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At least 199 records · Page 11

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NASA NTRS1973

Preparation and properties of polytetrafluoroethylene impregnated with rhenium oxides

The results of tests carried out to determine the properties of polytetrafluorethylene (PTFE) impregnated with rhenium oxides are presented. The tests included measurement of physical properties of the impregnated material and investigation of the effects of preparation process variables. Based on the latter tests a mechanism to describe the permeation process is postulated which identifies the rate controlling step to be diffusion of ReF6 molecules into the solid during the initial ReF6 soak. Physical property tests indicated that the electronic conductance is increased by many orders of magnitude while the desirable properties of the PTFE remain virtually unchanged.

Leibecki, H. F.↗

NASA NTRS1972

CMB-13 research on carbon and graphite

Research and development are reported on phenolic resin binders, coke flour, binder soaking, hot molding glass-like carbons, and particle packing.

Smith, M. C.↗

NASA NTRS1973

Environmental compatibility of the all-silica rigid surface insulation

Testing has demonstrated the compatibility of the all-silica surface insulation system to a variety of space shuttle orbiter environmental aspects for launch, on-orbit, and special reentry conditions. Among the more important results are the success of the cold soak tests, which indicate the suitability of the foam/bond attachment system with a 2 mm thick foam pad for strain isolation, and the reentry temperature overshoot tests (to 1924 K), which show that this system can tolerate considerable dispersion in reentry heating environment.

Housten, S. J.↗

NASA NTRS1973

Optimum TPS Design with Rei-mullite

It has been shown that a ceramic mullite fiber/mullite insulation has adequate margins-of-safety based on minimum strengths for the critical thermostructural conditions of the shuttle mission. Introduction into the design of the new lower density foam bond material provides cold soak and cold entry capability at 116 K (-250 F). Finally, design solutions to the coating cracking tendencies have been identified and the solution analytically verified with three dimensional thermostructural analysis.

Hess, T. E.↗

NASA NTRS1973

Silica RSI for Application to the Shuttle Orbiter

Silica reusable surface insulation is analyzed for its cold soak properties, bond properties at low temperature, gap and step heating effects, and aerodynamic surface roughness effects to determine space shuttle weight and cost sensitivity to structure subsystem weights. Computerized simulation studies show that total program cost savings of silica (vs. mullite) exceed thermal protection system design and development costs and that an early introduction of silica increases total program cost savings.

Forsberg, K. J.↗

NASA NTRS1973

Heat shielding for Venus entry probes.

Two contrasted approaches to ablative thermal protection of Venus entry probes are presented - a typical carbonaceous charring ablator and a dielectric reflective ablator. The interesting observation in this study is that mass loss is not the controlling variable in heat-shield sizing. A heat-soak problem determines the carbon phenolic sizing. For Teflon, the material thickness required to accomplish reflection is the sizing factor. The total heat-shield weight required to handle either steep or shallow entry is computed to be 13% less for a Teflon shield (if at least 3.2 mm are required for reflection) than for a charring ablator shield. If an efficient reflective backing is used with Teflon, the thickness can be reduced 1.0 mm and the computed weight is 31% less for Teflon than for the charring ablator. Such weight reductions may significantly increase the science payload weight of the miniprobes.

Peterson, D. L.↗

NASA NTRS1973

Initial development of an ablative leading edge for the Space Shuttle orbiter.

A state-of-the-art preliminary design for typical wing areas is developed. Seven medium-density ablators (with/without honeycomb, flown on Apollo, Prime, X15A2) are evaluated. The screening tests include (1) leading-edge models sequentially subjected to ascent heating, cold soak, entry heating, post-entry pressure fluctuations, and touchdown shock, and (2) virgin/charred models subjected to bondline strains. Four materials (none molded) are found acceptable. The ESA 3560 HF and MOD 7 Hc (an AVCO 30 pcf elastomer) are selected. Roughness/recession degradation of low speed aerodynamics appears acceptable. The design, including attachments, substructure and joints, is presented.

Daforno, G.↗

NASA NTRS1974

Development of coatings to control electroosmosis in zero gravity electrophoresis

A major problem confronting the operation of free fluid electrophoresis in zero gravity is the control of electrokinetic phenomena and, in particular, electroosmosis. Due to the severity of counter flow, as a result of electroosmosis, the electrical potential developed at the surface of shear must be maintained at near, or as close to, zero millivolts as possible. Based upon this investigation, it has been found that the amount of bound water or the degree of hydroxylation plays a major role in the control of this phenomena. Of necessity, factors, such as adhesion, biocompatibility, protein adsorption, and insolubility were considered in this investigation because of the long buffer-coating exposure times required by present space operations. Based upon tests employing microcapillary electrophoresis, it has been found that gamma amino propyl trihydroxysilane produced a coating which provides the lowest potential (minus 3.86 mv) at the surface of shear between the stationary and mobile layers. This coating has been soaked in both borate and saline buffers, up to three months, in a pH range of 6.5 to 10 without deleterious effects or a change in its ability to control electrokinetic effects.

Krupnick, A. C.↗

NASA NTRS1974

Performance of LI-1542 reusable surface insulation system in a hypersonic stream

The thermal and structural performance of a large panel of LI-1542 reusable surface insulation tiles was determined by a series of cyclic heating tests using radiant lamps and aerothemal tests in the Langley 8-foot high-temperature structures tunnel. Aerothermal tests were conducted at a free-stream Mach number of 6.6, a total temperature of 1830 K, Reynolds numbers of 2.0 and 4,900,000 per meter, and dynamic pressures of 29 and 65 kPa. The results suggest that pressure gradients in gaps and flow impingement on the header walls at the end of longitudinal gaps are sources for increased gap heating. Temperatures higher than surface radiation equilibrium temperature were measured deep in gaps and at the header walls. Also, the damage tolerance of the LI-1542 tiles appears to be very high. Tile edge erosion rate was slow; could not be tolerated in a shuttle application. Tiles soaked with water and subjected to rapid depressurization and aerodynamic heating showed no visible evidence of damage.

Hunt, L. R.↗

NASA NTRS1974

Initial development of an ablative leading edge for the space shuttle orbiter

A state-of-the-art preliminary design for typical wing areas is developed. Seven medium-density ablators (with/without honeycomb, flown on Apollo, Prime, X15A2) are evaluated. The screening tests include: (1) leading-edge models sequentially subjected to ascent heating, cold soak, entry heating, post-entry pressure fluctuations, and touchdown shock, and (2) virgin/charred models subjected to bondline strains. Two honeycomb reinforced 30 pcf elastomeric ablators were selected. Roughness/recession degradation of low speed aerodynamics appears acceptable. The design, including attachments, substructure and joints, is presented.

Daforno, G.↗

NASA NTRS1974

Concentration changes during eutectic solidification

Thermotransport (or thermal diffusion, Soret effect) is shown to cause significant amount of segregation during the directional solidification of aluminum-copper eutectic. The concentration changes are predicted quantitatively and they are a function of temperature gradient, rate of melting and solidification and the time of soaking. There is a fair agreement between the experiments and calculations. A process is suggested where these concentration changes may be minimized.

Bhat, B. N.↗

NASA NTRS1974

High temperature antenna development for space shuttle, volume 2

An S-band antenna system and a group of off-the-shelf aircraft antenna were exposed to temperatures simulating shuttle orbital cold soak and entry heating. Radiation pattern and impedance measurements before and after exposure to the thermal environments were used to evaluate the electrical performance. The results of the electrical and thermal testing are given. Test data showed minor changes in electrical performance and established the capability of these antenna to withstand both the low temperatures of space flight and the high temperatures of entry.

Kuhlman, E. A.↗

NASA NTRS1974

Preparation, testing and analysis of zinc diffusion samples, NASA Skylab experiment M-558

Transport mechanisms of zinc atoms in molten zinc were investigated by radiotracer techniques in unit and in near-zero gravity environments. Each melt in the Skylab flight experiments was maintained in a thermal gradient of 420 C to 790 C. Similar tests were performed in a unit gravity environment for comparison. After melting in the gradient furnace followed by a thermal soak period (the latter was used for flight samples only), the samples were cooled and analyzed for Zn-65 distribution. All samples melted in a unit gravity environment were found to have uniform Zn-65 distribution - no concentration gradient was observed even when the sample was brought rapidly to melting and then quenched. Space-melted samples, however, showed textbook distributions, obviously the result of diffusion. It was evident that convection phenomena were the dominant factors influencing zinc transport in unit gravity experiments, while diffusion was the dominant factor in near-zero gravity experiments.

Braski, D. N.↗

NASA NTRS1975

Experimental evaluation of joint designs for a space-shuttle orbiter ablative leading edge

The thermal performance of two types of ablative leading-edge joints for a space-shuttle orbiter were tested and evaluated. Chordwise joints between ablative leading-edge segments, and spanwise joints between ablative leading-edge segments and reusable surface insulation tiles were exposed to simulated shuttle heating environments. The data show that the thermal performance of models with chordwise joints to be as good as jointless models in simulated ascent-heating and orbital cold-soak environments. The suggestion is made for additional work on the joint seals, and, in particular, on the effects of heat-induced seal-material surface irregularities on the local flow.

Tompkins, S. S.↗

NASA NTRS1975

Fiber reinforced solids possessing great fracture toughness: The role of interfacial strength

The results of angle-ply investigations for strength and toughness of brittle fiber/brittle filament composites are presented. General results are discussed for both unidirectional and angle-ply intermittently bonded boron/epoxy composites as affected by soaking and freezing water environments. A description of and the operating instructions are included for the modified 230 mm (9 inch) wide intermittent coating tape making apparatus.

Atkins, A. G.↗

NASA NTRS1977

Temperature reference for microwave radiometer calibration

New temperature reference avoids need to physically remove antenna and replace it with calibrating termination. Device is piece of porous microwave absorber fitted with cap of nonporous plastic foam. Absorbent material is soaked with cryogen. Procedure ensures that temperature at which microwaves are absorbed is exactly that of cryogen.

Love, A. W.↗

NASA NTRS1975

Application and utilization of a space chamber for the drying and decontamination of books, documents and other materials

Truckloads of materials such as rare books, papers, engineering drawings, blue prints, art work, leather objects such as shoes, and clothing were successfully dried, decontaminated and impregnated against future infestation by microorganisms in a large 12 x 24 foot vacuum chamber designed originally for testing unmanned spacecraft. The process is unique in that it allows either frozen or wet material, soaked by some castastrophic event to be dried and sterilized in the same chamber with a minimum of handling and transportation.

Koesterer, M. G.↗

NASA NTRS1976

Monotectic and syntectic alloys experiment MA-044

The flight test furnace run of the monotectic and syntectic alloys experiment was successfully performed during the Apollo Soyuz Test Project mission. All three experiment cartridges were returned intact. A second ground based test was conducted after the mission to provide one g samples with an equivalent thermal history. The examinations of all flight and ground based cartridges and ampoules have been completed. Encouraging results have been obtained in the preliminary analysis of one flight aluminum antimonide sample as compared to ground based and prototype test counterparts. In terms of reduction of the unwanted second phase, the low g sample shows a homogeneity improvement by a factor of 5 to 20. Preliminary examination of one lead zinc flight sample shows a dispersion of lead in the zinc matrix. However, complete homogenization of the material did not occur. A thermal analysis of flight data shows that the average soak temperature for the head zinc ampoules was 20 C lower than planned but 35 C above the published consolute temperature..

Ang, C. Y.↗