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At least 217 records · Page 12

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NASA NTRS1981

Oblique-incidence secondary emission from charged dielectronics

Experimental measurements and computer simulation of secondary electron emission coefficients for FEP-Teflon, for normal and oblique incidence in the presence of a normal electric field are reported. Knowledge of the electrostatic environment surrounding the specimen calculation of particle trajectories are considered. A simulation using a conformal mapping, a Green's integral, and a trajectory generator provides the necessary mathematical support for the measurements which have been made with normal fields of 1.5 and 2.7 kV/mm. When incidence is normal and energy exceeds the critical energy, the coefficient is given by V.58 and for oblique incidence this expression may be divided by the cosine of the angle. The parameter V sub 0 is a function of normal field. Measurements for values of V sub f are presented.

Robinson, J. W.↗

NASA NTRS1981

Materials characterization study of conductive flexible second surface mirrors

The status of prequalification and qualification work on conductive flexible second surface mirrors is described. The basic material is FEP Teflon witn either aluminium or silver vacuum deposited reflectors. The top layer has been made conductive by deposition of layer of a indium oxide. The results of a prequalification program comprised of decontamination, humidity, thermal cycling, thermal shock and vibration tests are presented. Thermo-optical and electrical properties. The results of a prequalification program comprised of decontamination, humidity, thermal cycling, thermal shock and vibration tests are presented. Thermo-optical and electrical properties, the electrostatic behavior of the materials under simulated substorm environment and electrical conductivity at low temperatures are characterized. The effects of simulated ultra violet and particles irradiation on electrical and thermo-optical properties of the materials are also presented.

Levadou, F.↗

NASA NTRS1981

Charging control techniques

Transparent conductive thin films of indium oxide and indium-tin oxide were evaluated for their properties to control charge buildup on satellite materials. Both oxide coatings were evaluated for their uniformity, stability, reproducibility and characteristics on various substrate materials such as FEP Teflon, Kapton, and glass. The process development toward optimization and characterization of these thin semiconductor oxide coatings and the evaluation on large sizes performed for qualification for use on thermal control satellite materials is described. The materials have been characterized in multiple energy electron plasma environment and at low temperatures. All radiation measurements of the coatings under simulated substorm conditions have exhibited the characteristics of stable charge control. Measurement of surface potential during and after irradiation by electrons up to 30 KeV and ionizing gamma radiation show an effective stable grounding surface.

Schmidt, R. E.↗

NASA NTRS1982

Secondary electron emission from a charged dielectric in the presence of normal and oblique electric fields

The secondary electron emission coefficient was obtained for a FEP-Teflon dielectric charged with monoenergetic electrons normally incident upon the surface of the specimen. Measurements of secondary emission coefficient were done for normal and oblique incidence with different primary beam energies in the presence of normal and oblique electric fields. A collimated probing beam was directed to different points on the surface of the specimen and the released or accumulated charge was monitored using an electrometer. The measured data for different probing beam energies, different impact points and different angles of incidence were plotted vs. impact energy and impact point. Data analyzed by computer simulations to find the potential distribution on the surface of the specimen and the electric field around it, is presented and discussed.

Javidi, B.↗

NASA NTRS1982

Development of a large area space solar cell assembly

The development of a large area high efficiency solar cell assembly is described. The assembly consists of an ion implanted silicon solar cell and glass cover. The important attributes of fabrication are the use of a back surface field which is compatible with a back surface reflector, and integration of coverglass application and cell fabrications. Cell development experiments concerned optimization of ion implantation processing of 2 ohm-cm boron-doped silicon. Process parameters were selected based on these experiments and cells with area of 34.3 sq cm wre fabricated. The average AMO efficiency of the twenty-five best cells was 13.9% and the best bell had an efficiency of 14.4%. An important innovation in cell encapsulation was also developed. In this technique, the coverglass is applied before the cell is sawed to final size. The coverglass and cell are then sawed as a unit. In this way, the cost of the coverglass is reduced, since the tolerance on glass size is relaxed, and costly coverglass/cell alignment procedures are eliminated. Adhesive investigated were EVA, FEP-Teflon sheet and DC 93-500. Details of processing and results are reported.

Spitzer, M. B.↗

NASA NTRS1983

Mass analysis of neutral particles and ions released during electrical breakdowns on spacecraft surfaces

A specialized spectrometer was designed and developed to measure the mass and velocity distributions of neutral particles (molecules and molecular clusters) released from metal-backed Teflon and Kapton films. Promising results were obtained with an insulation breakdown initiation system based on a moveable contact touching the insulated surfaces. A variable energy, high voltage pulse is applied to the contact. The resulting surface damage sites can be made similar in size and shape to those produced by a high voltage electron beam system operating at similar discharge energies. The point discharge apparatus was used for final development of several high speed recording systems and for measurements of the composition of the materials given off by the discharge. Results with this apparatus show evolution of large amounts of fluorocarbon fragments from discharge through Teflon FEP, while discharges through Kapton produce mainly very light hydrocarbon fragments at masses below about 80 a.m.u.

Kendall, B. R. F.↗

NASA NTRS1982

Use of high L.E.T. radiation to improve adhesion of metals to polytetrafluoroethylene

MgK alpha X-rays (1254 eV) and 2 keV electrons irradiate the surface of polytetrafluoro ethylene (PTFE). The damage is confined to a few tenths of a micron below the surface, and the doses exceed 10 to the eight power rad. X-ray Photoelectron Spectroscopy (XPS) of the irradiated surfaces and mass spectroscopy of the gaseous products of irradiation indicate that the damaged layer is crosslinked or branched PTFE. After either type of irradiation, the surface has enhanced affinity for metals and a lower contact angle with hexadecane. Tape pull tests show that evaporated Ni and Au films adhere better to the irradiated surface. XPS shows the Ni interacts chemically with PTFE forming NiF2 and possibly NiC. However, the gold adhesion and contact angle results indicate that the interaction is, at least in part, chemically nonspecific. Decreased contact angles on FEP Teflon crystallized against gold were attributed to either the presence of a polar oxygen layer or increased physical forces due to greater density. In the case of irradiated PTFE, no oxygen on the surface was observed. The crosslinked structure might, however, have a greater density, thus accounting for the observed increase in adhesion and wettability.

Wheeler, D. R.↗

NASA NTRS1983

A compact hydrogen maser with exceptional long-term stability

A passive hydrogen maser employing a smaller microwave cavity than previous masers is described. The volume of the entire resonator package, including a conventional source, hexapole state selector, and four magnetic shields, is estimated at 20 liters. The techniques for constructing the ceramic cavity, coating it with FEP, and attaching the endcaps to achieve a stable container (to allow its use as a single vacuum system) are described in detail. Frequency stability measurements were made of four such masers, against an NBS-4 cesium primary standard, against each other, and against eight commercial cesium clocks; frequency stability level is reported as 1.7 x 10 to the -12th tau exp -1/2 from 1 to 100,000 sec, and no drift above 1 x 10 to the -15th/day was found. Pressure and temperature effects on frequency stability were found at the 1 x 10 to the -14th level. Noise behavior beyond 200,000 sec is characterized as random walk. The potential use of a compact stable maser as a clock is suggested.

Howe, D. A.↗

NASA NTRS1985

Front-End Program for SYSGEN

SYSGEN, Power Generation System Production costing and Reliability Analysis program, simulates production costs and reliability of electric utility with and without time-dependent generating units. FEPS transforms inputs into proper formats, builds data files and adds Job Control Language necessary to running SYSGEN program.

Carlson, C. R.↗

NASA NTRS1984

Ion-beam-textured and coated surfaces experiment (S1003)

The objective of this LDEF experiment is to measure the effects of exposure to the shuttle launch and near Earth space environments on the optical properties of ion beam textured high absorptance solar thermal control surfaces, the optical and electrical properties of ion beam sputtered conductive solar thermal control surfaces, and the weight loss of ion beam deposited oxide polymer films. The various types of surfaces to be tested include six major categories: (1) ion beam textured surfaces suitable for space solar thermal (solar concentration) application; (2) painted and/or state of the art solar thermal surfaces; (3) ion beam sputtered conductive coatings for thermal and space charge control (e.g., indium-oxide coated metalized FEP Teflon); (4) ion beam sputtered conductive coated solar sail materials for space charge control and cooling through emittance; (5) micrometeoroid sensitive samples whose optical properties change only as a result of micrometeoroid impact; and (6) Kapton coated with oxide polymer films to minimize oxygen degradation at near Earth orbit altitudes.

Mirtich, M. J., Jr.↗

NASA NTRS1985

Mass spectra of neutral particles released during electrical breakdown of thin polymer films

A special type of time-of-flight mass spectrometer triggered from the breakdown event was developed to study the composition of the neutral particle flux released during the electrical breakdown of polymer films problem. Charge is fed onto a metal-backed polymer surface by a movable smooth platinum contact. A slowly increasing potential from a high-impedance source is applied to the contact until breakdown occurs. The breakdown characteristics is made similar to those produced by an electron beam charging system operating at similar potentials. The apparatus showed that intense instantaneous fluxes of neutral particles are released from the sites of breakdown events. For Teflon FEP films of 50 and 75 microns thickness the material released consists almost entirely of fluorocarbon fragments, some of them having masses greater than 350 atomic mass units amu, while the material released from a 50 micron Kapton film consists mainly of light hydrocarbons with masses at or below 44 amu, with additional carbon monoxide and carbon dioxide. The apparatus is modified to allow electron beam charging of the samples.

Kendall, B. R. F.↗

NASA NTRS1985

Electron yields from spacecraft materials

Photoyields and secondary electron emission (SEE) characteristics were determined under UHV conditions for a group of insulating materials used in spacecraft applications. The SEE studies were carried out with a pulsed primary beam while photoyields were obtained with a chopped photon beam from a Kr resonance source with major emission at 123.6 nm. This provides a photon flux close to that of the Lyman alpha in the space environment. Yields per incident photon are obtained relative to those from a freshly evaporated and air oxidized Al surface. Results are presented for Kapton, FEP Teflon, the borosilicate glass covering of a shuttle tile, and spacesuit outer fabric.

Yang, K.↗

NASA NTRS1984

Atomic hydrogen maser measurements with wall surfaces of carbon tetrafluoride

The principal objectives of the Smithsonian Astrophysical Observatory cold maser research programs are given. This work is aimed principally at understanding more about the interaction of hydrogen atoms with wall coatings of fluorinated ethylene propylene (Dupont Teflon FEP-120 co-polymer) and of carbon tetrafluoride (CE4). The principal measured quantity in these experiments is the wall shift of the maser's output frequency. The wall shift per atomic collision was calculated from the measured wall frequency shift. This assumes that the wall surface area is smooth on a molecular scale.

Vessot, R. F. C.↗

NASA NTRS1985

Solar maximum: Solar array degradation

The 5-year in-orbit power degradation of the silicon solar array aboard the Solar Maximum Satellite was evaluated. This was the first spacecraft to use Teflon R FEP as a coverglass adhesive, thus avoiding the necessity of an ultraviolet filter. The peak power tracking mode of the power regulator unit was employed to ensure consistent maximum power comparisons. Telemetry was normalized to account for the effects of illumination intensity, charged particle irradiation dosage, and solar array temperature. Reference conditions of 1.0 solar constant at air mass zero and 301 K (28 C) were used as a basis for normalization. Beginning-of-life array power was 2230 watts. Currently, the array output is 1830 watts. This corresponds to a 16 percent loss in array performance over 5 years. Comparison of Solar Maximum Telemetry and predicted power levels indicate that array output is 2 percent less than predictions based on an annual 1.0 MeV equivalent election fluence of 2.34 x ten to the 13th power square centimeters space environment.

Miller, T.↗

NASA NTRS1985

Protective coatings for atomic oxygen susceptible spacecraft materials - STS-41G results

Sixteen materials consisting of metallizations, silicones, and FEP Teflon were applied as protective coatings to selected spacecraft material surfaces and exposed on STS-41G to the LEO atomic oxygen environment. Evaluations of their protective effectiveness were made through assessing their mass loss/gain characteristics, maintenance of base material optical properties, and imperviousness to atomic oxygen attack. Generally, all coatings provided some degree of protection for the underlying material. In some cases the overcoat appeared to be too thin thereby providing inadequate protection.

Whitaker, A. F.↗

NASA NTRS1986

Mass spectrometric studies of the electrical breakdown of thin polymer films

The composition of the neutral particles released during the electrical breakdown of 50-micron and 75-micron insulating films of the type used on spacecraft exteriors investigated experimentally using a time-of-flight mass spectrometer triggered by the breakdown event. The experimental apparatus is described in detail, and the results are presented in photographs. It is found that the particle flux from Teflon FEP and PFA films comprise mainly fluorocarbon fragments, some with mass 350 amu or greater, but the flux from Kapton oxygen-ion-beam treated Kapton, Tefzel, and Mylar comprises mainly molecules of mass 44 amu or less.

Kendall, B. R. F.↗

NASA NTRS1987

Coating a Hydrogen-Maser Chamber With CF4

Coating of carbon tetrafluoride formed on interior surface of atomic-hydrogen maser by allowing gas to freeze on surface. New coating enables maser to oscillate down to 26 K; most effective previous coating, fluorinated ethylene/polypropylene (FEP) copolymer allowed oscillation down to about 50 K.

Vessot, Robert F. C.↗

NASA NTRS1989

Inflatable-Seal Assembly For Cryogenic Fluids

Connector for cryogenic fluid lines quickly joined or separated, seals tightly, and reduces transfer of heat to fluid. Features redundant sealing rings inflated after joining so they wedge tightly against connector base, preventing leakage. Cylinder of FEP inflatable. Pair of threaded stainless-steel rings - one at each end of cylinder - secure cylinder in quick-disconnect assembly.

Buehler, Kurt↗