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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 217 records · Page 12
All sourcesNASA NTRSDOE OSTI
NASA NTRSDate not supplied

Developmental Hardware Testing Results and Forward Plans for Spacecraft Water Impurity Monitor (SWIM) Organic Water Module (OWM)

We present testing results for developmental hardware of the Spacecraft Water Impurity Monitor (SWIM) Organic Water Module (OWM). SWIM-OWM will monitor spacecraft potable water and system water for trace organic contaminants. The system will detect and identify the specific organic chemical that makes up a given total organic carbon reading. We have built a first development unit (1DU) for SWIM-OWM, which directly injects aqueous water samples and detects chemicals with both a thermal conductivity detector and mass spectrometer sensor. The gas chromatography mass spectrometer (GCMS) system that comprises SWIM-OWM draws on the success of ISS-proven mass spectrometer hardware, and the demonstration of GCMS detection of trace organic contaminants in ISS cabin air. SWIM-OWM benefits from the excellent sensitivity and specificity afforded by GCMS. We have demonstrated detection of a set of chemicals relevant to both crew health and performance as well as system monitoring; these target chemicals range from light, volatile organics such as acetone and ethanol, to heavier, very non-volatile compounds such as dimethyl sulfone and o-phthalaldehyde. Direct aqueous injection was chosen for the general applicability of the technique to clean water sampling and to preclude sample pre-processing, which facilitates an on-line implementation of the SWIM-OWM when deployed in a spacecraft or habitation module. A specific advantage of direct aqueous injection when coupled with appropriate methods is that both the light, volatile organics and heavier non-volatiles can be detected from a single injection, in a single chromatogram. Results from 1DU testing will be discussed, and forward plans will be outlined for continued maturation of SWIM-OWM with the goal of implementing a technology demonstration for the purposes of maturing the engineering design and operations in an environment relevant to NASA’s future goals of exploring and setting up habitation on the Moon and Mars.

Water Monitoring↗
NASA NTRS1997

A Measurement of the Energy Spectra of Cosmic Rays from 20 to 1000 GeV Per Amu

The design features and operational performance from the test flight of the fourth generation of spherical geometry cosmic ray detectors developed at Bristol University (Bristol University Gas Scintillator 4 - BUGS-4) are presented. The flight from Ft. Sumner (NM) in Sept. 1993 was the premier flight of a large (1m radius) spherical drift chamber which also gave gas scintillation and Cerenkov signals. The combinations of this chamber with one gas and two solid Cerenkov radiators lead to a large aperture factor (4.5 m2sr), but low (approximately 3.5 g/sq cm) instrument mass over the energy sensitive range 1 to several hundred GeV/a. Moreover, one simple timing measurement determined the impact parameter which provided a trajectory (path length) correction for all detector elements. This innovative and efficient design will be of interest to experimental groups engaged in studies of energetic charged particles. Although there were technical problems on the flight, which were compounded by the total destruction of BUGS-4 by fire while landing in Oklahoma, there was a period of stable operation during which the instrument was exposed at float altitude (approximately 125,000 ft.) to high energy cosmic rays. We present the performance of the instrument as determined from the analysis of these data and an appraisal of its novel design features. Suggestions for design improvements in a future instrument are made.

Gregory, J. C.↗
NASA NTRS1973

A unique method of leak-rate measurements.

Description of an acceptable method for precision helium leak-rate measurement, for rather large pressurized vessels. Precise leakage rates of gaseous helium were measured by adapting a nominal helium leak detector in such a way that the gas load of the vacuum system plus the test vessel could be handled by the augmented pumping equipment while still being traced through the incorporated mass spectrometer. The vacuum chamber used for this experiment was maintained in 100 ntorr pressure range with a foreline pressure of 4 microns. Although sensitivity of the leak detector was diminished by reason of the larger pumping system, this did not affect the overall result in the capture and measurement of a complete leakage rate.

Ross, D. S.↗
NASA NTRS1985

The development of a high energy cosmic ray detector for Spacelab-2

A large cosmic ray detector aimed at measurements of the energy spectra and of the elemental abundances of cosmic ray nuclei at very high energies, up to several TeV/nucleon was constructed. The instrument is an electronic counter telescope with a geometric factor of 5 sq ster. It accomplishes measurements of the particle energies through the use of gas Cerenkov counters and of transition radiation detectors. The solutions of a number of technological problems that are encountered when developing such instrumentation for Shuttle missions are discussed.

Lheureux, J.↗
NASA NTRS1993

A Hybrid Gas Detector/Phoswich for Hard X-ray Astronomy

A hybrid detector, which combines an optical avalanche chamber with a phoswich, is currently under development. The optical avalanche chamber - a proportional counter designed to give large quantities of light photons during charge multiplication, mounts on the front of the scintillator and gives response at low energies, while the solid scintillator takes over at energies where the gas becomes transparent (greater than 90 keV). Both sections of the hybrid will be read out by a common set of photomultipliers under the phoswich. The addition of the gas section to the phoswich improves the energy resolution of the instrument by a factor of 2.5 at 25 keV and the spatial resolution by a factor of 10 at the same energy. The net result is an instrument with broad band coverage and high sensitivity which will be used for coded aperture imaging on long duration balloon flights.

Ramsey, B. D.↗
NASA NTRS1995

Flow Splitter For Measuring Large Leaks

Flow splitter increases size of leak measured by helium mass-spectrometer leak detector. Multiplies maximum measurable rate of leakage by factor of 1,000. Leaking gas flows into manifold, where small fraction of flow diverted to leak detector. Bulk of flow removed by mechanical vacuum pump.

Hyatt, William S.↗
NASA NTRS1978

Recent developments and applications with gas cell correlation spectrometer

Gaspec, a gas filter correlation spectrometer, is described. Gaspec is a dual-gas three-channel instrument using two detectors which receive amplitude-shared source signals modulated at the frequency of the chopper. Several units for operation around the 3-5 micron and the 8-15 micron region have been constructed, and gases such as CO2, CO, CH4, HCl, NO, and hydrazines can be detected. Advantages of Gaspec are considered with reference to improvements developed for the basic Cospec (gas cell correlation spectrometer) instrument.

Barringer, A. R.↗
NASA NTRS1983

A pyroloysis technique for determining microamounts of hydrogen in lunar soil using the helium ionization detector

A method has been developed which will determine hydrogen in sub-milligram samples of lunar soil. It consists of heating the sample in a pyroprobe followed by the gas chromatographic determination of hydrogen using the helium ionization detector. Using a 7 foot, 1/8 OD stainless steel column packed with Carbosieve S, 120/140 mesh, hydrogen was well-separated from the other gases released from lunar soil. Standards of hydrogen in helium were used for calibration. The limit to detection under the conditions used was about 2 ng. The method was linear from 2 ng to 270 ng. The method was checked using some actual lunar samples. Results were typical of those obtained for lunar soils using other methods.

Bustin, R.↗
NASA NTRS2013

Ultrasonic Detectors Safely Identify Dangerous, Costly Leaks

In 1990, NASA grounded its space shuttle fleet. The reason: leaks detected in the hydrogen fuel systems of the Space Shuttles Atlantis and Columbia. Unless the sources of the leaks could be identified and fixed, the shuttles would not be safe to fly. To help locate the existing leaks and check for others, Kennedy Space Center engineers used portable ultrasonic detectors to scan the fuel systems. As a gas or liquid escapes from a leak, the resulting turbulence creates ultrasonic noise, explains Gary Mohr, president of Elmsford, New York-based UE Systems Inc., a long-time leader in ultrasonic detector technologies. "In lay terms, the leak is like a dog whistle, and the detector is like the dog ear." Because the ultrasound emissions from a leak are highly localized, they can be used not only to identify the presence of a leak but also to help pinpoint a leak s location. The NASA engineers employed UE s detectors to examine the shuttle fuel tanks and solid rocket boosters, but encountered difficulty with the devices limited range-certain areas of the shuttle proved difficult or unsafe to scan up close. To remedy the problem, the engineers created a long-range attachment for the detectors, similar to "a zoom lens on a camera," Mohr says. "If you are on the ground, and the leak is 50 feet away, the detector would now give you the same impression as if you were only 25 feet away." The enhancement also had the effect of reducing background noise, allowing for a clearer, more precise detection of a leak s location.

Source record↗
NASA NTRS1985

Detection threshold energy of high energy cascade showers using thermoluminescence PTFE-sheet and hot-gas reader

A new thermoluminescence (TL) sheet was developed as a detector for high energy components in air showers. For the investigation of detection threshold energy for a cascade showeer, TL sheets were exposed at Mt. Fuji with X ray films in emulsion chambers and were scanned by a hot-gas reader. It is concluded that if a gamma ray whose energy is more than 6 TeV enters vertically into lead chambers, the resulting cascade shower is readily detectable at maximum development.

Kino, S.↗
NASA NTRS2010

Regolith Volatile Characterization (RVC) in RESOLVE

Resource investigation in the lunar poles is of importance to the potential impact of in-situ resource utilization (ISRU). The RESOLVE project developed a payload to investigate the permanently shadowed areas of the lunar poles and demonstrate ISRU technology. As a part of the RESOLVE project, the regolith volatile characterization (RVC) subsystem was designed to examine the release of volatiles from sample cores. The test sample was heated in the reactor to release the volatiles where they were analyzed with gas chromatography. Subsequently, the volatile sample was introduced into the lunar water resource demonstration (LWRD) subsystem where the released hydrogen and water were selectively captured. The objective of the Regolith Volatile Characterization (RVC) subsystem was to heat the crushed core sample and determine the desorption of volatile species of interest. The RVC subsystem encompasses the reactor and the system for volatile analysis. The system was designed to analyze H2, He, CO, CO2, N2, 02, CH4, H2S and H2O. The GC chosen for this work is a Siemens MicroSAM process GC with 3 columns and 8 TCD detectors. Neon was chosen as the carrier gas to enhance the analysis of hydrogen and helium.The limit of detection for the gases is approx.1000ppm for H2, CO. CO2 , N2, O2 and H2 S. The limit of detection for CH4 is approx.4000ppm and the water limit of detection is -10000 ppm with a sample analysis time of 2-3 minutes. These values (with the exception of water and H2S) were determined by dilution of a six gas mixture from Scott Gas (5% CO2, CO, O2, N2, 4% CH4 and H2) using mass flow controllers (MFC5). Water was calibrated at low levels using an in house relative humidity (RH) generator. H 2S and high concentrations of H2 were calibrated by diluting a pure stream of gas with MFCs. Higher concentrations of N2 and 02 were calibrated using Air again diluting with MFCs. There were three modification goals for the GC in EBU2 that would allow this process GC to be used in the field demo for RESOLVE. The first modification was to decrease the weight associated with the GC, this included eliminating the explosion proof case (Figure 1) and replacing it with a lightweight case as well as using an on board COPV tank for the neon carrier gas. The next goal was to add a second oven for the molecular sieve column to allow for dual temperature control during GC operation; the separation of hydrogen and helium is optimum at lower temperatures while the water analysis required higher temperatures creating a competing design requirement. The second oven also allows a lower limit of detection for water quantification and avoids the possibility of water condensing in the GC which could ruin the column characteristics. The final goal was to modify the column arrangement to optimize the system for our specific application. Figure 2 shows the internal details of the module optimized optimized for our field application. The modifications and performance of the gas analysis system will be discussed in detail.

Captain, Janine↗
NASA NTRS1997

Cosmic Ray Induced Degradation in X-Ray Detectors On Board the Near Earth Asteroid Rendezvous Spacecraft

The Near-Earth Asteroid Rendezvous (NEAR) mission is the first in NASA's new Discovery Program to explore the solar system. Launched in February 1996, the NEAR spacecraft will take a long cruise flight arriving at the asteroid 433 Eros in January 1999 for a one year orbiting survey operation. This long exposure to the space environment has already proven to be an additional complication for the x-ray spectrometer. The asteroid pointing detectors for the x-ray spectrometer are three gas-filled proportional counters with resolving power in the range of 1 keV. Therefore, to resolve the important but closely spaced magnesium, aluminum and silicon k alpha lines( 1.255, 1.487, 1.739 keV respectively), magnesium and aluminum balanced filters are used on two of the detectors. The x-ray florescence from the surface of Eros is stimulated by solar x-rays. A proportional counter and a silicon PIN detector are used to monitor the solar incident x-ray flux. The proportional counters are single wire gas filled beryllium lined steel tubes operating at about 1100 volt. The 25 cm(exp 2) optical window is one mil. thick beryllium. To define the detector's active region, two boron nitride disks were incorporated in the tube just outside window area. It appears from the space flight data that the space environment is creating a charge on these boron nitride disks which ultimately distorts the tube gain and resolution. This broadening of the photo peak makes it more difficult to identify weak peaks and so degrades the statistical accuracy for some very important elements such as sulfur, calcium and iron (2.307, 3.690, 6.403 keV respectively). If the broadening is severe enough in the low energy region, counts will be lost as the photo peak spreads below the lower level discriminator (0.7 keV).

Floyd, S. R.↗
NASA NTRS1973

Techniques for the analysis of gases sequentially released from lunar samples

Description of two methods for the analysis of light gases that are sequentially evolved from 2 to 10 mg of lunar sample. A hydrofluoric acid hydrolysis of lunar material is achieved by repeated exposure of the sample to hydrogen fluoride. In the second technique, gases are evolved from lunar samples by the stepwise heating of these samples to 1400 C. The gases evolved by either hydrolysis or pyrolysis are analyzed in a gas chromatographic system using a helium ionization detector. The sensitivities of this detector for the gases, as analyzed, range from 20 picograms/sec for hydrogen to 0.2 picogram/sec for carbon dioxide.

Desmarais, D. J.↗
NASA NTRS1975

Analysis of Aerobee 17.012 data

The results are summarized of reduction and analysis of data acquired during the flight of NASA-Aerobee 17.012CG. This rocket was launched from White Sands Missile Range on 6 April 1974 at 0410 U.T. The primary instrument in the experiment payload was a singly focussing x-ray reflector system sensitive in the range from 0.18 to 3 keV. X-ray detectors for this system consisted of two gas flow proportional counters with fields of view defined by apertures of 0.1 deg and 0.3 deg at the reflector focus. A Bragg spectrometer utilizing KAP crystals was included in the payload with the objective of detecting the Lyman alpha line of 0 VIII at 18.97A in the Puppis supernova remanant. A 35 mm camera photographed the star field every 1.6 sec throughout the flight to provide aspect information.

Catura, R. C.↗
NASA NTRS1976

Chemical Analysis of Outgassing Contaminants on Spacecraft Surfaces

Samples of S-13 paint on aluminum, reflection grating anomalies as affected by dielectric coatings, and rocket effluents were analyzed along with Skylab window scrapings and a gas activated semiconductor. Development of an HCl detector is also discussed. Results are briefly summarized.

Mcnutt, R. C.↗