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Hanford Waste Treatment Plant Low Activity Waste Facility Stack Effluent Monitoring - Sampling Probe Location Qualification Evaluation

The Hanford Tank Waste Treatment and Immobilization Plant low activity waste (LAW) facility stack monitor locations were qualified using scale model stacks to mitigate the risk of identifying that sampling locations do not meet the qualification criteria on the full-scale stack. As required by the American National Standards Institute/Health Physics Society (ANSI/HPS) N13.1-1999 standard, the scale model and its sampling location were geometrically similar to the actual stack and the Reynolds numbers for both the actual and model stacks were >10,000. An additional criterion is that the product of the hydraulic diameter and mean velocity (DV) of the full-scale stack must be between 1/6 DV and 6 DV of the scale model stack tests. Verification tests of the LAW stacks were performed at normal operating conditions. The minimum 1/6 DV value, along with the maximum 6 DV value from the scale model testing determines the range of conditions for which the full-scale stack may be operated and remain in compliance with the stack verification criterion. Based on these DV values, the corresponding stack flow rates for each of the LAW stacks are 815–55,758 scfm for LV-S1, 980–112,078 scfm for LV-S2, 264–22,901 scfm for LV-S3, and 981–79,832 scfm for LV-C2. The remaining criteria for the stack verification to be considered valid involve the flow angle and velocity uniformity results. First, the flow angle at the full-scale stack must be =20°. Second, the velocity uniformity at the full-scale stack must be =20% coefficient of variance (COV). Finally, the velocity uniformity results for the actual and scale model stack tests must agree within 5% COV. These criteria were met through the full-scale stack tests at the LAW facility. Flow angle results were primarily less than 10°, except for one LV-S2 Fan A result, which was 13.2°; all flow angle results were within the =20° criterion. The velocity uniformity results for each test condition ranged between 1.5 COV and 9.2% COV, which were all within the range of the target % COV values from the scale model tests. Based on these stack verification test results, the four LAW filtered exhaust stack sampling locations meet the qualification criteria provided in the ANSI/HPS N13.1-1999 standard for all fan operating configurations. This includes single-fan operating conditions for LV-S1 and LV-S2, dual-fan operations for LV-S3 at both the continuous air monitor and record sampler locations, and both the single-fan as well as the dual-fan operations for LV-C2. Further changes to the system configuration or operating conditions that are outside the bounds described in this report may require additional tests or analyses to determine compliance with the standard.

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Summary of Savannah River Site FY21 Salt Waste Qualification Data and Characterization Data from Salt Waste Batches Processed Since 2008

The Savannah River National Laboratory analyzed samples from Savannah River Site Waste Tank 41H and 21H to support qualification of Salt Waste Processing Facility Waste Batches 3 and 4 (the FY21 Salt Batch Qualification samples) for processing. Neither of the samples displayed any unusual or unexpected characteristics such as large amounts of solids, floating solids, or unusual color. Characterization of these samples confirmed similar chemical composition and characteristics to previous salt waste batches. These results were initially provided to Savannah River Remediation (Liquid Waste Operations Sub-contractor) as External Sample Results LIMS Reports. The analytical results (both expedited and routine) are now summarized and discussed in this technical report.

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Updated Liquid Secondary Waste Grout Formulation and Preliminary Waste Form Qualification

This report describes the results from liquid secondary waste grout (LSWG) formulation and cementitious waste form qualification tests performed by Pacific Northwest National Laboratory (PNNL) for Washington River Protection Solutions, LLC (WRPS). New formulations for preparing a cementitious waste form from a high-sulfate liquid secondary waste stream simulant, developed for Effluent Management Facility (EMF) process condensates merged with low activity waste (LAW) caustic scrubber, and the release of key constituents (e.g. 99Tc and 129I) from these monoliths were evaluated. This work supports a technology development program to address the technology needs for Hanford Site Effluent Treatment Facility (ETF) liquid secondary waste (LSW) solidification and supports future Direct Feed Low-Activity Waste (DFLAW) operations. High-priority activities included simulant development, LSWG formulation, and waste form qualification. The work contained within this report relates to waste form development and testing and does not directly support the 2017 integrated disposal facility (IDF) performance assessment (PA). However, this work contains valuable information for use in PA maintenance past FY17, and for future waste form development efforts. The provided data should be used by (i) cementitious waste form scientists to further understanding of cementitious dissolution behavior, (ii) IDF PA modelers who use quantified constituent leachability, effective diffusivity, and partitioning coefficients to advance PA modeling efforts, and (iii) the U.S. Department of Energy (DOE) contractors and decision makers as they assess the IDF PA program. The results obtained help fill existing data gaps, support final selection of a LSWG waste form, and improve the technical defensibility of long-term waste form performance estimates.

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Summary of Savannah River Site FY22 Salt Waste Qualification Data

The Savannah River National Laboratory analyzed samples from Savannah River Site Waste Tank 41H, 21H and 42H to support qualification of Salt Waste Processing Facility (SWPF) Waste Batches 5, 6, and 7 for processing (the FY22 Salt Batch Qualification samples). None of the samples displayed any unusual or unexpected characteristics such as large amounts of solids, floating solids, or unusual color. Characterization of these samples confirmed similar chemical composition and characteristics to previous salt waste batches. These results were initially provided to Savannah River Mission Completion (Liquid Waste Operations subcontractor) as External Sample Results LIMS Reports and the Tank 41H (Salt Batch 5 sample) was also summarized in two separate technical reports. The analytical results (both rapid and long term) are now summarized and discussed in this technical report.

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Analytical Results of the Tank 51H Sludge Batch 11 As-Received Qualification Sample

Savannah River National Laboratory (SRNL) has been requested by Savannah River Mission Completion (SRMC) to qualify the next sludge batch, Sludge Batch 11 (SB11), for processing at the Defense Waste Processing Facility (DWPF). This report documents the first steps of the qualification process, characterization of the Tank 51H as-received qualification material. SRMC sent SRNL two 200 mL samples received from Tank 51H on the 12th of August 2024. The combined sample, HTF-51-24-85/86, was analyzed for the following: supernate and slurry density, weight percent solids, settling, chemical composition, and radionuclides.

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Summary of Savannah River Site FY23 Salt Waste Qualification Data

The Savannah River National Laboratory (SRNL) analyzed samples from Savannah River Site (SRS) Waste Tanks 41H and 21H to support qualification of Salt Waste Processing Facility (SWPF) Waste Batches 8 and 9 for processing (the FY23 Salt Batch Qualification samples). These Tanks (i.e. 41H and 21H) are blend tanks for feed to SWPF. None of the samples displayed any unusual or unexpected characteristics such as large amounts of solids, floating solids, or unusual color. Characterization of these samples confirmed similar chemical composition and characteristics to previous salt waste batches. The results for Batches 8 and 9 were provided by SRNL to Savannah River Mission Completion (SRMC), the Liquid Waste Operations subcontractor at SRS, as External Sample Results (Laboratory Information Management System (LIMS)) Reports. Additionally, a separate technical memo was issued by SRNL to report re-test data for Batch 8 for Cs-137 for filtered samples only which were run at the request of SWPF. For Batch 9, a set of samples was also analyzed in parallel by the SWPF-Analytical Laboratory (SWPF-AL). The SWPF-AL data is included herein for comparison with the SRNL data where applicable. The analytical results (both rapid, typically 4 weeks, and long term, typically 8 weeks) for Batches 8 and 9 are now summarized and discussed in this technical report.

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Thermal Performance of Neutron Sensor Qualification Device

The neutron sensor qualification device was developed to provide a temperature-controlled environment for neutron sensors and dosimetry, enabling irradiation in a neutron field at the Armed Forces Radiobiology Research Institute (AFRRI) TRIGA reactor facility. The device, constructed from low-activation and low neutron cross-section materials, features a modular tube furnace design with three independently controlled heating zones for controlling axial temperature distribution. Laboratory testing validated the device's thermal performance, including uniform temperature distribution with less than 6°C variation across the central region, a steady-state operational temperature of 350°C achieved in approximately 3 hours, and a cooling time constant of 3.5 hours. External surface temperatures remained safe for handling, with the surrounding aluminum structure remaining at ambient conditions. The results confirm the device’s suitability for neutron sensor qualification experiments, with potential for future operation at higher temperatures and further optimization of performance.

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Techniques for control of long-term reliability of complex integrated circuits. I - Reliability assurance by test vehicle qualification.

Development of an alternate approach to the conventional methods of reliability assurance for large-scale integrated circuits. The product treated is a large-scale T squared L array designed for space applications. The concept used is that of qualification of product by evaluation of the basic processing used in fabricating the product, providing an insight into its potential reliability. Test vehicles are described which enable evaluation of device characteristics, surface condition, and various parameters of the two-level metallization system used. Evaluation of these test vehicles is performed on a lot qualification basis, with the lot consisting of one wafer. Assembled test vehicles are evaluated by high temperature stress at 300 C for short time durations. Stressing at these temperatures provides a rapid method of evaluation and permits a go/no go decision to be made on the wafer lot in a timely fashion.

Van Vonno, N. W.↗

Qualification plan for the ultraviolet spectrometer experiment (S-169), revision A

The qualification methods used to verify that the UVS hardware meets the technical requirements of the contract are defined. Included in this plan are test location, the qualification UVS to be tested, test objectives, and all tests required to verify that the UVS meets all performance and environmental requirements of the CEI specification. Additionally, environmental test conditions, testing time or cycles, allowable maintenance, logging requirements, manner of analysis, and utilization of test results, disposition of test specimens, failure criteria, retest requirements, facilities and support requirements, and the time phasing of the tests are presented.

Eckard, L. D., Jr.↗

Flight qualification of mortar-actuated parachute deployment systems

A brief discussion outlines background of mortar use in parachute deployment systems. A description of the system operation is presented. Effects of the environment on performance are discussed as well as the instrumentation needed to assess this performance. Power unit qualification and lot qualification for shear pins and cartridges is delineated. Functional mortar system tests are described. Finally, bridle deployment and parachute deployment are discussed.

Pleasants, J. E.↗

Environmental qualification testing of terrestrial solar cell modules

The placement of solar cell modules in various climates and locations throughout the world results in different degrees and combinations of environmental stresses. Coupled with a design lifetime goal of 20 years, early detection and correction of module design deficiencies can result in significantly better long-term economics. This paper describes an environmental test research program for developing qualification requirements and procedures for flat-plate solar cell modules. A multiple iterative approach for establishing and evaluating test requirements is discussed as well as the rationale for the selection of levels and durations for the current qualification tests. The status of study efforts involving optical surface soiling, encapsulation delamination, and voltage bias-humidity testing is reviewed.

Hoffman, A. R.↗

Space Shuttle solid rocket motor /SRM/ development and qualification

The configuration of the reusable Space Shuttle solid rocket motors is described. In addition, their design evolution is reviewed, noting that the requirement that certain components be recovered, refurbished, and used on as many as 20 flights dictated a conservative design approach, the validity of which has been proven by successful testing of all development and qualification motors. Aspects discussed include ballistics, the motor case, nozzle, nozzle materials, and the ignition system. Finally, summary results of the first two of three qualification motor firings designated QM-1 and QM-2 are presented.

Lund, R. K.↗

Development of electrical test procedures for qualification of spacecraft against EID. Volume 1: The CAN test and other relevant data

A combined experimental and analytical program to develop system electrical test procedures for the qualification of spacecraft against damage produced by space-electron-induced discharges (EID) occurring on spacecraft dielectric outer surfaces is described. The data on the response of a simple satellite model, called CAN, to electron-induced discharges is presented. The experimental results were compared to predicted behavior and to the response of the CAN to electrical injection techniques simulating blowoff and arc discharges. Also included is a review of significant results from other ground tests and the P78-2 program to form a data base from which is specified those test procedures which optimally simulate the response of spacecraft to EID. The electrical and electron spraying test data were evaluated to provide a first-cut determination of the best methods for performance of electrical excitation qualification tests from the point of view of simulation fidelity.

Wilkenfeld, J. M.↗

Development of electrical test procedures for qualification of spacecraft against EID. Volume 2: Review and specification of test procedures

A combined experimental and analytical program to develop system electrical test procedures for the qualification of spacecraft against damage produced by space-electron-induced discharges (EID) occurring on spacecraft dielectric outer surfaces is described. A review and critical evaluation of possible approaches to qualify spacecraft against space electron-induced discharges (EID) is presented. A variety of possible schemes to simulate EID electromagnetic effects produced in spacecraft was studied. These techniques form the principal element of a provisional, recommended set of test procedures for the EID qualification spacecraft. Significant gaps in our knowledge about EID which impact the final specification of an electrical test to qualify spacecraft against EID are also identified.

Wilkenfeld, J. M.↗

Development of a qualification standard for adhesives used in hybrid microcircuits

Improved qualification standards and test procedures for adhesives used in microelectronic packaging are developed. The test methods in specification for the Selection and Use of Organic Adhesives in Hybrid Microcircuits are reevaluated versus industry and government requirements. Four electrically insulative and four electrically conductive adhesives used in the assembly of hybrid microcircuits are selected to evaluate the proposed revised test methods. An estimate of the cost to perform qualification testing of an adhesive to the requirements of the revised specification is also prepared.

Licari, J. J.↗

Qualification tests and electrical measurements: Practice and problems

As part of the Flat-Plate Solar Array Project, 138 different module designs were subjected to qualification tests. Electrical measurements were subjected on well over a thousand modules representing more than 150 designs. From this experience, conclusions are drawn regarding results and problems, with discussion of the need for change or improvement. The qualification test sequence incuded application of environmental and electrical stresses to the module. With few exceptions, the tests have revealed defects necessitation of environmental and electrical stresses to the module. With few exceptions, the tests have revealed defects necessitating module design or process changes. However, the continued need for these tests may be questioned on the basis of technical and logistical factors. Technically, the current test sequence does not cover all design characteristics, does not include all field conditions and is not known to represent the desired 30-year module life. Logistically, the tests are time-consuming and costly, and there is a lack of, fully qualified independent test organizations. Alternatives to the current test program include simplification based on design specification and site environment, and/or the use of warranties or other commercial practices.

Smokler, M. I.↗

Qualification testing and electrical measurement experience: A manufacturer's view

ARCO Solar's experiences as a participant in an industry-utility-government environmental qualification team examining photovoltaic devices are discussed. Included is an assessment of the applicability, completeness and appropriateness of the testing procedures and of the acceptance criteria for megawatt-sized procurements for utilities. Like the stand-alone users, the utility industry is interested in obtaining low costs, but additional concerns exist related to reliability and durability, safety, grounding and overall system criteria including performance prediction (related to output power acceptance testing), power quality and dispatchability. For purposes of this first major purchase of photovoltaic modules and panels by the utility industry, there was a carry-over of the JPL specifications. The need exists for futher development, assessement, and selection of qualification and testing standards and evaluation criteria specifically addressing these additional concerns for utility-connected PV power-plant applications.

Arnett, J. C.↗

Qualification needs for advanced integrated aircraft

In an effort to achieve maximum aircraft performance, designers are integrating aircraft systems. The characteristics of aerodynamics, vehicle structure, and propulsion systems are being integrated and controlled through embedded, often flight critical, electronic systems. The qualification needs for such highly integrated aircraft systems are addressed. Based on flight experience with research aircraft, a set of test capabilities is described which allows for complete and efficient qualification of advanced integrated aircraft.

Mackall, D. A.↗