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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 199 records · Page 11
All sourcesNASA NTRSDOE OSTI
NASA NTRS2011

In Situ Aerosol Detector

An affordable technology designed to facilitate extensive global atmospheric aerosol measurements has been developed. This lightweight instrument is compatible with newly developed platforms such as tethered balloons, blimps, kites, and even disposable instruments such as dropsondes. This technology is based on detection of light scattered by aerosol particles where an optical layout is used to enhance the performance of the laboratory prototype instrument, which allows detection of smaller aerosol particles and improves the accuracy of aerosol particle size measurement. It has been determined that using focused illumination geometry without any apertures is advantageous over using the originally proposed collimated beam/slit geometry (that is supposed to produce uniform illumination over the beam cross-section). The illumination source is used more efficiently, which allows detection of smaller aerosol particles. Second, the obtained integral scattered light intensity measured for the particle can be corrected for the beam intensity profile inhomogeneity based on the measured beam intensity profile and measured particle location. The particle location (coordinates) in the illuminated sample volume is determined based on the information contained in the image frame. The procedure considerably improves the accuracy of determination of the aerosol particle size.

Vakhtin, Andrei↗
NASA NTRS1992

Deriving the velocity distribution of meteoroids from the measured meteoroid impact directionality on the various LDEF surfaces

Because of spacecraft orbital motion about the Earth, a much higher flux of meteoroids is expected to strike spacecraft surfaces that face in the direction of spacecraft motion (apex direction) than would strike apex facing or trailing edge surfaces. Impact velocities are also higher on apex facing surfaces compared to antapex facing surfaces which futher increases the apex/antapex ratio of spatial density of impact craters of a given size. Measurements of the areal densities of impact craters on the different LDEF surfaces should give important clues about the velocity distribution, and therefore the origins, of meteoroids. Preliminary results appear to support the meteoroid velocity distributions derived by Erickson and by Kessler, which would lead to a mean impact velocity on the LDEF spacecraft of about 19 km/s.

Zook, Herbert A.↗
NASA NTRS2018

A Rain Taxonomy for Degraded Visual Environment Mitigation

This Technical Memorandum (TM) provides a description of a rainfall taxonomy that defines the detailed characteristics of naturally occurring rainfall. The taxonomy is based on raindrop size measurements collected around the globe and encompasses several different climate types. Included in this TM is a description of these rainfall observations, an explanation of methods used to process those data, and resultant metrics comprising the rain taxonomy database. Each of the categories in the rain taxonomy are characterized by a unique set of raindrop sizes that can be used in simulations of electromagnetic wave propagation through a rain medium.

meteorology↗
NASA NTRS1988

Small-droplet spray measurements with a scattered-light scanner

Interacting two-phase flow through pneumatic two-fluid nozzles was investigated to determine the effect of nitrogen gas mass-velocity on the Sauter mean diameter of water sprays produced by the breakup of small diameter liquid-jets in high velocity gas streams. Tests were conducted primarily in the aerodynamic-stripping regime of liquid-jet atomization. It was found that the loss of droplets due to vaporization and dispersion had a marked effect on drop size measurements. A scattered-light scanner, developed at NASA Lewis Research Center was used to measure Sauter mean diameters, D sub 32, as small as 5 microns, which were correlated with nitrogen gas mass-velocity to give the following expression: D(sup -1)(sub 32) = 11.7(rho (sub n) V(sub n))(sup 1.33) where D sub 32 and p(sub n)V(sub n) are given in centimeters and g/sq cm-sec, respectively. The exponent 1.33 is the same as that predicted by atomizing theory for liquid-jet breakup in high velocity gas streams.

Ingebo, Robert D.↗
NASA NTRS1978

Anthropometry

Data on body-size measurement are presented to aid in spacecraft design. Tabulated dimensional anthropometric data on 59 variables for 12 selected populations are given. The variables chosen were those judged most relevant to the manned space program. A glossary of anatomical and anthropometric terms is included. Selected body dimensions of males and females from the potential astronaut population projected to the 1980-1990 time frame are given. Illustrations of drawing-board manikins based on those anticipated body sizes are included.

Mcconville, J. T.↗
DOE OSTI2020

Controlled plasma–droplet interactions: a quantitative study of OH transfer in plasma–liquid interaction

Plasmas in contact with liquids are a rich source of OH radicals and have been extensively studied in the last decade to leverage the ability to generate chemically reactive species in gas phase plasmas to decompose organics. Multiphase transfer of OH radicals is highly transport limited and to overcome transport limits, the plasma activation of aerosols, small liquid droplets, interspersed in the plasma has been proposed. In this work, we report a combined experimental and modeling study of a controlled plasma–droplet interaction experiment using a diffuse RF glow discharge in He + 0.2% H 2 O with detailed plasma diagnostics, ex situ analysis of the plasma-induced chemistry in the droplet containing formate, droplet trajectory and size measurements. This enables a quantitative study of the reactivity transfer of OH from the gas phase plasma to the liquid phase and how its diffusion limitations impact formate decomposition in the water droplet. For a droplet with a diameter of 36 μm, we observed 50% reduction in formate concentration in the droplets after plasma treatment for droplet residence times in the plasma of ~10 ms. These short droplet residence times in the plasma allow in some cases for droplet size reductions of ~5% in spite gas temperatures of 360 K. A one-dimensional reaction–diffusion model was used to calculate the OH transport and formate oxidation inside the droplet and was able to predict the conversion of formate by plasma in a droplet without any fitting parameters. The model further shows that formate conversion is dominated by near-interfacial reactions with OH radicals and is limited by diffusion of formate in the droplet. Here, the results show that a controlled plasma–micro-droplet reactor as reported in this study might be an excellent tool for detailed quantitative plasma–liquid interaction studies.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
NASA NTRS2017

Surveys of Returned ISS Hardware for MMMOD Impacts

Since February 2001, the Hypervelocity Impact Technology (HVIT) group at the Johnson Space Center (JSC) in Houston has performed 35 post-flight inspections on space exposed hardware returned from the International Space Station (ISS). Data on 1,188 observations of micrometeoroid and orbital debris (MMOD) damage have been collected from these inspections. Survey documentation typically includes impact feature location and size measurements as well as microscopic photography (25-200x). Sampling of impacts sites for projectile residue was performed for the largest features. Results of energy dispersive X-ray spectroscopic analysis to discern impactor source are included in the database when available. This paper will focus on two inspections, the Pressurized Mating Adapter 2 (PMA-2) cover returned in 2015 after 1.6 years exposure with 26 observed impact features, and two Airlock shield panels returned in 2010 after 8.75 years exposure with 58 MMOD impacts. Feature sizes from the observed data are compared to predictions using the Bumper 3 risk assessment code.

Hyde, J. L.↗
DOE OSTI2022

Onion-Like nanoparticles of the metal–organic framework UiO-66 synthesized by sequential spike crystal growth

Reproducible size and morphology of metal–organic framework (MOF) particles are essential for tuning these materials for applications like heterogeneous catalysis. Particle size measurements from electron micrographs provide information about the impact of changing synthetic parameters on MOF growth, but reported data are usually limited to averages and statistical distributions. Further elucidating synthetic control parameters could facilitate studies of facet-dependent and non-classical growth mechanisms. Here, in this work, phase-pure nanoparticles of the MOF UiO-66 were synthesized using alternating spikes of zirconium and hafnium-based nodes, forming an onion-like structure with alternating layers of Zr-UiO-66 and Hf-UiO-66. In conventional, bright-field transmission electron micrographs, Hf-UiO-66 and Zr-UiO-66 layers appeared darker and lighter, respectively. Alternating layers of Hf-UiO-66 and Zr-UiO-66 were also apparent in elemental maps obtained using scanning transmission electron microscopy with energy-dispersive X-ray spectroscopy. Average particle sizes increased monotonically with each spike, and no Zr-only or Hf-only particles were observed after the first spike, indicating that new material was consistently incorporated onto existing seeds. Surface area of the onion-like particles and their uptake of Ni 2+ from solution were both between the values measured for Zr-UiO-66 and Hf-UiO-66. Results demonstrate the use of sequential spikes of nodes in monitoring crystal growth in MOFs.

36 MATERIALS SCIENCE↗
NASA NTRS2017

Surveys of ISS Returned Hardware for MMOD Impacts

Since February 2001, the Hypervelocity Impact Technology (HVIT) group at the Johnson Space Center in Houston has performed 26 post-flight inspections on space exposed hardware that have been returned from the International Space Station. Data on 1,024 observations of MMOD damage have been collected from these inspections. Survey documentation typically includes impact feature location and size measurements as well as microscopic photography (25-200x). Sampling of impacts sites for projectile residue was performed for the largest features. Results of Scanning Electron Microscopy (SEM) analysis to discern impactor source is included in the database. This paper will summarize the post-flight MMOD inspections, and focus on two inspections in particular: (1) Pressurized Mating Adapter-2 (PMA-2) cover returned in 2015 after 1.6 years exposure with 26 observed damages, and (2) Airlock shield panels returned in 2010 after 8.7 years exposure with 58 MMOD damages. Feature sizes from the observed data are compared to predictions using the Bumper risk assessment code.

Hyde, James↗
NASA NTRS1996

Physical and Optical/Radiative Characteristics of Aerosol and Cloud Particles in Tropical Cirrus: Importance in Radiation Balance

Whether cirrus clouds heat or cool the Earth-atmosphere system depends on the relative importance of the cloud shortwave albedo effect and the cloud thermal greenhouse effect. Both are determined by the distribution of ice condensate with cloud particle size. The microphysics instrument package flown aboard the NASA DC-8 in TOGA/COARE included an ice crystal replicator, a 2D Greyscale Cloud Particle Probe and a Forward Scattering Spectrometer Aerosol Probe. In combination, the electro-optical instruments permitted particle size measurements between 0.5 micrometer and 2.6 millimeter diameter. Ice crystal replicas were used to validate signals from the electrooptical instruments. Both optical and scanning electron microscopy were utilized to analyze aerosol and ice particle replicas between 0.1 micrometer and several 100 micrometer diameter. In first approximation, the combined aerosol-cloud particle spectrum in several clouds followed a power law N alpha D(sup -2.5). Thus, large cloud particles carried most of the condensate mass, while small cloud and aerosol particles determined the surface area. The mechanism of formation of small particles is growth of (hygroscopic, possibly ocean-derived) aerosol particles along the Kohler curves. The concentration of small particles is higher and less variable in space and time, and their tropospheric residence time is longer, than those of large cloud particles because of lower sedimentation velocities. Small particles shift effective cloud particle radii to sizes much smaller than the mean diameter of the cloud particles. This causes an increase in shortwave reflectivity and IR emissivity, and a decrease in transmissivity. Occasionally, the cloud reflectivity increased with altitude (decreasing temperature) stronger than did cloud emissivity, yielding enhanced radiative cooling at higher altitudes. Thus, cirrus produced by deep convection in the tropics may be critical in controlling processes whereby energy from warm tropical oceans is injected to different levels in the atmosphere to subsequently influence not only tropical but mid-latitude climate.

Pueschel, R. F.↗
NASA NTRS1995

Sizing of colloidal particle and protein molecules in a hanging fluid drop

We report non-invasive particle size measurements of polystyrene latex colloidal particles and bovine serum albumin (BSA) protein molecules suspended in tiny hanging fluid drops of 30 micro-Liter volume using a newly designed fiber optic probe. The probe is based upon the principles of the technique of dynamic light scattering (DLS). The motivation for this work comes from growing protein crystals in outer space. Protein crystals have been grown previously in hanging drops in microgravity experiments on-board the space shuttle orbiter. However, obtaining quantitative information on nucleation and growth of the protein crystals in real time has always been a desired goal, but hitherto not achieved. Several protein researchers have shown interest in using DLS to monitor crystal growth process in a droplet, but elaborate instrumentation and optical alignment problems have made in-situ applications difficult. We demonstrate that such an experiment is now possible. Our system offers fast (5 seconds) determination of particle size, utilize safe levels of very low laser power (less than or equal to 0.2 mW), a small scattering volume (approximately 2 x 10(exp -5) cu mm) and high spatial coherence (Beta) values. This is a major step forward when compared to currently available DLS systems.

Ansari, Rafat R.↗
DOE OSTI2022

The Wormholes Within: A Study of 1, 3, 5–Triamino–2, 4, 6–Trinitrobenzene Crystal Morphology by Micro and Nano–Scale X–Ray Computed Tomography and its Effects Upon the Shock Sensitivity of Detonation

We report that we understand heterogeneous-explosive detonation only to the extent that we can first measure the salient chemical and microstructural features. Barring an inordinate amount of trial and error, we can tailor the detonation properties of our HE formulations only to the extent that we understand (at least qualitatively) the same effects. As an insensitive high explosive, 1, 3, 5-triamino-2, 4, 6-trinitrobenzene (TATB) burns more heterogeneously than conventional high explosives, making its detonation properties sensitive to microstructure. The Benziger route can produce various grain morphologies depending on the amount of water used in the amination step. So-called dry-aminated (DA) TATB crystals are riddled with a void structure called wormholes, which are washed out ammonium chloride (NH4Cl) inclusions that form during synthesis. So-called wet-aminated (WA) TATB crystals do not contain NH 4 Cl inclusions but possess a very convoluted external structure. Using both micro and nano-scale CT, we explore three DA-TATB lots that reflect evolutionary processing changes, plus one WA-TATB material. Micro CT imaged crystal collections show the exterior grain structure, revealing its roughness and providing a crude particle size measurement. The DA-TATB lots that test most sensitively in the LANL ECOT corner-turning test are roughest, having the appearance of being “corroded”. Nano-scale CT reveals both internal NH 4 Cl inclusions and void structures. The DA-TATB lots that tested intermediate and high sensitivity in ECOT exhibited similar wormhole structures, which were more extensive than that of the low-sensitivity lot. The least sensitive DA-TATB lot also retained more NH 4 Cl, consistent with reduced connectivity of voids to the surface.

1, 3, 5-triamino-2,4↗
DOE OSTI2021

A review of the effect of nanoclays on the fresh and hardened properties of cement-based materials

This paper provides an overview of the use of nanoclays in cement-based materials. The effect of nanoclays on shear rheological properties will be discussed, with a focus on structural build-up behavior. This macroscale flow behavior will then be tied to the effect of nanoclays on the fresh microstructure as characterized via in-situ particle size measurements and rheological techniques. This will provide insight on the mechanisms underlying the effect of nanoclays on fresh state properties through an improved understanding of their effect on flocculation and coagulation behavior. In addition, secondary effects nanoclays have on the hardening and hardened properties will also be discussed. Examples of casting applications in which nanoclays have been effectively utilized as rheological modifiers, i.e. reducing self-consolidating concrete formwork pressure, extrusion, semi-flowable concrete for slipform paving, and 3D concrete printing, will be presented. Finally, some thoughts on potential directions for future work will be shared.

36 MATERIALS SCIENCE↗
NASA NTRS1984

Comparative measurements using different particle size instruments

This paper discusses the measurement and comparison of particle size and velocity measurements in sprays. The general nature of sprays and the development of standard, consistent research sprays are described. The instruments considered in this paper are: pulsed laser photography, holography, television, and cinematography; laser anemometry and interferometry using visibility, peak amplitude, and intensity ratioing; and laser diffraction. Calibration is by graticule, reticle, powders with known size distributions in liquid cells, monosize sprays, and, eventually, standard sprays. Statistical analyses including spatial and temporal long-time averaging as well as high-frequency response time histories with conditional sampling are examined. Previous attempts at comparing instruments, the making of simultaneous or consecutive measurements with similar types and different types of imaging, interferometric, and diffraction instruments are reviewed. A program of calibration and experiments for comparing and assessing different instruments is presented.

Chigier, N.↗
DOE OSTI2023

Stochastic Unit Commitment: Model Reduction via Learning

As weather-dependent renewable generation increases its share in the generation mix of most electric energy systems, a stochastic unit commitment becomes the natural day-ahead scheduling tool. However, such a tool is generally computationally intractable if a detailed uncertainty description is considered. Taking this into account, we proposed a learning method to make the stochastic unit commitment problem tractable. Here, recent advances in statistical learning and machine learning to address optimization problems can be advantageously applied to the rather intractable stochastic unit commitment problem. Considering these advances, we explore simple learning techniques to drastically reduce the size of a stochastic unit commitment problem without significantly altering its optimal solution. The considered stochastic unit commitment problem is formulated as a two-stage stochastic programming problem. The first stage represents commitment decisions, while the second one represents the operation conditions under different scenarios. Taking into account historical solved instances (or proxies for them), we reduce the size (measured by numbers of constraints and variables) of the stochastic unit commitment problem by (i) fixing unchanged binary variables and by (ii) eliminating inactive inequality constraints. Our numerical results show that the reduced problem generally requires significantly less time to solve while obtaining high-quality solutions, which are very close to or indistinguishable from the one obtained by solving the original problem. We use an Illinois 200-bus system to illustrate and characterize the performance of the proposed problem-reduction method.

42 ENGINEERING↗
DOE OSTI2024

Impact of Backing Plate and Thermal Boundary Conditions for High-Speed Friction Stir Welding of 25-mm Thick Aluminum Alloy 7175-T79

Here this study demonstrates high-speed (150 mm/min) single pass friction stir butt joining of 25 mm thick aluminum alloy 7175-T79. To understand the impact of quenching and cooling rate on process responses, joint strength, and grain size distributions across the weld thickness, we performed a series of friction stir welding (FSW) trials in air and with a trailing water spray using steel and composite backing plates (BP). Welds made in air and trailing water spray exhibit significantly different hardness distributions across the nugget, heat affected zone (HAZ), and HAZ minimum hardness as evidenced by detailed microhardness mapping. The effect of trailing water spray (TWS) on joint efficiency overshadows the influence of BP composition due to the vastly different contribution to quenching. TWS also resulted in a multifaceted effect on FSW such as lowering processing temperature, increasing X and Z forces while lowering Y force, and narrow heat affecting zone. Finally, digital image correlation (DIC)-based fracture mode analysis and grain size measurements correlate with the hardness distribution.

42 ENGINEERING↗
DOE OSTI2024

Particle-wall heat transfer in narrow-channel bubbling fluidized beds for thermal energy storage

Robust metal oxide particles can provide low-cost and stable thermal energy storage (TES) to temperatures up to 1200 °C or higher. The transfer of heat into and out of the particles in cost-effective high-temperature particle heat exchangers remains a principal challenge to implementing particle-based TES. The present work expands on prior studies of particle-wall heat transfer in narrow-channel fluidized beds operated in the bubbling fluidization regime. Batch-mode experiments with various oxide particles over a range of temperatures and airflow rates indicate that particle-wall heat transfer increases with higher bed temperature and decreasing particle size. Measured particle-wall heat transfer coefficients in a 12 mm deep channel are fit to a Nusselt number correlation proportional to a non-monotonic function of excess fluidization velocity. Particle-wall heat transfer coefficients rise rapidly with excess fluidization velocities until reaching a maximum at intermediate air velocities due to a trade-off between enhanced transverse particle mixing and decreasing particle volume fraction with increased fluidization velocity. The heat transfer coefficient reaches a maximum of ≈ 400% of values without fluidization for oxide particles ranging in diameter d p from 159 to 408 μm. For the smallest particles tested, composed of olivine sand, particle-wall heat transfer coefficients peak above 1100 Wm –2 K –1 at 450 °C. 100-h tests at 500 °C and near-optimal heat transfer fluidization velocities indicated minimal wall wear or oxide scaling. Furthermore, high particle-wall heat transfer coefficients suggest narrow channel fluidized beds as a potential pathway for reducing the required surface area and cost of high-temperature particle heat exchangers, as needed in large-scale thermal energy storage applications.

14 SOLAR ENERGY↗
DOE OSTI2021

Burst characteristics of advanced accident-tolerant FeCrAl cladding under temperature transient testing

Here assessment of burst characteristics of accident-tolerant fuel (ATF) claddings is essential to evaluate the safety margins of nuclear reactors, and better understanding can enable accelerated licensing for reactor concepts that include the new materials. Therefore, this study investigated the burst behavior of an ATF candidate of C26M, which is an iron–chromium–aluminum alloy (FeCrAl) under transient testing like the simulated loss-of-coolant accident (LOCA) conditions, except the water-quenching phase, in light-water reactors (LWRs). The effect of LOCA specimen length was assessed in terms of post-burst tube parameters. No critical length effect was determined on the burst pressure, burst location, and burst size measurements. Burst temperature showed larger variation likely due to its measurement approach used in this study. The post-test diametral strain was identified as the critical parameter to reduce the specimen length as compared to tube burst length or width. Postmortem optical metrology and digital image correlation were employed to determine the local strain-state during the simulated LOCA, which showed the loading path was close to equibiaxial conditions in regions away from the burst location, rather than internally pressurized conditions (or “plane-strain” tension). Pst-test microstructural characterizations of the FeCrAl revealed that ductile damage was present at the edge of the outer radial surface while the rest of the material was ruptured via cleavage at LOCA burst temperatures. Furthermore, internal grain boundary cracks were observed at locations away from the tube burst region. This behavior was considered to occur during the cooling down period of the simulated LOCA test. Overall, this study aimed to provide essential data for fuel performance code development by considering micromechanics of the deformation and failure.

36 MATERIALS SCIENCE↗