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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 217 records · Page 12
All sourcesNASA NTRSDOE OSTI
NASA NTRS1993

Giotto Ion Mass Spectrometer Measurements at Comet P/Grigg-Skjellerup

The Giotto Ion Mass Spectrometer High Intensity Spectrometer (IMS-HIS) measured fluxes of ions from about 260,000 km before (10:08:37 UT spacecraft time) to about 86,000 km after (17:01:33 UT spacecraft time) closest approach to comet P/Grigg- Skjellerup during the encounter on July 10, 1992. Although the HIS sensor was not designed to measure protons, the unusual flyby geometry at Grigg-Skjellerup allowed the sensor to detect these ions. Considerable temporal structure appears in the data, well- correlated with the data of other instruments onboard, especially those of the magnetometer. In particular, the proton count rate correlates with the direction of the magnetic field.

Rosenbauer, H.↗
NASA NTRS2014

Performance of the Linear Ion Trap Mass Spectrometer for the Mars Organic Molecule Analyzer (MOMA) Investigation on the 2018 Exomars Rover

The 2018 ExoMars rover mission includes the Mars Organic Molecule Analyzer (MOMA) investigation. MOMA will examine the chemical composition of samples acquired from depths of up to two meters below the martian surface, where organics may be protected from degradation derived from cosmic radiation and/or oxidative chemical reactions. When combined with the complement of instruments in the rover's Pasteur Payload, MOMA has the potential to reveal the presence of a wide range of organics preserved in a variety of mineralogical environments, and to begin to understand the structural character and potential origin of those compounds. The MOMA investigation is led by the Max Planck Institute for Solar System Research (MPS) with the mass spectrometer subsystem provided by NASA GSFC. MOMA's linear ion trap mass spectrometer (ITMS) is designed to analyze molecular composition of: (i) gas evolved from pyrolyzed powder samples and separated in a gas chromatograph; and, (ii) ions directly desorbed from crushed solid samples at Mars ambient pressure, as enabled by a pulsed UV laser system, fast-actuating aperture valve and capillary ion inlet. Breadboard ITMS and associated electronics have been advanced to high end-to-end fidelity in preparation for flight hardware delivery to Germany in 2015.

linear ion trap mass spectrometer↗
NASA NTRS2019

Spacecraft Induced Molecular Return Flux Considerations for Icy Moon Missions Targeting Detection of Organics with Mass Spectrometers

Science missions targeting the detection of organics from jet plumes originating from icy moons (i.e. Europa and Enceladus) will employ next-generation, state-of-the-art mass spectrometers to measure the composition of icy moon plume effluents and exospheres. During fly-bys, as mass spectrometers make their scientific measurements, molecular emissions from the spacecraft can interact with the local exosphere and associated jet plumes from the sub-surface oceans of the icy moons. Spacecraft-induced molecular effluents collide with molecules from the ambient exosphere, and a fraction of the spacecraft emissions are returned to the spacecraft and its complement of science instruments. The rate at which emitted molecules are returned to the spacecraft by collisions with other molecules (e.g. in Europa’s exosphere) is the return flux. The return flux of molecular emission from spacecraft sources is a major contributor to contaminant deposition onto the complement of contamination-sensitive instruments. Characterization of return flux is critical to the definition of requirements for materials outgassing for the spacecraft and its instruments, and for the definition of thruster operations.

Soares, C. E.↗
NASA NTRS1978

A feasibility study of ion implantation techniques for mass spectrometer calibration

An experimental study was undertaken to examine the feasibility of using ion-implanted filaments doped with either an alkali metal or noble gas for in situ recalibration of onboard mass spectrometers during extended space missions. Implants of rubidium and krypton in rhenium ribbon filaments were subsequently tested in a bakeable 60 deg sector mass spectrometer operating in the static mode. Surface ionization and electron impact ion sources were both used, each yielding satisfactory results. The metallic implant with subsequent ionization provided a means of mass scale calibration and determination of system operating parameters, whereas the noble gas thermally desorbed into the system was more suited for partial pressure and sensitivity determinations.

Koslin, M. E.↗
NASA NTRS2014

Recent Advances in Water Analysis with Gas Chromatograph Mass Spectrometers

We report on progress made in developing a water sampling system for detection and analysis of volatile organic compounds in water with a gas chromatograph mass spectrometer (GCMS). Two approaches are described herein. The first approach uses a custom water pre-concentrator for performing trap and purge of VOCs from water. The second approach uses a custom micro-volume, split-splitless injector that is compatible with air and water. These water sampling systems will enable a single GC-based instrument to analyze air and water samples for VOC content. As reduced mass, volume, and power is crucial for long-duration, manned space-exploration, these water sampling systems will demonstrate the ability of a GCMS to monitor both air and water quality of the astronaut environment, thereby reducing the amount of required instrumentation for long duration habitation. Laboratory prototypes of these water sampling systems have been constructed and tested with a quadrupole ion trap mass spectrometer as well as a thermal conductivity detector. Presented herein are details of these water sampling system with preliminary test results.

quadrupole ion trap↗
NASA NTRS1998

Chemical composition measurements of the atmosphere of Jupiter with the Galileo Probe mass spectrometer

The Galileo Probe entered the atmosphere of Jupiter on December 7, 1995. Measurements of the chemical and isotopic composition of the Jovian atmosphere were obtained by the mass spectrometer during the descent over the 0.5 to 21 bar pressure region over a time period of approximately 1 hour. The sampling was either of atmospheric gases directly introduced into the ion source of the mass spectrometer through capillary leaks or of gas, which had been chemically processed to enhance the sensitivity of the measurement to trace species or noble gases. The analysis of this data set continues to be refined based on supporting laboratory studies on an engineering unit. The mixing ratios of the major constituents of the atmosphere hydrogen and helium have been determined as well as mixing ratios or upper limits for several less abundant species including: methane, water, ammonia, ethane, ethylene, propane, hydrogen sulfide, neon, argon, krypton, and xenon. Analysis also suggests the presence of trace levels of other 3 and 4 carbon hydrocarbons, or carbon and nitrogen containing species, phosphine, hydrogen chloride, and of benzene. The data set also allows upper limits to be set for many species of interest which were not detected. Isotope ratios were measured for 3He/4He, D/H, 13C/12C, 20Ne/22Ne, 38Ar/36Ar and for isotopes of both Kr and Xe.

unmanned↗
NASA NTRS1981

The retarding ion mass spectrometer on dynamics Explorer-A

An instrument designed to measure the details of the thermal plasma distribution combines the ion temperature-determining capability of the retarding potential analyzer with the compositional capabilities of the mass spectrometer and adds multiple sensor heads to sample all directions relative to the spacecraft ram directions. The retarding ion mass spectrometer, its operational modes and calibration are described as well as the data reduction plan, and the anticipated results.

Chappell, C. R.↗
NASA NTRS1987

The ion mass spectrometer on Giotto

The design of the Giotto ion mass spectrometer (IMS) system, its calibration, and the initial flight performance are discussed. The IMS system consists of two sensors: one optimized for the outer coma, the other for the inner coma, with each sensor obtaining complementary information in the region for which it was not optimized. Both sensors feature mass-imaging characteristics, permitting simultaneous measurements of several ion species by means of multi-detector arrays, with resultant mass per charge resolution of not less than 20. In addition to mass per charge, the energy per charge and the elevation and azimuth of the incident ions were measured during the Giotto flight.

Balsiger, H.↗
NASA NTRS1983

Development of a mass spectrometer system for the measurement of inert gases in meteorites

The study of the inert gases in meteorites has provided many clues as to the origin and evolution of the solar system. Particularly crucial and complex are the gases krypton and xenon. To accurately measure the isotopic compositions of these gases requires a mass spectrometer of high sensitivity and resolution. A previously unused and largely untested mass spectrometer system was brought to the point where it was ready for routine sample analyses. This involved, among other things, focusing the ion beam for optimal peak shape and sensitivity, documenting the instrument's response to a series of characteristic tests such as multplier gain checks, and interfacing the instrument to a computer to run the sample analyses. Following this testing and setting up, three iron meteorite samples were to be analyzed for argon, krypton, and xenon. The three samples were shown in prior work to possibly contain primordial heavy inert gases. Although these analyses have not yet been carried out, it is anticipated that they will be completed in the near future.

Palma, R. L.↗
NASA NTRS1987

Mass spectrometers and atomic oxygen

The likely role of atmospheric atomic oxygen in the recession of spacecraft surfaces and in the shuttle glow has revived interest in the accurate measurement of atomic oxygen densities in the upper atmosphere. The Air Force Geophysics Laboratory is supplying a quadrupole mass spectrometer for a materials interactions flight experiment being planned by the Johnson Space Center. The mass spectrometer will measure the flux of oxygen on test materials and will also identify the products of surface reactions. The instrument will be calibrated at a new facility for producing high energy beams of atomic oxygen at the Los Alamos National Laboratory. The plans for these calibration experiments are summarized.

Hunton, D. E.↗