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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 217 records · Page 12

Genome-centric view of carbon processing in thawing permafrost

As global temperatures rise, large amounts of carbon sequestered in permafrost are becoming available for microbial degradation. However, accurate prediction of carbon gas emissions produced from thawing permafrost is limited by our understanding of the resident microbial communities and their associated carbon metabolism. Here, metagenomic sequencing of 214 samples from intact, thawing and thawed sites collected over three years enabled the recovery of 1,529 metagenome-assembled genomes (MAGs), including many from phyla with poor genomic representation. These genomes were shown to broadly reflect the diversity of this complex ecosystem with genus-level representatives recovered for >60% of the community, constituting a two orders of magnitude increase in the number of genomes available for understanding carbon processing in this environment. Metabolic reconstruction, supported by metatranscriptomic and metaproteomic data, revealed key populations involved in organic matter degradation, including bacteria encoding a pathway for xylose degradation only previously identified in fungi. Combined analysis of the microbial communities and geochemical data highlighted lineages correlated with the production of greenhouse gases and suggest novel syntrophic relationships. Our findings link changing biogeochemistry to specific microbial lineages involved in each stage of carbon processing, providing key information for predicting the impact of climate change on these systems.

Woodcroft, Ben J.↗

Evaluation of Simple Chemical Interactions in the Defense Waste Processing Facility (DWPF) Chemical Process Cell (CPC) Under the Glycolic Acid Flowsheet

This report describes results from testing developed for the increased understanding of simple chemical interactions relevant to the processing and vitrification of radioactive waste at the Savannah River Site (SRS) in Aiken, SC. This work is outlined in task 3 of the Technical Task Request X-TTR-S-00024, Rev. 0 and task 4 of the Task Technical & Quality Assurance Plan SRNL- RP-2014-01183 Rev. 0. The testing was conducted from May 2016 through February 2017 at the Aiken County Technology Laboratory (ACTL) and performed by Savannah River National Laboratory (SRNL) personnel. This testing involved the investigation of simple reactions and interactions of glycolic or nitric acids with combinations of sodium nitrite, manganese dioxide, mercuric oxide, and noble metals (silver, palladium, rhodium, and ruthenium). The aim of this testing was to better understand the reactions and chemical phenomena previously observed in the Sludge Receipt and Adjustment Tank (SRAT) cycle of the Chemical Process Cell (CPC) in the Defense Waste Processing Facility (DWPF).

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Understanding Part to Part Variability During Directed Energy Deposition Processes Using In Situ and Ex Situ Process Characterization

The overall goal of this technical collaboration is the use of in situ and ex situ characterization techniques to understand part to part variability in Ti-6Al-4V parts fabricated using directed energy deposition (DED) process, and subsequently qualify parts fabricated using AM. The primary goal of the Phase-1 of this CRADA was to demonstrate the feasibility of capturing the above changes using a combination of high speed stereo imaging and in situ monitoring using two wavelength pyrometers. The in situ monitoring was then correlated using ex situ characterization performed using optical microscopy. The results from phase-1 clearly show that changes to the process and shielding gases have a significant impact on the geometric conformity of the build and the build layer height. The results from phase-1 show that in addition to using IR thermography as a tool to measure the temperature and gradients, we could use it to monitor the build topography and the layer height and use the information to develop closed loop control systems. The phase-1 results show that there is a narrow zone under which the process must operate in order to be “passively stable” or autocorrect for over building. In addition, the results demonstrate that when operated within this range the build autocorrects and there is a drastic reduction in the interlayer lack of fusion defect formation.

36 MATERIALS SCIENCE↗

Historical Scaling Performance from Laboratory to Full Scale for The Defense Waste Processing Facility's Chemical Process Cell

The Defense Waste Processing Facility (DWPF) is planning to modify the chemical processing flowsheet by replacing formic acid with glycolic acid in the Chemical Process Cell (CPC) Sludge Receipt and Adjustment Tank (SRAT) and Slurry Mix Evaporator (SME). The replacement of formic acid with glycolic acid virtually eliminates the CPC’s largest flammability hazards, catalytic hydrogen and ammonia.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Adapting LEU-Modified Cintichem Process for Processing Up to 750 Grams of Uranium Targets

Argonne National Laboratory (Argonne) developed a low-enriched uranium (LEU)-modified Cintichem (LMC) process to enable production and purification of fission-produced molybdenum-99 (Mo-99) from LEU foil targets. This separation scheme starts with nitric acid (HNO 3 ) dissolution of irradiated LEU foil targets that yields an approximate final volume of 2 L. The dissolved uranium solution containing fission products, including Mo-99, is then treated by loading the solution on a titania-based recovery column to separate Mo-99 from bulk uranium. After several washing steps, Mo and other fission products are stripped from the titania column using sodium hydroxide (NaOH). The eluate is then acidified using nitric acid and subsequently processed for final purification using the LMC process. Uranium and most fission products are not adsorbed on the titania column but are eluted (i.e., removed using a solvent) during the wash steps; they can be purified and recycled into new uranium targets.

07 ISOTOPE AND RADIATION SOURCES↗

Sparse Data Machine Learning Integration with Theory, Experiment and Uncertainty Quantification: Process-Structure-Property-Performance of Friction Deformation Processing

Computer vision and deep learning tools that advance the ability to establish processing-structure-property-performance (PSPP) relations are presented. The Bayesian binning method for image segmentation enables quantitative analysis of microstructural features in an automated way, while the analysis of shapes and relative orientation of these features reveals local deformation maps indicative of both, material flow and residual stresses due to materials processing. The deep learning method leads to the previous knowledge agnostic mapping of empirically observed microstructural zones in friction stir welding (FSW) process and synthetic microstructure generation capability that is statistically equivalent to experimentally collected data.

97 MATHEMATICS AND COMPUTING↗

Study of random process theory aids digital data processing

Study of techniques for all random process technology, including stationary, nonstationary, and Gaussian bivariate, aids digital data processing. It presents material on digital filtering, correlation function, optimal spectral smoothing, deterministic data processing, and nonstationary spectrum and correlation analyses.

Bordner, G. W.↗

Alsep data processing: How we processed Apollo Lunar Seismic Data

The Apollo lunar seismic station network gathered data continuously at a rate of 3 x 10 to the 8th power bits per day for nearly eight years until the termination in September, 1977. The data were processed and analyzed using a PDP-15 minicomputer. On the average, 1500 long-period seismic events were detected yearly. Automatic event detection and identification schemes proved unsuccessful because of occasional high noise levels and, above all, the risk of overlooking unusual natural events. The processing procedures finally settled on consist of first plotting all the data on a compressed time scale, visually picking events from the plots, transferring event data to separate sets of tapes and performing detailed analyses using the latter. Many problems remain especially for automatically processing extraterrestrial seismic signals.

Latham, G. V.↗

Neutron capture time scale of the s-process, estimated from s-process krypton in a meteorite

A krypton fraction enriched in s-process isotopes was extracted from a mineral fraction of the Murchison C2 chondrite. The (Kr-86)/(Kr-84) ratio is enhanced by 6 standard deviations, showing that significant amounts of Kr-86 were made in the s-process, despite the short, 10.8 yr beta-decay half-life of its precursor, Kr-85. Judging from this sample, the mean neutron capture time in the s-process was on the order of 5-100 yr for nuclei with cross sections of 125 mb.

Matsuda, J.-I.↗

Flat-plate solar array project: Experimental process system development unit for producing semiconductor-grade silicon using the silane-to-silicon process

The engineering design, fabrication, assembly, operation, economic analysis, and process support research and development for an Experimental Process System Development Unit for producing semiconductor-grade silicon using the slane-to-silicon process are reported. The design activity was completed. About 95% of purchased equipment was received. The draft of the operations manual was about 50% complete and the design of the free-space system continued. The system using silicon power transfer, melting, and shotting on a psuedocontinuous basis was demonstrated.

Source record↗

APPLEPIPS /Apple Personal Image Processing System/ - An interactive digital image processing system for the Apple II microcomputer

Recent developments related to microprocessor-based personal computers have made low-cost digital image processing systems a reality. Image analysis systems built around these microcomputers provide color image displays for images as large as 256 by 240 pixels in sixteen colors. Descriptive statistics can be computed for portions of an image, and supervised image classification can be obtained. The systems support Basic, Fortran, Pascal, and assembler language. A description is provided of a system which is representative of the new microprocessor-based image processing systems currently on the market. While small systems may never be truly independent of larger mainframes, because they lack 9-track tape drives, the independent processing power of the microcomputers will help alleviate some of the turn-around time problems associated with image analysis and display on the larger multiuser systems.

Masuoka, E.↗

Flat-plate solar array project: Experimental process system development unit for producing semiconductor-grade silicon using the silane-to-silicon process

The process technology for the manufacture of semiconductor-grade silicon in a large commercial plant by 1986, at a price less than $14 per kilogram of silicon based on 1975 dollars is discussed. The engineering design, installation, checkout, and operation of an Experimental Process System Development unit was discussed. Quality control of scaling-up the process and an economic analysis of product and production costs are discussed.

Source record↗

Reasoning with case histories of process knowledge for efficient process development

The significance of compiling case histories of empirical process knowledge and the role of such histories in improving the efficiency of manufacturing process development is discussed in this paper. Methods of representing important investigations as cases and using the information from such cases to eliminate redundancy of empirical investigations in analogous process development situations are also discussed. A system is proposed that uses such methods to capture the problem-solving framework of the application domain. A conceptual design of the system is presented and discussed.

Bharwani, Seraj S.↗

Innovative techniques for the production of energetic radicals for lunar processing including cold plasma processing of local planetary ores

Hydrogen reduction of ilmenite has been studied by a number of investigators as a potential means for recovery of oxygen from lunar soil. Interest in this process has always rested with the simplicity of the flow diagram and the utilization of established technology. Effective utilization of hydrogen in the reduction process at temperatures of 1200 C and below has always been disappointing and, as such, has led other investigators to focus attention on other systems. Effective utilization of hydrogen in the reduction of ilmenite can be significantly enhanced in the presence of a non-equilibrium hydrogen plasma. Ilmenite at solid specimen temperatures of 600 C to 970 C were reacted in a hydrogen plasma. Those experiments revealed that hydrogen utilization can be significantly enhanced. At a specimen temperature of 850 C the fraction of H2 reacted was 24 percent compared to the 7 percent theoretical limit calculated with thermodynamic theory for the same temperature. An added advantage for a hydrogen plasma involves further reduction of TiO2. Reduction of the iron oxide in ilmenite yields TiO2 and metallic iron as by products. Titanium forms a number of oxides including TiO, Ti2O3, Ti3O5 and the Magneli oxides (Ti4O7 to Ti50O99). In conventional processing of ilmenite with hydrogen it is possible to reduce TiO2 to Ti7O13 within approximately an hour, but with poor utilization of hydrogen on the order of one mole of H2 per thousand. In the cold or non-equilibrium plasma TiO2 can be rapidly reduced to Ti2O3 with hydrogen utilization exceeding 10 percent. Based on design considerations of the plasma reactor greater utilization of the hydrogen in the reduction of TiO2 is possible.

Bullard, D.↗

The alpha-process and the r-process

The paper explores the alpha-rich freeze-out for values of neutron excesses larger than previously treated, and reports the discovery of nuclear systematics that, for neutron excesses greater than about 0.05, allow the creation of heavier elements all the way up to A of about 100, even when most of the ejecta is in the form of heavy elements. It is found that a large part of the nuclear flow in the r-process may be carried by charged particle reactions up to about A of about 100. It is speculated that the site of these processes is the high-entropy 'wind' of a young neutron star in which neutrino energy deposition is driving mass loss. The pass of r-process ejected per supernova is expected to be about 0.0001 solar mass per Type II or Ib supernova, but this is sensitive to details of the presupernova structure, the explosion mechanism, and the amount of material that falls back onto the neutron star when the reverse shock arrives there.

Woosley, S. E.↗

Using experimental design modules for process characterization in manufacturing/materials processes laboratories

Modules dealing with statistical experimental design (SED), process modeling and improvement, and response surface methods have been developed and tested in two laboratory courses. One course was a manufacturing processes course in Mechanical Engineering and the other course was a materials processing course in Materials Science and Engineering. Each module is used as an 'experiment' in the course with the intent that subsequent course experiments will use SED methods for analysis and interpretation of data. Evaluation of the modules' effectiveness has been done by both survey questionnaires and inclusion of the module methodology in course examination questions. Results of the evaluation have been very positive. Those evaluation results and details of the modules' content and implementation are presented. The modules represent an important component for updating laboratory instruction and to provide training in quality for improved engineering practice.

Ankenman, Bruce↗

Generic Health Management: A System Engineering Process Handbook Overview and Process

Health Management, a System Engineering Process, is one of those processes-techniques-and-technologies used to define, design, analyze, build, verify, and operate a system from the viewpoint of preventing, or minimizing, the effects of failure or degradation. It supports all ground and flight elements during manufacturing, refurbishment, integration, and operation through combined use of hardware, software, and personnel. This document will integrate Health Management Processes (six phases) into five phases in such a manner that it is never a stand alone task/effort which separately defines independent work functions.

Wilson, Moses Lee↗