusses on complete conversion of waste to biogas (primarily carbon dioxide and methane). However, the intermediate metabolites of the AD process, which includes short- and long-chain volatile fatty acids (VFAs), that could serve as the precursors for useful industrial applications are typically ignored. The goal of this project is to eliminate production of biogas while enhancing the production of the intermediate VFAs. Using a mixed microbial consortium (from rumen sources and waste-water sludge), we have determined the optimal carbon loading (chemical oxygen demand, "COD") and optimal pH, that results in high VFA concentrations from food waste. The best VFA yields were obtained using 15 g COD/L and a pH of 9.0 for this substrate. pH 9 produced over 200% higher VFA titers than the controlled conditions (i.e., ph 7.0) after 35 d of digestion, in comparison to pH 5 that showed - 88% higher titers than the control digestion. As expected, the cumulative biogas production was highest in the pH 7.0 condition, in comparison to pH 5.0 or pH 9.0. We further observed that removal of VFAs using solid-liquid separation technique reduce the inhibitory effects of VFAs, thereby leading to overall improvement in conversion efficiency. 16s rRNA analysis is being carried out to explain and identify the biocatalysts that enable VFA production in these AD cultures. Additional efforts to improve VFA yields via increasing the total solid content, temperature optimizations, VFA removal via electrodialysis, and improving hydrolysis via microaeration will be presented.

anaerobic digestion↗
DOE OSTI2023

Development of a Multi Sensor Data Science System for Monitoring a Solvent Extraction Process

Idaho National Laboratory is designing and constructing a solvent extraction test bed, Beartooth, as part of a nuclear fuel cycle stewardship initiative. The test bed will provide facilities and equipment for testing novel extraction processes and give early career scientists opportunities to gain skills in performing separations chemistry. The test bed is being uniquely designed to enable machine learning capabilities for the characterization of chemical process operations. One of the intentions of incorporating machine learning methods is to provide process operators with enhanced situational awareness for the optimization of separations techniques and possible detection of a diversion event. As a result, the objective of this Laboratory Directed Research and Development project is to develop a multi-sensor data collections system and implement machine learning techniques on signals from an existing centrifugal contactor cascade to identify equipment usage and process events. This presentation will provide an overview of sensors used and experiments conducted to date.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2025

LDRD Concluding Poster for Project 23A1070-162FP

This is the poster for the concluding LDRD project, Development of Two-Phase Separation Techniques for Advanced Fuel Cycle Studies, Project number: 23A1070-162FP.

37 - INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL C↗
DOE OSTI2022

Applications of a dual-column technique in actinide separations

Selective separation of an individual actinide of interest from other actinides and accompanying lanthanides is a challenging task in radiochemistry and radioanalytical chemistry. This paper illustrates a dual column technique (i.e., stacked columns of two appropriate resins) to separate an individual actinide of interest, where the selection of two resins and a common effluent running through the stacked columns are key parameters in design of an appropriate dual column. This paper describes the dual column design and practice with two examples, one for a heavy actinide 249Bk and the other for a light actinide 230U. In the former case, stacked columns of anion exchange (AX) resin and LN resin replaced the traditional CX-AHIB method used at Oak Ridge National Laboratory for 60 years. In the latter case, an elution process with an AX column followed with a stacked column of AX resin and a DGA resin was applied, instead of traditional methods, e.g., PUREX or U-TEVA methods. Application results of the dual column method to the two example actinides are displayed, while the considerations in method design and the required conditions are discussed.

Du, Miting↗
NASA NTRS1985

Development of a boundary-layer-type solver based on simultaneous iteration technique for axisymmetric separated flows

A boundary-layer-type solver is developed for the numerical solution of axisymmetric separated flows. A new fully implicit coupling scheme for the viscous and inviscid regions is demonstrated. This fully implicit coupling technique is similar to the work of Carter, Veldman, and an extension of an earlier work of Halim and Hafez. A comparison is made for the convergence rate using this new fully implicit coupling technique and the semiimplicit coupling of Halim and Hafez. Numerical results using the fully implicit coupling are obtained for laminar incompressible separated flows, including a boattail and a series of trough geometries. Also, the near-wake flow problem is considered using the present formulation. A clear conclusion of this investigation is that the present scheme using the fully implicit coupling method converges at a faster rate than the semiimplicit coupling and the partially parabolized Navier-Stokes (PPNS) procedures.

Halim, A. A. M.↗
NASA NTRS1996

A Structured Grid Based Solution-Adaptive Technique for Complex Separated Flows

The objective of this work was to enhance the predictive capability of widely used computational fluid dynamic (CFD) codes through the use of solution adaptive gridding. Most problems of engineering interest involve multi-block grids and widely disparate length scales. Hence, it is desirable that the adaptive grid feature detection algorithm be developed to recognize flow structures of different type as well as differing intensity, and adequately address scaling and normalization across blocks. In order to study the accuracy and efficiency improvements due to the grid adaptation, it is necessary to quantify grid size and distribution requirements as well as computational times of non-adapted solutions. Flow fields about launch vehicles of practical interest often involve supersonic freestream conditions at angle of attack exhibiting large scale separate vortical flow, vortex-vortex and vortex-surface interactions, separated shear layers and multiple shocks of different intensity. In this work, a weight function and an associated mesh redistribution procedure is presented which detects and resolves these features without user intervention. Particular emphasis has been placed upon accurate resolution of expansion regions and boundary layers. Flow past a wedge at Mach=2.0 is used to illustrate the enhanced detection capabilities of this newly developed weight function.

Thornburg, Hugh↗
NASA NTRS1983

Separation of cells from the rat anterior pituitary gland

Various techniques for separating the hormone-producing cell types from the rat anterior pituitary gland are examined. The purity, viability, and responsiveness of the separated cells depend on the physiological state of the donor, the tissue dissociation procedures, the staining technique used for identification of cell type, and the cell separation technique. The chamber-gradient setup and operation, the characteristics of the gradient materials, and the separated cell analysis of velocity sedimentation techniques (in particular Staput and Celsep) are described. Consideration is given to the various types of materials used in density gradient centrifugation and the operation of a gradient generating device. The use of electrophoresis to separate rat pituitary cells is discussed.

Hymer, Wesley C.↗
NASA NTRS1980

Separating liquid and gaseous solutions

Clusius-Dickel separation (CDS) technique, currently used in laboratoryscale separation of certain isotopes, may find more effective applications in low-gravity, space environments. Many advantages in power supply, mechanical stresses, and spatial arragement can be realized in space, making technique suitable for biological and polymer separations.

Benefield, J. W.↗
NASA NTRS1983

An allpass filter design for luminance and chrominance separation of NTSC signals

Abstract- Digital techniques for separation of luminance and chrominance components from composite NTSC broadcast television signals are explored. First, comb filters are introduced. Secondly, filters based on linear regression are developed. Finally, a third filtering form, the allpass filter is considered. Techniques are compared based on mean squared error criteria and subjective testing. It is demonstrated that the allpass filtering technique is superior to both the comb filtering as well as the regression filtering.

Border, D. A.↗
NASA NTRS1974

New diagnostic technique for the study of turbulent boundary-layer separation

Description of a diagnostic technique for determining the unsteady character of turbulent boundary-layer separation. The technique uses thin platinum films mounted flush with the model surface. Voltages from these films provide measurements related to the flow character above the film. For illustration, results obtained by this technique are presented for the interaction of a hypersonic shock wave and a turbulent boundary layer, with and without separation.

Horstman, C. C.↗
NASA NTRS1985

Control plate for shock-boundary layer interaction

Paper describes tests and computations for a relatively unique technique to greatly reduce/eliminate the separation region for shock-boundary layer interactions. A number of studies have shown that the usual effects of such interactions include increased local heating and wall pressures, thickening of the boundary layer and a decrease in the momentum of the flow and, for stronger waves, flow separation. This flow situation is particularly prevalent in supersonic and hypersonic inlets where severe performance degradation can occur due to flow separation. High performance engine design generally requires a uniform entering flow field with little stagnation pressure loss. Previous approaches to the problem involved primarily active devices (e.g., suction or blowing); the present paper considers a passive device. The boundary layer separation control technique considered herein involves the placement of an embedded plate in the outer portion of the boundary layer and parallel to the wall. This control plate is situated such that the incident shock impinges upon and reflects from its surface, thus greatly lessening the pressure gradient in the low momentum near wall region.

Goodman, W. L.↗
NASA NTRS1988

Visualization techniques for studying high angle of attack separated vortical flows

Flow visualization techniques can provide information on high angle of attack separated flows around slender aircraft configurations that may be unobtainable otherwise. At large angles of attack the flow field is dominated by vortical structures originating on the forebody wing extension, wing and forward control surfaces. Several techniques that are suitable for tracking vortices in subsonic wind tunnels are introduced. A discussion of visualization photographs and quantitative data obtained from visualization studies on vortex trajectory and breakdown position on both static and dynamic wind tunnel models is presented.

Nelson, Robert C.↗
DOE OSTI2025

Using Separation-Enhanced Isotope Ratio Mass Spectrometry to Enable Increased Renewable Carbon Content in Transportation Fuels (CRADA 525)

Stable isotope ratio measurements of carbon atoms using isotope ratio mass spectrometry (IRMS) can be an effective tool for quantifying biogenic carbon in co-processed fuels, with results approaching the precision and accuracy of accelerator mass spectrometry (AMS). The lower cost of an IRMS may enable deployment to refineries, improving access and analysis turnaround times (≤2 hours), and, by extension, provide data that can allow process optimization to maximize renewable carbon in desired refinery products. This project explored the integration of chemical separation with IRMS analyses to enable highly detailed tracking of biogenic carbon into fuel product streams separated by boiling point range, chemical class, or specific compound. Forty-nine fuels and fuel components of fossil and biogenic origin, spanning gasoline and diesel boiling point ranges, were received from three refiners and were analyzed for their δ 13 C values via IRMS. Results spanned a 13 C range from ca. 10‰ to 44‰ and reflect materials derived from sustainable sources (e.g., C4 or C3 plants, animal-based pathways, syngas) or from fossil-derived fuels. Common ranges are approximately 18‰ to 9‰ and approximately 30‰ to 20‰ for C4 and C3 plants, respectively, and approximately 34‰ to 24‰ and approximately 70‰ to 33‰ for petroleum-derived fuels and methane, respectively. Fuel-like standards were developed and tested using direct-injection elemental analyzer (EA) IRMS for liquid fuels. This method was compared with the published methods, yielding statistically similar results. Four blend curve sets were produced ranging from 0% to 100% of a fuel containing biogenic carbon, focusing on 0% to 10% biogenic carbon. Linear fits were the most applicable for two of the four blend curve sets; however, two sets were found to exhibit slightly quadratic behavior, which was more pronounced in low biogenic blend samples, necessitating second-order fits. The origin of the slight quadratic behavior remains unclear; however, the discussion points to possible interpretations. CanmetENERGY thoroughly characterized a majority of the samples using one- and two-dimensional gas chromatography (GC and GC×GC, respectively) and other analyses. Selected samples were subjected to solid phase extraction (SPE) for saturate, olefin, aromatic, and polar (SOAP) analysis, and the resulting solvent-diluted fractions containing saturates and aromatics were returned to Pacific Northwest National Laboratory (PNNL), where the solvent was removed via evaporation or physical separation using GC techniques. Characterization and separations provided an understanding of saturate and aromatic content, as well as boiling point ranges for each sample and sample fraction. Samples resulting from SPE were examined using EA-IRMS and gas chromatography combustion IRMS (GC-C-IRMS) analyses. Both approaches suggest that the range in values between end-members can be increased by selecting the paraffinic or aromatic fraction of the end-member or by selecting among individual compounds resulting from GC separation of the paraffinic fractions. Considerable work remains to put these approaches into practice and statistically validate the benefit for using a fraction or individual compound over bulk analysis of a sample. However, initial results suggest that separations provide advantages for samples having blend ratios of less than 10% biogenic blendstocks. 13 C results showed statistically similar biofuel blend results to those obtained at PNNL, although additional work is needed to obtain better reproducibility. Select samples were sent to Los Alamos National Laboratory (LANL) for IRMS measurements and Beta Analytics for AMS measurements. This work suggests that IRMS and AMS yield closely comparable results and in some circumstances, IRMS could serve as a surrogate for AMS. While additional work is needed to better resolve statistical advantages for separations and better show the comparable nature of IRMS and AMS in both the biogenic carbon analysis of bulk chemical classes, initial results from this study suggest that these should be pursued in order to proliferate this approach for quantifying biogenic carbon in transportation fuels to the refinery level, thereby potentially enabling process optimization in co-processing scenarios.

09 BIOMASS FUELS↗
NASA NTRS1973

Development of a household waste treatment subsystem, volume 1

The domestic waste treatment subsystem was developed to process the daily liquid and non-metallic solid wastes provided by a family of four people. The subsystem was designed to be connected to the sewer line of a household which contained water conservation features. The system consisted of an evaporation technique to separate liquids from solids, an incineration technique for solids reduction, and a catalytic oxidizer for eliminating noxious gases from evaporation and incineration processes. All wastes were passed through a grinder which masticated the solids and deposited them in a settling tank. The liquids were transferred through a cleanable filter into a holding tank. From here the liquids were sprayed into an evaporator and a spray chamber where evaporation occurred. The resulting vapors were processed by catalytic oxidation. Water and latent energy were recovered in a combination evaporator/condenser heat exchanger. The solids were conveyed into an incinerator and reduced to ash while the incineration gases were passed through the catalytic oxidizer along with the processed water vapor.

Gresko, T. M.↗