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At least 217 records · Page 12

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NASA NTRS2003

Quantitating Iron in Serum Ferritin by Use of ICP-MS

A laboratory method has been devised to enable measurement of the concentration of iron bound in ferritin from small samples of blood (serum). Derived partly from a prior method that depends on large samples of blood, this method involves the use of an inductively-coupled-plasma mass spectrometer (ICP-MS). Ferritin is a complex of iron with the protein apoferritin. Heretofore, measurements of the concentration of serum ferritin (as distinguished from direct measurements of the concentration of iron in serum ferritin) have been used to assess iron stores in humans. Low levels of serum ferritin could indicate the first stage of iron depletion. High levels of serum ferritin could indicate high levels of iron (for example, in connection with hereditary hemochromatosis an iron-overload illness that is characterized by progressive organ damage and can be fatal). However, the picture is complicated: A high level of serum ferritin could also indicate stress and/or inflammation instead of (or in addition to) iron overload, and low serum iron concentration could indicate inflammation rather than iron deficiency. Only when concentrations of both serum iron and serum ferritin increase and decrease together can the patient s iron status be assessed accurately. Hence, in enabling accurate measurement of the iron content of serum ferritin, the present method can improve the diagnosis of the patient s iron status. The prior method of measuring the concentration of iron involves the use of an atomic-absorption spectrophotometer with a graphite furnace. The present method incorporates a modified version of the sample- preparation process of the prior method. First, ferritin is isolated; more specifically, it is immobilized by immunoprecipitation with rabbit antihuman polyclonal antibody bound to agarose beads. The ferritin is then separated from other iron-containing proteins and free iron by a series of centrifugation and wash steps. Next, the ferritin is digested with nitric acid to extract its iron content. Finally, a micronebulizer is used to inject the sample of the product of the digestion into the ICPMS for analysis of its iron content. The sensitivity of the ICP-MS is high enough to enable it to characterize samples smaller than those required in the prior method (samples can be 0.15 to 0.60 mL).

Smith, Scott M.↗

DOE OSTI2026

Lethality is Local, but Survival is Systemic: Temporal and Multi-Organ Responses to Chlorine Gas Exposure in a Murine Model

Chlorine gas (Cl2) is a highly toxic chemical associated with both localized lung injury and systemic health effects. While pulmonary damage has been well characterized, the systemic inflammatory and metabolic responses remain poorly understood. We aimed to define the temporal and multi-organ responses to Cl2 exposure in a murine model, with a focus on identifying spatiotemporal inflammation and its impact on survival and lethality. SKH1 mice were exposed for 10 min to varying concentrations of Cl2 (94.4–810 ppm, representative of non-lethal, LD10, and LD50 doses) and monitored for respiratory function, perfusion, and acidosis using organ-specific imaging. At multiple time points (40 min, 6 h, 24 h, and 7 d), we measured phosphoproteins, cytokines, chemokines, growth factors, and metabolic hormones in the lungs, heart, cortex, and plasma. Statistical modeling and logistic regression were used to identify biomarkers associated with lethality and survival. We found that lung injury was the primary cause of potential lethality, particularly via early phosphoprotein signaling disruptions. However, survival correlated with early systemic coordination of inflammatory and metabolic signals across organs. Perfusion and acidosis imaging were strongly associated with chemokine and hormone responses. Key survival-associated plasma biomarkers included decreased insulin, increased ghrelin, and decreased eotaxin. While potential lethality from Cl2 exposure is locally driven by pulmonary injury, survival depends on systemic, multi-organ responses that occur rapidly post-exposure. Within this model, our findings identify a potential therapeutic window to enhance survival and suggest candidate biomarkers that may be explored translationally for both triage and treatment of chlorine-related incidents.

chlorine gas↗

DOE OSTI2024

Phased array-based nonlinear wave mixing technique: Application to lack-of-fusion porosity characterization in additively manufactured metals

The objective of this research is to demonstrate the effectiveness of a phased array-based nonlinear wave mixing technique to characterize internal, localized microscale damage in an additively manufactured (AM) component. By using phased arrays for the generation of the incident waves, it is possible to produce a nonlinear wave mixing scanning technique without the need for immersion or changing coupling conditions. The phased arrays can be configured to generate incident waves in multiple directions that meet the resonance conditions required for nonlinear wave mixing at a variety of internal locations. This allows for the scanning of a specimen without the removal and re-coupling of the source transducers, leading to greater scanning speed and repeatability. To demonstrate the accuracy of this phased array wave mixing approach, measurements of acoustic nonlinearity in an AM component are first made with a bulk wave second harmonic generation through thickness measurement. Next, nonlinear wave mixing measurements are made with single element transducers to confirm the sensitivity of the proposed nonlinear wave mixing approach to lack-of-fusion porosity in AM metals. Finally, phased arrays are used to highlight the effectiveness of the proposed nonlinear wave mixing technique in these same AM components.

Acoustics↗

NASA NTRS1977

The Space Shuttle Main Engine High-Pressure Fuel Turbopump rotordynamic instability problem

The SSME (Space Shuttle Main Engine) HPFTP (High-Pressure Fuel Turbopump) has been subject to a rotordynamic instability problem, characterized by large and damaging subsynchronous whirling motion. The original design of the HPFTP (from a rotordynamic viewpoint) and the evolution of the HPFTP subsynchronous whirl problem are reviewed. The models and analysis which have been developed and utilized to explain the HPFTP instability and improve its stability performance are also reviewed. Elements of the rotordynamic model which are discussed in detail include the following: (a) hydrodynamic forces due to seals, (b) internal rotor damping, (c) bearing and casing support stiffness asymmetry, and (d) casing dynamics. The stability and synchronous response characteristics of the following two design alternatives are compared: (a) a 'stiff' symmetric bearing support design and (b) a damped asymmetric stiffness design. With appropriate interstage seal designs, both designs are shown, in theory to provide substantially improved stability and synchronous response characteristics in comparison to the original design. The asymmetric design is shown to have better stability and synchronous response characteristics than the stiffly supported design.

Childs, D. W.↗

NASA NTRS1988

Nondestructive evaluation of advanced ceramics

A review is presented of Lewis Research Center efforts to develop nondestructive evaluation techniques for characterizing advanced ceramic materials. Various approaches involved the use of analytical ultrasonics to characterize monolythic ceramic microstructures, acousto-ultrasonics for characterizing ceramic matrix composites, damage monitoring in impact specimens by microfocus X-ray radiography and scanning ultrasonics, and high resolution computed X-ray tomography to identify structural features in fiber reinforced ceramics.

Klima, Stanley J.↗

NASA NTRS1991

Large area QNDE inspection for airframe integrity

Quantitative Nondestructive Evaluation (QNDE) technology is being developed to provide new options for cost effective inspection of airframes. An R&D effort based on five NDE technologies is addressing questions of structural bonding assessment, corrosion detection, multisite damage detection, and fatigue characterization. The research/applications are being conducted by prioritized focussing and staging of the following technologies: (1) thermal NDE; (2) ultrasonic NDE; (3) coherent optical NDE; (4) magnetic imaging NDE; and (5) radiographic NDE. The focus here is on the most recent applications of thermal NDE technology to large area inspection of lap-joint and stiffener bonds. The approach is based on pulsed radiant heating of the airframe and measurement of the surface temperature of the structure with an infrared imager. Several advantages of the technique are that it is noncontacting, inspects one square meter area in a period of less than 2 minutes and has no difficulty inspecting typical curvatures of the fuselage. Numerical models of heat flow in these geometries are used to determine appropriate techniques for reduction of the infrared images, thereby delineating regions of disbonds. These models are also used to determine the optimum heating and measurement times for maximizing the contrast between bonded and unbonded structures. Good agreement is found between these results and experimental measurements, and a comparison of the two are presented. Also presented are results of measurements on samples with fabricated defects which show the technique is able to clearly indicate regions of disbonds. Measurements on an airframe also clearly image subsurface structure.

Winfree, William P.↗

NASA NTRS1993

Investigation of Zerodur material processing

The Final Report of the Center for Applied Optics (CAO), of The University of Alabama (UAH) study entitled 'Investigation of Zerodur Material Processing' is presented. The objectives of the effort were to prepare glass samples by cutting, grinding, etching, and polishing block Zerodur to desired specifications using equipment located in the optical shop located in the Optical System Branch at NASA/MSFC; characterize samples for subsurface damage and surface roughness; utilize Zerodur samples for coating investigations; and perform investigations into enhanced optical fabrication and metrology techniques. The results of this investigation will be used to support the Advanced X Ray Astrophysics Facility (AXAF) program as well as other NASA/MSFC research programs. The results of the technical effort are presented and discussed.

Johnson, R. Barry↗

NASA NTRS1994

Milestone 4: Test plan for Reusable Hydrogen Composite Tank System (RHCTS). Task 3: Composite tank materials

This document is the detailed test plan for the series of tests enumerated in the preceding section. The purpose of this plan is to present the test objectives, test parameters and procedures, expected performance and data analysis plans, criteria for success, test schedules, and related safety provisions and to describe the test articles, test instrumentation, and test facility requirements. Initial testing will be performed to screen four composite materials for suitability for SSTO LH2 tank loads and environmental conditions. The laminates for this testing will be fabricated by fiber placement, which is the manufacturing approach identified as baseline for the tank wall. Even though hand layup will be involved in fabricating many of the internal structural members of the tank, no hand-layup laminates will be evaluated in the screening or subsequent characterization testing. This decision is based on the understanding that mechanical properties measured for hand-layup material should be at least equivalent to properties measured for fiber-placed material, so that the latter should provide no less than a conservative approximation of the former. A single material will be downselected from these screening tests. This material will be subsequently characterized for impact-damage tolerance and durability under conditions of mechanical and thermal cycling, and to establish a preliminary design database to support ongoing analysis. Next, testing will be performed on critical structural elements fabricated from the selected material. Finally, the 8-foot diameter tank article, containing the critical structural features of the full-scale tank, will be fabricated by fiber placement and tested to verify its structural integrity and LH2 containment.

Greenberg, H. S.↗

NASA NTRS2007

The Effect of Delamination on Damage Path and Failure Load Prediction for Notched Composite Laminates

The influence of delamination on the progressing damage path and initial failure load in composite laminates is investigated. Results are presented from a numerical and an experimental study of center-notched tensile-loaded coupons. The numerical study includes two approaches. The first approach considers only intralaminar (fiber breakage and matrix cracking) damage modes in calculating the progression of the damage path. In the second approach, the model is extended to consider the effect of interlaminar (delamination) damage modes in addition to the intralaminar damage modes. The intralaminar damage is modeled using progressive damage analysis (PDA) methodology implemented with the VUMAT subroutine in the ABAQUS finite element code. The interlaminar damage mode has been simulated using cohesive elements in ABAQUS. In the experimental study, 2-3 specimens each of two different stacking sequences of center-notched laminates are tensile loaded. The numerical results from the two different modeling approaches are compared with each other and the experimentally observed results for both laminate types. The comparisons reveal that the second modeling approach, where the delamination damage mode is included together with the intralaminar damage modes, better simulates the experimentally observed damage modes and damage paths, which were characterized by splitting failures perpendicular to the notch tips in one or more layers. Additionally, the inclusion of the delamination mode resulted in a better prediction of the loads at which the failure took place, which were higher than those predicted by the first modeling approach which did not include delaminations.

Satyanarayana, Arunkumar↗

NASA NTRS2012

Environmental Durability and Stress Rupture of EBC/CMCs

This research focuses on the strength and creep performance of SiC fiber-reinforced SiC ceramic matrix composite (CMC) environmental barrier coating (EBC) systems under complex simulated engine environments. Tensile-strength and stress-rupture testing was conducted to illustrate the material properties under isothermal and thermal gradient conditions. To determine material durability, further testing was conducted under exposure to thermal cycling, thermal gradients and simulated combustion environments. Emphasis is placed on experimental techniques as well as implementation of non-destructive evaluation, including modal acoustic emission and electrical resistivity monitoring, to characterize strength degradation and damage mechanisms. Currently, little is known about the behavior of EBC-CMCs under these conditions; consequently, this work will prove invaluable in the development of structural components for use in high temperature applications.

Appleby, Matthew↗

NASA NTRSDate not supplied

Lunar Dust Effects on Space Mechanism Ball Bearings for Sustained Human Lunar Operations

NASA has plans to send humans back to the moon under the Artemis Mission. In 2024, the first humans will set foot on the lunar surface since Apollo 17 in 1972. Additionally, extended plans include a sustained human presence on the moon for long duration habitation. These lofty goals will require many different kinds of space mechanisms including: life support, mobility, excavation, scientific instrumentation, etc. Many of these types of systems utilize rotating machinery which require rolling element bearings. As such, dust tolerance of bearings is a major concern for long life in these critical systems. A research activity has been undertaken to characterize and reduce the damage lunar soil (called regolith) dust causes to bearings. The present work details some preliminary results of ball bearings running with grease intentionally contaminated with known quantities and sizes of lunar simulant particles to assess damage. Various bearing material combinations were tested to determine how certain typical bearing materials respond.

BEARINGS↗

NASA NTRSDate not supplied

Prometheus and Constellation Materials Research and Testing Overview

Outline - New Technologies and New Materials meet Flight Program - Reactor Materials Selection - Material Radiation Resistance - Testing in four different radiation environments - Superalloy Creep Testing - Superalloy-Refractory Alloy Joining - Superalloy, Stainless Steel, Copper Brazing - Superalloy-Refractory Cross Contamination - Na and NaK Compatibility - Radiator Panel Materials Selection

nuclear power↗

NASA NTRS2024

Enhancing the Protection of Shielded Thermal Protection Systems in Sample Return Spacecraft Against MMOD Impact

Sample return missions seek to collect samples from planets, moons, asteroids, and other planetary bodies and return them to earth for in-depth analysis. Backward planetary protection requirements are often in place for such missions to prevent the introduction of any extra-terrestrial material into the Earth’s biosphere, which could occur if a meteoroid or space debris particle were to damage a critical part of the returning spacecraft. The ability of a shielding system used to mitigate this damage risk is typically characterized by a ballistic limit equation (BLE), which predicts whether or not a protected system or structural element will sustain a critical failure due to a high-speed impact. In this paper, we develop a particle-impact-based BLE for the thermal protection system (TPS) of a sample return spacecraft that is protected by a multi-shock shield. The predictions of the BLE we develop for TPS failure are shown to be consistent with the predictions of hydrocode simulations.

Sample Return Spacecraft↗

NASA NTRS2015

Cohesive Laws for Analyzing Through-Crack Propagation in Cross Ply Laminates

The laminate cohesive approach (LCA) is a methodology for the experimental characterization of cohesive through-the-thickness damage propagation in fiber-reinforced polymer matrix composites. LCA has several advantages over other existing approaches for cohesive law characterization, including: visual measurements of crack length are not required, structural effects are accounted for, and LCA can be applied when the specimen is too small to achieve steady-state fracture. In this work, the applicability of this method is investigated for two material systems: IM7/8552, a conventional prepreg, and AS4/VRM34, a non-crimp fabric cured using an out-of-autoclave process. The compact tension specimen configuration is used to propagate stable Mode I damage. Trilinear cohesive laws are characterized using the fracture toughness and the notch tip opening displacement. Test results are compared for the IM7/8552 specimens with notches machined by waterjet and by wire slurry saw. It is shown that the test results are nearly identical for both notch tip preparations methods, indicating that significant specimen preparation time and cost savings can be realized by using the waterjet to notch the specimen instead of the wire slurry saw. The accuracy of the cohesive laws characterized herein are assessed by reproducing the structural response of the test specimens using computational methods. The applicability of the characterization procedure for inferring lamina fracture toughness is also discussed.

Bergan, Andrew C.↗

NASA NTRS2014

MMOD Impact Damage to ISS

Paper will describe micrometeoroid and orbital debris (MMOD) damage that has been observed on the International Space Station (ISS). Several hundred documented MMOD damage sites on ISS have been identified through imagery from the windows of ISS modules or docked vehicles. Sites that are observable from ISS or shuttle windows exhibiting distinct features of hypervelocity impact damage are usually greater than 5mm in diameter. Many smaller features are revealed in on-orbit imagery are typically less distinct and difficult to characterize but could be MMOD damage. Additional images of on-orbit damage features have been collected by astronauts during extra vehicular activities. Ground inspection of returned ISS hardware has also contributed to the database of ISS MMOD impact damage. A handful of orbital replacement units (ORU) from the ISS active thermal control and electrical power subsystems were swapped out and returned during the Space Shuttle program. In addition, a reusable logistics module was deployed on ISS for a total 59.4 days on 11 shuttle missions between 2001 and 2011 and then brought back in the shuttle payload bay. All of this returned hardware was subjected to detailed post-flight inspections for MMOD damage, and a database with nearly 1000 impact records has been collected. A description of the largest observed damages will be provided in the paper. In addition, a discussion of significant MMOD impact sites with operational or design aspects will be presented. Some of the ISS modules/subsystems damaged by MMOD to be included in the discussion are (1) Solar Arrays, (2) US and Russian windows, (3) EVA handrails, (4) Radiators, and (5) Russian FGB module.

Hyde, James L.↗

NASA NTRS2017

Compendium of Current Total Ionizing Dose and Displacement Damage Results from NASA Goddard Space Flight Center and NASA Electronic Parts and Packaging Program

Total ionizing dose and displacement damage testing was performed to characterize and determine the suitability of candidate electronics for NASA space utilization. Devices tested include optoelectronics, digital, analog, linear bipolar devices, and hybrid devices. Displacement Damage, Optoelectronics, Proton Damage, Single Event Effects, and Total Ionizing Dose.

Proton Damage↗

NASA NTRS2008

Formation of Clustered DNA Damage after High-LET Irradiation: A Review

Radiation can cause as well as cure cancer. The risk of developing radiation-induced cancer has traditionally been estimated from cancer incidence among survivors of the atomic bombs in Hiroshima and Nagasaki. These data provide the best estimate of human cancer risk over the dose range for low linear energy transfer (LET) radiations, such as X- or gamma-rays. The situation of estimating the real biological effects becomes even more difficult in the case of high LET particles encountered in space or as the result of domestic exposure to particles from radon gas emitters or other radioactive emitters like uranium-238. Complex DNA damage, i.e., the signature of high-LET radiations comprises by closely spaced DNA lesions forming a cluster of DNA damage. The two basic groups of complex DNA damage are double strand breaks (DSBs) and non-DSB oxidative clustered DNA lesions (OCDL). Theoretical analysis and experimental evidence suggest there is increased complexity and severity of complex DNA damage with increasing LET (linear energy transfer) and a high mutagenic or carcinogenic potential. Data available on the formation of clustered DNA damage (DSBs and OCDL) by high-LET radiations are often controversial suggesting a variable response to dose and type of radiation. The chemical nature and cellular repair mechanisms of complex DNA damage have been much less characterized than those of isolated DNA lesions like an oxidized base or a single strand break especially in the case of high-LET radiation. This review will focus on the induction of clustered DNA damage by high-LET radiations presenting the earlier and recent relative data.

Hada, Megumi↗

DOE OSTI2025

A review of radiation-induced damage to quantum dots

Quantum dots (QDs) are versatile nano structures that have applications in many fields of research and production, including biosensor technology, computing, photovoltaics, and optoelectronics. QDs have gained interest in the field of radiation detection because of their relative ease of production, tunable photoluminescence, and sensitivity to ionizing radiation. The photoluminescent properties of QDs diminish proportionally to prolonged ionizing radiation interactions, leading many groups to seek out these materials as potential candidates for the next generation of inexpensive, easily manufactured dosimetry and sensors. To use QDs in these applications, the mechanisms of radiation damage to the nanomaterial must be clearly understood and characterized. Herein, we review the study of ionizing radiation damage to QDs. First, the synthesis and properties of QDs are briefly discussed. Next, the radiation damage to QDs due to heavy charged particles, fast electrons, high energy photons, and neutrons are detailed. After this, experimental methods and modelling of QDs in radiation environments are examined. Lastly, future research directions are provided. The goal of this review is to aid in understanding the ionizing radiation effects on QD-based devices.

Snow, Jesse [University of Utah, Salt Lake City, U↗