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At least 217 records · Page 12

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DOE OSTI2024

Low-temperature Leidenfrost-like jumping of sessile droplets on microstructured surfaces

The Leidenfrost effect—the levitation and hovering of liquid droplets on hot solid surfaces—generally requires a sufficiently high substrate temperature to activate liquid vaporization. Here, in this paper, we report the modulation of Leidenfrost-like jumping of sessile water microdroplets on micropillared surfaces at a relatively low temperature. Compared to traditional Leidenfrost effect occurring above 230 °C, the fin-array-like micropillars enable water microdroplets to levitate and jump off the surface within milliseconds at a temperature of 130 °C by triggering the inertia-controlled growth of individual vapour bubbles at the droplet base. We demonstrate that droplet jumping, resulting from momentum interactions between the expanding vapour bubble and the droplet, can be modulated by tailoring of the thermal boundary layer thickness through pillar height. This enables regulation of the bubble expansion between the inertia-controlled mode and the heat-transfer-limited mode. The two bubble-growth modes give rise to distinct droplet jumping behaviours characterized by constant velocity and constant energy regimes, respectively. This heating strategy allows the straightforward purging of wetting liquid droplets on rough or structured surfaces in a controlled manner, with potential applications including the rapid removal of fouling media, even when located in surface cavities.

42 ENGINEERING↗

DOE OSTI2021

Active motion of multiphase oil droplets: emergent dynamics of squirmers with evolving internal structure

Synthetic soft matter systems, when driven beyond equilibrium by active processes, offer the potential to achieve dynamical states and functions of a complexity found in living matter. Emulsions offer the basis of a simple yet versatile system for identification of the physicochemical principles underlying active soft matter, but how multiple internal phases within emulsion droplets (e.g., Janus morphologies) organize to impact emergent dynamics is not understood. Here, we create multiphase oil droplets with ultralow interfacial tensions but distinct viscosities, and drive them into motion in aqueous micellar solutions. Preferential solubilization of select components of the oil both drives the droplet motion and yields a progression of internal phase morphological states with distinct symmetries. In this work, we find the active droplets to exhibit five dynamical states during morphogenesis. By quantifying microscopic flow fields, we show that it is possible to map the diverse droplet behaviors to squirmer models of spherical microswimmers in Stokes flow, thus showing that multiphase droplets offer the basis of a versatile platform with which to study and engineer the hydrodynamics of microswimmers.

36 MATERIALS SCIENCE↗

DOE OSTI2021

Millimeter-wave electromagnetic monitoring for liquid metal droplet-on-demand printing

As new printing approaches emerge, in situ diagnostics to monitor the print quality in real-time become essential for long-term monitoring and feedback control. In this article, we present a millimeter-wave electromagnetic monitoring approach for liquid metal droplet-on-demand printing to support the high-speed and real-time evaluation of droplet ejection. An open-ended rectangular waveguide is placed perpendicular to a jetted droplet stream and operated at a continuous-wave frequency of 40 GHz. Liquid metal droplets with diameters as low as 1.2 mm are characterized, and droplet jetting events on the order of 500 μm are detected at ejection rates up to 80 Hz. The measured results demonstrate that trends at the macro-level (large-scale print variation and anomalies at the nozzle tip) as well as micro-level (droplet size, position, and dynamics) can be detected using this technique.

42 ENGINEERING↗

DOE OSTI2022

Sizes of pure and doped helium droplets from single shot x-ray imaging

Advancements in x-ray free-electron lasers on producing ultrashort, ultrabright, and coherent x-ray pulses enable single-shot imaging of fragile nanostructures, such as superfluid helium droplets. Furthermore, this imaging technique gives unique access to the sizes and shapes of individual droplets. In the past, such droplet characteristics have only been indirectly inferred by ensemble averaging techniques. Here, we report on the size distributions of both pure and doped droplets collected from single-shot x-ray imaging and produced from the free-jet expansion of helium through a 5 μm diameter nozzle at 20 bars and nozzle temperatures ranging from 4.2 to 9 K. This work extends the measurement of large helium nanodroplets containing 10 9 –10 11 atoms, which are shown to follow an exponential size distribution. Additionally, we demonstrate that the size distributions of the doped droplets follow those of the pure droplets at the same stagnation condition but with smaller average sizes.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

DOE OSTI2020

Lipid sponge droplets as programmable synthetic organelles

Living cells segregate molecules and reactions in various subcellular compartments known as organelles. Spatial organization is likely essential for expanding the biochemical functions of synthetic reaction systems, including artificial cells. Many studies have attempted to mimic organelle functions using lamellar membrane-bound vesicles. However, vesicles typically suffer from highly limited transport across the membranes and an inability to mimic the dense membrane networks typically found in organelles such as the endoplasmic reticulum. Here, we describe programmable synthetic organelles based on highly stable nonlamellar sponge phase droplets that spontaneously assemble from a single-chain galactolipid and nonionic detergents. Due to their nanoporous structure, lipid sponge droplets readily exchange materials with the surrounding environment. In addition, the sponge phase contains a dense network of lipid bilayers and nanometric aqueous channels, which allows different classes of molecules to partition based on their size, polarity, and specific binding motifs. The sequestration of biologically relevant macromolecules can be programmed by the addition of suitably functionalized amphiphiles to the droplets. We demonstrate that droplets can harbor functional soluble and transmembrane proteins, allowing for the colocalization and concentration of enzymes and substrates to enhance reaction rates. Droplets protect bound proteins from proteases, and these interactions can be engineered to be reversible and optically controlled. Our results show that lipid sponge droplets permit the facile integration of membrane-rich environments and self-assembling spatial organization with biochemical reaction systems.

59 BASIC BIOLOGICAL SCIENCES↗

DOE OSTI2022

NUMERICAL INVESTIGATION OF AIR DEHUMIDIFICATION THROUGH WATER DROPLETS DIELECTROPHORESIS

This paper numerically investigated the dehumidification of moist airflow in a converging rectangular duct with electrically enhanced condensation. The aim was to develop a condensation model that predicted water vapor condensation by employing the dielectrophoresis principle. The charged droplets were injected into the computational domain to produce a gradient electric field. The dielectrophoretic interaction between the droplets and vapor molecules of the humid air resulted in local water vapor condensation at the vapor and liquid droplet interface. This phenomenon is described in detail in this paper. A hybrid Eulerian-Lagrangian solver SprayFoam was developed based on OpenFOAM® to simulate condensation in two-phase gas-liquid mixtures. The following developments were made based on the standard compressible multiphase flow solver SprayFoam in OpenFOAM®: (1) Eulerian solver for gas phase (2) multi-component species transport, and (3) Lagrangian solver for gas-droplet two-phase flows and sub-models for liquid droplets. The newly developed numerical model was experimentally validated with data from a series of tests conducted in the authors' laboratory. The results showed that the simulations followed the same trends as the data, and the model predicted the condensation due to the electro-spray injection process in the air stream. The injected water droplets, which are electrically charged to their Rayleigh limits, increased in size while wiping out the humidity from the air. The simulations indicated that the dehumidification was about 1% for 0.5 cubic feet per minute airflow rate. Scaling up to larger flows is a future follow-up work.

Yel Mahi, *Maliha↗

NASA NTRS1974

Investigation of critical burning of fuel droplets

The steady combustion characteristics of droplets were considered in combustion chamber environments at various pressures, flow conditions, and ambient oxidizer concentrations for a number of hydrocarbon fuels. Using data obtained earlier, predicted gasification rates were within + or - 30% of measurements when the correction for convection was based upon average properties between the liquid surface and the flame around the droplet. Analysis was also completed for the open loop response of monopropellant droplets, based upon earlier strand combustion results. At the limit of large droplets, where the effect of flame curvature is small, the results suggest sufficient response to provide a viable mechanism for combustion instability in the frequency and droplet size range appropriate to practical combustors. Calculations are still in progress for a broader range of droplet sizes, including conditions where active combustion effects are small.

Faeth, G. M.↗

NASA NTRS1974

The effect of droplets in the air-sea transition zone on the sea brightness temperature

A model is presented which shows that, for a fully developed sea driven by the wind with speeds above 5 m/sec the air in the transition zone immediately above the air-sea interface is mixed with sea water droplets from bursting air bubbles. The absorptive droplet concentration in the zone is assumed to have a profile tapering off from the interface to zero at a certain height. The dielectric constant of the absorptive inhomogeneous droplet profile is thus both a function of the wind speed and the height above the interface. Both the inhomogeneity effect and the absorption-emission effect of the droplet concentration have been considered. Theoretical calculations show that the presence of the absorptive inhomogeneous droplet transition zone significantly increases the sea brightness temperature as wind speed rises. Combined effects of both the droplet areas and the foam areas on sea surface have also been considered.

Tang, C. C. H.↗

NASA NTRS1974

A zero-gravity demonstration of the collision and coalescence of water droplets

The mechanics of the collision and coalescence of liquid droplets is one of the main research areas in the fields of nuclear physics, astrophysics, meteorology and fluid mechanics. The crew members on the Skylab 3 and 4 missions were requested to perform demonstrations of the collision and coalescence of water droplets under the low gravity environment at orbital altitude. In Skylab 4 two water droplets with equal volumes, 30 cu cm each, were used. A dark colored droplet (contaminated with grape drink) moving with a velocity of 3.14 cm/sec collided with a stationary pink colored droplet (contaminated with strawberry drink) and coalescence occurred. Theoretical models are proposed to study the various stages of the collision-coalescence processes. Special considerations are concentrated in the investigation of the bounce-coalescence and coalescence-instability processes. The surface tension of the coalesced droplets was calculated to be 52 dynes/cm in perfect agreement with laboratory measurements made after the flight using a reproduction of the liquids.

Hung, R. J.↗

NASA NTRS1976

Oscillatory combustion of liquid monopropellant droplets

A theoretical investigation was conducted on the open-loop combustion response of monopropellant droplets and sprays to imposed pressure oscillations. The theoretical model was solved as a perturbation analysis through first order, yielding linear response results. Unsteady gas phase effects were considered in some cases, but the bulk of the calculations assumed a quasi-steady gas phase. Calculations were conducted using properties corresponding to hydrazine decomposition. Zero-order results agreed with earlier measurements of hydrazine droplet burning in combustion gases. The droplet response was greatest (exceeding unity in some cases) for large droplets with liquid phase temperature gradients; at frequencies near the characteristic frequency of the liquid phase thermal wave. The response of a spray is less than that of its largest droplet, however, a relatively small percentage of large droplets provides a substantial response (exceeding unity in some cases).

Chanin, S. P.↗

NASA NTRS1978

Sublimate morphology on 74001 and 74002 orange and black glassy droplets

SEM-EDX analysis of the surface morphology of the 74001 and 74002 orange and black glassy droplets has revealed the presence of ubiquitous micromound coatings. Assuming that the diameter of an individual micromound is an indication of total coating thickness, then the thickness of this volatile and metal-rich layer ranges from less than 20 A to over 300 A in thickness. On rare droplets the micromound coating is partially covered by a sparse population of crystals and masses that are essentially NaCl in composition. Additionally, an irregular mass on the surface of one black droplet may contain free sulfur. Amoeboid masses of iron, some with incipient crystal faces, are also present on a few droplet surfaces. The above features, i.e., halite crystals, sulfur-rich masses and amoeboid iron, are rare; the more common occurrence of metals and volatiles is in the micromound coating. Based on our observations of several hundred spheres from both Apollo and Luna missions, the classic micromound coating is unique to the Apollo 15 green and Apollo 17 orange and black droplets. Although some investigators have proposed various impact sequences to produce these unique droplets, the volcanic fire fountain origin is favored.

Clanton, U. S.↗

NASA NTRS1982

A new droplet generator

A new droplet generator is described. A loud speaker driven extractor needle was immersed in a pendant drop. Pulsing the speaker extracted the needle forming a fluid ligament which will decay into a droplet. The droplets were sized by stroboscopic photographs. The droplet's size was changed by varying the amplitude of the speaker pulses and the extractor needle diameter. The mechanism of droplet formation is discussed and photographs of ligament decay are presented. The droplet generator worked well on both oil and water based pesticide formulations. Current applications and results are discussed.

Slack, W. E.↗

NASA NTRS1983

The movement of water droplets in clouds around the nose of an atmospheric research aircraft

The dynamic interaction between droplets and the airflow around the hemispherical nose of an aircraft was evaluated. The effect of the aircraft nose on droplet sampling for cloud research is explained. The proportion of different droplet sizes and their concentration at each point around the aircraft nose were determined. In a cloud, interaction between droplets is negligible. Each particle acts, for the calculation of the forces applied to it, as if it is alone in the air. The airflow carrying the droplets, on the average, is not influenced by their presence. The trajectory of each droplet was studied separately after calculating dry airflow. Concentrations were found with a Lagrangian method, using two trajectories computed directly close to one another. Theory confirms that to within 3% experimentally measured concentrations are representative of those in a cloud.

Feuillebois, P.↗

NASA NTRS1985

The Stokes force on a droplet in an unbounded fluid medium due to capillary effects

The Stokes force on a fluid droplet is obtained when the droplet is placed in an unbounded fluid medium and motion ensues due to an arbitrary interfacial-tension gradient on the droplet surface. The force, derived here for a spherical droplet, is proportional to the integral of the interfacial-tension gradient over the droplet surface. When the interfacial-tension gradients are caused by temperature or concentration variations, the result for the force may be further specialized when convective transport effects are negligible. In this case, it is possible to express the force in terms of the gradient of the undisturbed temperature (or concentration) field evaluated at the location of the droplet center in a form analogous to Faxen's force law.

Subramanian, R. Shankar↗

NASA NTRS1987

Experimental test of liquid droplet radiator performance

The liquid droplet radiator (LDR) is a heat rejection system for space power systems wherein an array of heated liquid droplets radiates energy directly to space. The use of submillimeter droplets provides large radiating area-to-mass ratio, resulting in radiator systems which are several times lighter than conventional solid surface radiators. An experiment is described in which the power radiated by an array of 2300 streams of silicone oil droplets is measured to test a previously developed theory of the LDR radiation process. This system would be capable of rejecting several kW of heat in space. Furthermore, it would be suitable as a modular unit of an LDR designed for 100-kW power levels. The experiment provided confirmation of the theoretical dependence of droplet array emissivity on optical depth. It also demonstrated the ability to create an array of more than 1000 droplet streams having a divergence less than 1 degree.

Mattick, A. T.↗

NASA NTRS1991

Pressure-coupled vaporization and combustion responses of liquid-fuel droplets in high-pressure environments

The dynamic responses of liquid-fuel droplet vaporization and combustion to ambient pressure oscillations are examined. The analysis is based on the complete sets of conservation equations for both gas and liquid phases, and accommodates detailed treatments of finite-rate chemical kinetics and variable properties. With a full account of thermodynamic phase equilibrium at the droplet surface, the model enables a systematic examination of the effects of ambient flow conditions on the droplet behavior. The responses of hydrocarbon fuel droplets in both sub- and super-critical environments are investigated. Results indicate that the droplet gasification and burning mechanisms depend greatly on the ambient pressure. In particular, a rapid enlargement of the vaporization and combustion responses occurs when the droplet surface reaches its critical point, mainly due to the strong variations of latent heat of vaporization and thermophysical properties at the critical state.

Yang, Vigor↗

NASA NTRS1990

A Planar-Fluorescence Imaging Technique for Studying Droplet-Turbulence Interactions in Vaporizing Sprays

Droplet turbulence interactions directly affect the vaporization and dispersion of droplets in liquid sprays and therefore play a major role in fuel oxidizer mixing in liquid fueled combustion systems. Proper characterization of droplet turbulence interactions in vaporizing sprays require measurement of droplet size velocity and size temperature correlations. A planar, fluorescence imaging technique is described which is being developed for simultaneously measuring the size, velocity, and temperature of individual droplets in vaporizing sprays. Preliminary droplet size velocity correlation measurements made with this technique are presented. These measurements are also compared to and show very good agreement with measurements made in the same spray using a phase Doppler particle analyzer.

Santavicca, Dom A.↗

NASA NTRS1993

Studies of droplet burning and extinction

A project on droplet combustion, pursued jointly with F.L. Dryer of Princeton University, has now been in progress for many years. The project involves experiments on the burning of single droplets in various atmospheres, mainly at normal atmosperic pressure and below, performed in drop towers and designed to be performed aboard space-based platforms such as the Space Shuttle or the Space Station. It also involves numerical computations on droplet burning, performed mainly at Princeton, and asymptotic analyses of droplet burning, performed mainly at UCSD. The focus of the studies rests primarily on time-dependent droplet-burning characteristics and on extinction phenomena. The presentation to be given here concerns the recent research on application of asymptotic methods to investigation of the flame structure and extinction of hydrocarbon droplets. These theoretical studies are investigating the extent to which combustion of higher hydrocarbons - heptane, in particular - can be described by four-step reduced chemistry of the kind that has achieved a good degree of success for methane flames. The studies have progressed to a point at which a number of definite conclusions can now be stated. These conclusions and the reasoning that led to them are outlined here.

Williams, Forman A.↗