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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 217 records · Page 12

Control of volume resistivity in inorganic organic separators

Control of resistivity in NASA inorganic-organic separators is achieved by incorporating small percentages of high surface area, fine particle silica with other ingredients in the separator coating. The volume resistivity is predictable from the surface area of filler particles in the coating. The approach is applied to two polymer- plasticizer -filler coating systems, where the filler content of each is below the generally acknowledged critical pigment volume concentration of the coating. Application of these coating systems to 0.0254 cm thick (10-mil) fuel cell grade asbestos sheet produces inexpensive, flexible, microporous separators that perform as well as the original inorganic-organic concept, the Astropower separator.

Sheibley, D. W.↗

Cosmic rays in the Galaxy.

Galactic cosmic rays, discussing chemical composition, isotopic separation, proton and alpha particles energy spectra, propagation, interactions, etc

Meyer, P.↗

Technology utilization program report

The application of aerospace technology to the solution of public health and industrial problems is reported. Data cover: (1) development of an externally rechargeable cardiac pacemaker, (2) utilization of ferrofluids-colloidal suspensions of ferrite particles - in the efficient separation of nonferrous metals as Ni, Zn, Cu, and Al from shredded automobile scrap, and (3) development of a breathing system for fire fighters.

Source record↗

Application of optical fibers to wide-band differential interferometry

A broadband differential optical interferometer that uses an optical-fiber waveguide to transmit coherent light to a surface under inspection is discussed. Input laser light is coupled into two single-mode optical fibers in a stationary input optics enclosure. The fibers transmit the light to a small, remote detection head where it is used in a wide-band differential interferometer to detect continuous and pulsed surface-particle displacements. The effective separation between the input optics and the detection head allows simple surface scanning and probe alignment. Detection of simulated acoustic emission pulses by a prototype test unit is reported.

Garg, A. O.↗

Evaluation of the Separability of Monodisperse Polystyrene Latex Microspheres in a Continuous Flow Electrophoresis System

The continuous flow electrophoresis system makes electrophoresis possible in a free flowing film of aqueous electrolyte medium. The sample is introduced at one end of the chamber and is subjected to a lateral dc field. This process separates the sample into fractions since each component has a distinctive electrophoric mobility. Evaluations were made of sample conductivity and buffer conductivity as they affect sample band spread and separation using the Continuous Particle Electrophoresis (CPE) system. Samples were prepared from mixtures of 5 percent and 1 percent polystyrene latex (PSL) microspheres which were .4, .56 and .7 microns in diameter. These were prepared in electrolyte media 1x and 3x the conductivity of the curtain buffer, approximately 150 and 450 micro mhos/cm. Samples with matched conductivities produced greater resolution and less band spread than those with 3x the conductivity of the curtain buffer.

Williams, G., Jr.↗

Numerical simulation of the tip vortex off a low-aspect-ratio wing at transonic speed

The viscous transonic flow around a low-aspect-ratio wing has been computed using an implicit, three-dimensional, 'thin-layer' Navier-Stokes solver. The grid around the geometry of interest is obtained numerically as a solution to a Dirichlet problem for the cube. The geometry chosen for this study is a low-aspect-ratio wing with large sweep, twist, taper, and camber. The topology chosen to wrap the mesh around the wing with good tip resolution is a C-O type mesh. Using this grid, the flow around the wing was computed for a free-stream Mach number of 0.82 at an angle of attack of 5 deg. At this Mach number, an oblique shock forms on the upper surface of the wing, and a tip vortex and three-dimensional flow separation off the wing surface are observed. Particle path lines indicate that the three-dimensional flow separation on the wing surface is part of the roots of the tip-vortex formation. The lifting of the tip vortex before the wing trailing edge is clearly observed by following the trajectory of particles released around the wing tip.

Mansour, N. N.↗

Density gradient electrophoresis of cultured human embryonic kidney cells

Ground based confirmation of the electrophoretic heterogeneity of human embryonic kidney cell cultures, the general characterization of their electrophoretic migration, and observations on the general properties of cultures derived from electrophoretic subpopulations were studied. Cell migration in a density gradient electrophoresis column and cell electrophoretic mobility was determined. The mobility and heterogeneity of cultured human embryonic kidney cells with those of fixed rat erythrocytes as model test particle was compared. Electrophoretically separated cell subpopulations with respect to size, viability, and culture characteristics were examined.

Plank, L. D.↗

GAS 450: A space payload for the People Central Coast Student Experimenters

The Get Away Special 450 is described. This discussion includes the peoples efforts, the experiments, lessons learned, and a few powerful positive steps toward community involvement. The following is a list of experiment titles: Guppies in Space; Electrophoresis of Enzymes in Microgravity; Diffusion of Ions in Solution; Space Cement; Bubbles in Space; Small Particle Studies; and Liquid Separation in Microgravity.

Ray, Glen↗

Granular instability in fluidized beds: A small-over-large instability

For different particle diameters arranged in a gas fluidized bed, a new gravitational instability is predicted. The first order stability analysis yields conditions for growth of the most unstable wavenumber both as a function of particle diameter and dimensionless Bond number. Gravity acts to distribute the greater fluid mass associated with smaller particles, while surface tension stabilizes the entire bed against accelerations. The phenomenon, called the 'Small-over-Large' (SL) instability, evolves somewhat akin to a Rayleigh-Taylor mechanism and in addition to fundamental interest, carries implications for predicting solute redistribution and gravitational alignments in particle beds and chemical separation columns.

Noever, David A.↗

Containerless processing of undercooled melts

The investigation focused on the control of microstructural evolution in Mn-Al, Fe-Ni, Ni-V, and Au-Pb-Sb alloys through the high undercooling levels provided by containerless processing, and provided fundamental new information on the control of nucleation. Solidification analysis was conducted by means of thermal analysis, x-ray diffraction, and metallographic characterization on samples processed in a laboratory scale drop tube system. The Mn-Al alloy system offers a useful model system with the capability of phase separation on an individual particle basis, thus permitting a more complete understanding of the operative kinetics and the key containerless processing variables. This system provided the opportunity of analyzing the nucleation rate as a function of processing conditions and allowed for the quantitative assessment of the relevant processing parameters. These factors are essential in the development of a containerless processing model which has a predictive capability. Similarly, Ni-V is a model system that was used to study duplex partitionless solidification, which is a structure possible only in high under cooling solidification processes. Nucleation kinetics for the competing bcc and fcc phases were studied to determine how this structure can develop and the conditions under which it may occur. The Fe-Ni alloy system was studied to identify microstructural transitions with controlled variations in sample size and composition during containerless solidification. This work was forwarded to develop a microstructure map which delineates regimes of structural evolution and provides a unified analysis of experimental observations. The Au-Pb-Sb system was investigated to characterize the thermodynamic properties of the undercooled liquid phase and to characterize the glass transition under a variety of processing conditions. By analyzing key containerless processing parameters in a ground based drop tube study, a carefully designed flight experiment may be planned to utilize the extended duration microgravity conditions of orbiting spacecraft.

Perepezko, J. H.↗

An Initial Analysis of the Pixel-Level Uncertainties in Global MODIS Cloud Optical Thickness and Effective Particle Size Retrievals

Moderate Resolution Imaging Spectroradiometer (MODIS) retrievals of cloud optical thickness and effective particle radius employ well-known solar reflectance techniques using pre-calculated reflectance look-up tables. We evaluate the quantitative uncertainty in simultaneous retrievals of cloud optical thickness and particle size for this type of algorithm. The technique uses sensitivity calculations derived from the reflectance look-up tables, coupled with estimates for the effect of various error terms on the uncertainty in inferring the actual cloud-top reflectance. The error terms include the effects of instrument calibration, surface spectral albedo, and atmospheric corrections on both water and ice cloud retrievals. Because particle shapes in ice clouds are highly variable, the effect of particle shape is analyzed separately with a more approximate method. Results will deal exclusively with pixel-level uncertainties associated with plane-parallel clouds; real-world radiative departures from a plane-parallel model are an additional consideration. While we demonstrate the uncertainty technique with operational 1 km MODIS retrievals from the Terra and Aqua satellite platforms, the technique is applicable to any reflectance-based satellite- or air-borne sensor retrieval using similar spectral channels.

Platnick, S.↗

Cloud-to-Ground Lightning Estimates Derived from SSMI Microwave Remote Sensing and NLDN

Lightning observations are collected using ground-based and satellite-based sensors. The National Lightning Detection Network (NLDN) in the United States uses multiple ground sensors to triangulate the electromagnetic signals created when lightning strikes the Earth's surface. Satellite-based lightning observations have been made from 1998 to present using the Lightning Imaging Sensor (LIS) on the NASA Tropical Rainfall Measuring Mission (TRMM) satellite, and from 1995 to 2000 using the Optical Transient Detector (OTD) on the Microlab-1 satellite. Both LIS and OTD are staring imagers that detect lightning as momentary changes in an optical scene. Passive microwave remote sensing (85 and 37 GHz brightness temperatures) from the TRMM Microwave Imager (TMI) has also been used to quantify characteristics of thunderstorms related to lightning. Each lightning detection system has fundamental limitations. TRMM satellite coverage is limited to the tropics and subtropics between 38 deg N and 38 deg S, so lightning at the higher latitudes of the northern and southern hemispheres is not observed. The detection efficiency of NLDN sensors exceeds 95%, but the sensors are only located in the USA. Even if data from other ground-based lightning sensors (World Wide Lightning Location Network, the European Cooperation for Lightning Detection, and Canadian Lightning Detection Network) were combined with TRMM and NLDN, there would be enormous spatial gaps in present-day coverage of lightning. In addition, a globally-complete time history of observed lightning activity is currently not available either, with network coverage and detection efficiencies varying through the years. Previous research using the TRMM LIS and Microwave Imager (TMI) showed that there is a statistically significant correlation between lightning flash rates and passive microwave brightness temperatures. The physical basis for this correlation emerges because lightning in a thunderstorm occurs where ice is first present in the cloud and electric charge separation occurs. These ice particles efficiently scatter the microwave radiation at the 85 and 37 GHz frequencies, thus leading to large brightness temperature depressions. Lightning flash rate is related to the total amount of ice passing through the convective updraft regions of thunderstorms. Confirmation of this relationship using TRMM LIS and TMI data, however, remains constrained to TRMM observational limits of the tropics and subtropics. Satellites from the Defense Meteorology Satellite Program (DMSP) have global coverage and are equipped with passive microwave imagers that, like TMI, observe brightness temperatures at 85 and 37 GHz. Unlike the TRMM satellite, however, DMSP satellites do not have a lightning sensor, and the DMSP microwave data has never been used to derive global lightning. In this presentation, a relationship between DMSP Special Sensor Microwave Imager (SSMI) data and ground-based cloud-to-ground (CG) lightning data from NLDN is investigated to derive a spatially complete time history of CG lightning for the USA study area. This relationship is analogous to the established using TRMM LIS and TMI data. NLDN has the most spatially and temporally complete CG lightning data for the USA, and therefore provides the best opportunity to find geospatially coincident observations with SSMI sensors. The strongest thunderstorms generally have minimum 85 GHz Polarized Corrected brightness Temperatures (PCT) less than 150 K. Archived radar data was used to resolve the spatial extent of the individual storms. NLDN data for that storm spatial extent defined by radar data was used to calculate the CG flash rate for the storm. Similar to results using TRMM sensors, a linear model best explained the relationship between storm-specific CG flash rates and minimum 85 GHz PCT. However, the results in this study apply only to CG lightning. To extend the results to weaker storms, the probability of CG lightning (instead of the flash rate) was calculated for storms having 85 GHz PCT greater than 150 K. NLDN data was used to determine if a CG strike occurred for a storm. This probability of CG lightning was plotted as a function of minimum 85 GHz PCT and minimum 37 GHz PCT. These probabilities were used in conjunction with the linear model to estimate the CG flash rate for weaker storms with minimum 85 GHz PCTs greater than 150 K. Results from the investigation of CG lightning and passive microwave radiation signals agree with the previous research investigating total lightning and brightness temperature. Future work will take the established relationships and apply them to the decades of available DMSP data for the USA to derive a map of CG lightning flash rates. Validation of this method and uncertainty analysis will be done by comparing the derived maps of CG lightning flash rates against existing NLDN maps of CG lightning flash rates.

Winesett, Thomas↗

Coordinated Analysis 101: A Joint Training Session Sponsored by LPI and ARES/JSC

The Lunar and Planetary Institute (LPI) and the Astromaterials Research and Exploration Science (ARES) Division, part of the Exploration Integration and Science Directorate at NASA Johnson Space Center (JSC), co-sponsored a training session in November 2016 for four early-career scientists in the techniques of coordinated analysis. Coordinated analysis refers to the approach of systematically performing high-resolution and -precision analytical studies on astromaterials, particularly the very small particles typical of recent and near-future sample return missions such as Stardust, Hayabusa, Hayabusa2, and OSIRIS-REx. A series of successive analytical steps is chosen to be performed on the same particle, as opposed to separate subsections of a sample, in such a way that the initial steps do not compromise the results from later steps in the sequence. The data from the entire series can then be integrated for these individual specimens, revealing important in-sights obtainable no other way. ARES/JSC scientists have played a leading role in the development and application of this approach for many years. Because the coming years will bring new sample collections from these and other planned NASA and international exploration missions, it is timely to begin disseminating specialized techniques for the study of small and precious astromaterial samples. As part of the Cooperative Agreement between NASA and the LPI, this training workshop was intended as the first in a series of similar training exercises that the two organizations will jointly sponsor in the coming years. These workshops will span the range of analytical capabilities and sample types available at ARES/JSC in the Astromaterials Research and Astro-materials Acquisition and Curation Offices. Here we summarize the activities and participants in this initial training.

Draper, D. S.↗

Electric Field Generation in Martian Dust Devils

Terrestrial dust devils are known to generate electric fields from the vertical separation of charged dust particles. The particles present within the dust devils on Mars may also be subject to similar charging processes and so likely contribute to electric field generation there as well. However, to date, no Marsin situ instrumentation has been deployed to measure electric field strength. In order to explore the electric environment of dust devils on Mars, the triboelectric dust charging physics from the MacroscopicTriboelectric Simulation (MTS) code has been coupled to the Mars Regional Atmospheric ModelingSystem (MRAMS). Using this model, we examine how macroscopic electric fields are generated within martian dust disturbances and attempt to quantify the time evolution of the electrodynamical system.Electric fields peak for several minutes within the dust devil simulations. The magnitude of the electric field is a strong function of the size of the particles present, the average charge on the particles and the number of particles lifted. Varying these parameters results in peak electric fields between tens of millivolts per meter and tens of kilovolts per meter.

Aeolian processes↗

Engineered Interfaces in Extruded Polyphenylsulfone- Boron Nitride Composite Insulation

Improving matrix-filler interactions is critical for optimizing dielectric performance in composite insulation; however, the technique used to an introduce inorganic filler into organic matrices varies in its ability to satisfactorily reduce the size of cavities and interfaces. This study reports how sample rheology influenced the dielectric performance and thermal conductivity of extruded polyphenylsulfone (PPSU) – hexagonal boron nitride (BN) composite insulation through changing the BN incorporation strategy. Depending on the technique used to introduce BN into the host matrix, the low melt viscosity, torque, and melt viscosity temperature of the polymer were reduced, enabling better mixing, heat transfer, and smaller voids. This corresponded to an increase in dielectric strength compared to other formulations; however, the thermal conductivity shifted further away from the thermal conductivity target of 1 W/m·K target, which was an indication of a larger separation distance between the particles in samples with smaller interfaces. A trade-off between dielectric strength and thermal conductivity may exist when maximizing thermal conduction without sacrificing dielectric strength.

polyphenylsulfone↗

Engineered Interfaces in Extruded Polyphenylsulfone-Boron Nitride Composite Insulation

Improving matrix-filler interactions is critical for optimizing dielectric performance in composite insulation; however, the technique used to introduce inorganic fillers into an organic matrix varies in its ability to satisfactorily reduce the size of cavities and interfaces. This study reports effects from changing the filler incorporation strategy on the rheology, dielectric performance and thermal conductivity of extruded polyphenylsulfone (PPSU) – hexagonal boron nitride (hBN) composite insulation. Depending on the technique used to introduce BN into the host matrix, the viscosity, torque, and melt viscosity temperature of the polymer were reduced, enabling better mixing, heat transfer, and smaller voids. This corresponded to an increase in dielectric strength compared to other formulations at either a similar or lower filler loading. On the other hand, the thermal conductivity in these specimens shifted further away from the thermal conductivity target of 1 W/m·K, which was an indication of a larger separation distance between the particles in samples with smaller interfaces. A trade-off between dielectric strength and thermal conductivity may exist when maximizing thermal conduction without sacrificing dielectric strength.

Polyphenylsulfone↗

Immunomicrospheres - Reagents for cell labeling and separation

Immunomicrospheres are specially designed microscopic particles that have antibodies or similar molecules chemically bound to their surfaces. The antibody-coated microspheres react in a highly specific way with target cells, viruses, or other antigenic agents. Immunomicrospheres may be synthesized so that they incorporate compounds that are highly radioactive, intensely fluorescent, magnetic, electron opaque, highly colored, or pharmacologically active. These various types of microspheres may be coated with pure, highly specific monoclonal antibodies obtained by the new hybridoma cell cloning techniques or with conventional antibody preparations. Some of the many present and potential applications for these new reagents are (1) new types of radioimmune or immunofluorescent assays, (2) improved fluorescence microscopy, (3) separation of cells on the basis of the fluorescent, electrophoretic, or magnetic properties of bound immunomicrospheres, (4) markers for use in several types of electron or standard light microscopy, and (5) delivery of lethal compouds to specific undesirable living cells. The combination of the various new types of synthetic microspheres and the newly available homogeneous antibodies offers new opportunities in research, diagnosis, and therapy.

Rembaum, A.↗

Fracto-emission - The role of charge separation

Fracto-emission is the emission of particles (e.g., electrons, ions, ground state and excited neutrals, and photons) during and following fracture. It is found that during fracture in vacuum of adhesive bonds and crystalline materials involving large amounts of charge separation on the surface the emission of charged particles, excited neutrals, light, and radio waves occurs with unique and revealing time dependencies. Simultaneous fracto-emission measurements on several systems are reported. The results are interpreted in terms of a conceptual model involving the following steps: (1) charge separation due to fracture, (2) desorption of gases from the material into the crack tip, (3) a gas discharge in the crack, (4) energetic bombardment of the freshly created crack walls, and (5) thermally stimulated electron emission, accompanied by electron stimulated desorption of ions and excited neutrals. In addition to evidence from fracture experiments, results from studies of electron bombardment of a polymer surface are presented.

Dickinson, J. T.↗