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NASA NTRS2012

Combustion, Complex Fluids, and Fluid Physics Experiments on the ISS

From the very first days of human spaceflight, NASA has been conducting experiments in space to understand the effect of weightlessness on physical and chemically reacting systems. NASA Glenn Research Center (GRC) in Cleveland, Ohio has been at the forefront of this research looking at both fundamental studies in microgravity as well as experiments targeted at reducing the risks to long duration human missions to the moon, Mars, and beyond. In the current International Space Station (ISS) era, we now have an orbiting laboratory that provides the highly desired condition of long-duration microgravity. This allows continuous and interactive research similar to Earth-based laboratories. Because of these capabilities, the ISS is an indispensible laboratory for low gravity research. NASA GRC has been actively involved in developing and operating facilities and experiments on the ISS since the beginning of a permanent human presence on November 2, 2000. As the lead Center both Combustion, Fluid Physics, and Acceleration Measurement GRC has led the successful implementation of an Acceleration Measurement systems, the Combustion Integrated Rack (CIR), the Fluids Integrated Rack (FIR) as well as the continued use of other facilities on the ISS. These facilities have supported combustion experiments in fundamental droplet combustion fire detection fire extinguishment soot phenomena flame liftoff and stability and material flammability. The fluids experiments have studied capillary flow magneto-rheological fluids colloidal systems extensional rheology pool and nucleate boiling phenomena. In this paper, we provide an overview of the experiments conducted on the ISS over the past 12 years. We also provide a look to the future development. Experiments presented in combustion include areas such as droplet combustion, gaseous diffusion flames, solid fuels, premixed flame studies, fire safety, and super critical oxidation processes. In fluid physics, experiments are discussed in multiphase flows, capillary phenomena, and heat pipes. Finally in complex fluids, experiments in rheology and soft condensed materials will be presented.

Motil, Brian↗

NASA NTRS2014

On Characterizing Particle Shape

It is well known that particle shape affects flow characteristics of granular materials, as well as a variety of other solids processing issues such as compaction, rheology, filtration and other two-phase flow problems. The impact of shape crosses many diverse and commercially important applications, including pharmaceuticals, civil engineering, metallurgy, health, and food processing. Two applications studied here include the dry solids flow of lunar simulants (e.g. JSC-1, NU-LHT-2M, OB-1), and the flow properties of wet concrete, including final compressive strength. A multi-dimensional generalized, engineering method to quantitatively characterize particle shapes has been developed, applicable to both single particle orientation and multi-particle assemblies. The two-dimension, three dimension inversion problem is also treated, and the application of these methods to DEM model particles will be discussed. In the case of lunar simulants, flow properties of six lunar simulants have been measured, and the impact of particle shape on flowability - as characterized by the shape method developed here -- is discussed, especially in the context of three simulants of similar size range. In the context of concrete processing, concrete construction is a major contributor to greenhouse gas production, of which the major contributor is cement binding loading. Any optimization in concrete rheology and packing that can reduce cement loading and improve strength loading can also reduce currently required construction safety factors. The characterization approach here is also demonstrated for the impact of rock aggregate shape on concrete slump rheology and dry compressive strength.

Ennis, Bryan J.↗

NASA NTRS2017

Field Detection of Chemical Assimilation in A Basaltic Lava Flow

Lava channels are features seen throughout the inner Solar System, including on Earth, the Moon, and Mars. Flow emplacement is therefore a crucial process in the shaping of planetary surfaces. Many studies, including some completed by members of this team at the December 1974 lava flow, have investigated the dynamics of lava flow emplacement, both on Earth and on the Moon and how pre-flow terrain can impact final channel morphology, but far fewer have focused on how the compositional characteristics of the substrate over which a flow was em-placed influenced its final flow morphology. Within the length of one flow, it is common for flows to change in morphology, a quality linked to rheology (a function of multiple factors including viscosi-ty, temperature, composition, etc.). The relationship between rheology and temperature has been well-studied but less is known about the relationship between an older flow's chemistry and how the interaction between this flow and the new flow might affect lava rheology and therefore emplacement dynamics. Lava erosion. Through visual observations of active terrestrial flows, mechanical erosion by flowing lava has been well-documented. Lava erosion by which flow composition is altered as the active lava melts and assimilates the pre-flow terrain over which it moves is also hypothesized to affect channel formation. However, there is only one previous field study that geochemically documents the process in recent basaltic flow systems.

Young, K. E.↗

NASA NTRS2017

Documenting Chemical Assimilation in a Basaltic Lava Flow

Lava channels are features seen throughout the inner Solar System, including on Earth, the Moon, and Mars. Flow emplacement is therefore a crucial process in the shaping of planetary surfaces. Many studies have investigated the dynamics of lava flow emplacement, both on Earth and on the Moon [1,2,3] but none have focused on how the compositional and structural characteristics of the substrate over which a flow was emplaced influenced its final flow morphology. Within the length of one flow, it is common for flows to change in morphology, a quality linked to lava rheology (a function of multiple factors including viscosity, temperature, composition, etc.). The relationship between rheology and temperature has been well-studied [4,5,6] but less is understood about the relationship between a pre-flow terrain's chemistry and how the interaction between this flow and the new flow might affect lava rheology and therefore emplacement dynamics. Lava erosion. Through visual observations of active terrestrial flows, lava erosion has been well-documented [i.e. 7,8,9,10]. Lava erosion is the process by which flow composition is altered as the active lava melts and assimilates the pre-flow terrain over which it moves. Though this process has been observed, there is only one instance of where it was been geochemically documented.

assimilation↗

NASA NTRS2016

New Approaches to Inferences for Steep-Sided Domes on Venus

New mathematical approaches for the relaxation and emplacement of viscous lava domes are presented and applied to steep-sided domes on Venus. A similarity solution approach is applied to the governing equation for fluid flow in a cylindrical geometry for two distinct scenarios. In the first scenario, dome relaxation is explored assuming a constant volume of fluid (i.e. lava) has been rapidly emplaced onto the surface. Cooling of lava is represented by a time-variable viscosity and singularities inherent in previous models for dome relaxation have been eliminated. At the onset of relaxation, bulk dynamic viscosities lie in the range between 10(exp 10) - 10(exp 16) Pa s, consistent with basaltic-andesite to rhyolitic compositions. Plausible relaxation times range from 5 to 5000 years, depending on initial lava viscosity. The first scenario, however, is only valid during the final stages of dome relaxation and does not consider the time taken for lava to be extruded onto the surface. In the second scenario, emplacement and growth of a steep-sided dome is considered when the volume of lava on the surface increases over time (i.e. time-variable volume approach). The volumetric flow rate may depend on an arbitrary power of the dome thickness, thus embracing Newtonian as well as other rheologies for describing terrestrial and planetary mass flows. The approach can be used to distinguish between basic flow rate models for fluid emplacement. The formalism results in radial expansion of a dome proportional to t(sup 1/2), consistent with the diffusive nature of the governing equation. The flow at the front is shown to thicken as the front advances for a constant rate of lava supply. Emplacement times are intimately correlated with the bulk rheology. Comparison of the theoretical profiles with the shape of a typical dome on Venus indicates that a Newtonian bulk rheology is most appropriate, consistent with prior studies. However, results here suggest a bulk dynamic viscosity of 10(exp 12) - 10(exp 13) Pa s and emplacement times of approximately 2-16 years. Both scenarios investigated give emplacement times significantly less than prior estimates and compositions consistent with basaltic andesite.

steep-sided domes↗

NASA NTRS1972

Comparison of conventional and microasperity elastohydrodynamic lubrication of a ballspinning in a nonconforming groove

An analysis was developed for the microasperity elastohydrodynamic lubrication of a ball spinning in a nonconforming groove. This analysis was compared to the conventional elastohydrodynamic analysis of a ball spinning in a nonconforming groove. Rheological models for a di-2-ethylhexyl sebacate, a super-refined naphthenic mineral oil, and a polyphenyl ether (5P4E) were constructed from spinning torque data by using both analyses. The value of the lubricant pressure-viscosity coefficient that makes the data fit the analyses of the fluids differs somewhat from published data. For all three lubricants, an exponential composite model best described the lubricant rheology. Good agreement existed with the experimental and analytical values of torque for both the conventional and microasperity elastohydrodynamic analysis for a spinning ball in a nonconforming groove.

Allen, C. W.↗

NASA NTRS1975

Potential seal candidates for high-energy propellants

Five potential seal candidates (linear Tefzel, linear Halar, crosslinked Halar, Viton ECD-006, and phosphazine fluoroelastomer) were evaluated for the orbital maneuvering system of the space shuttle. Since this system employs nitrogen tetroxide (N2O4) and monomethyl hydrazine (MMH) as hypergolic propellants, the seal candidates were selected on the basis of projected chemical resistance as well as rheological behavior. Chemical resistance to these high-energy fuels was determined via conventional isothermal and thermal cycling immersion tests. Rheological measurements, however, were performed on O-rings molded from the subject seal candidates. Properties determined, such as cyclic work and hysteresis, stress relaxation, and indicated modulus, therefore, relate to the O-ring seals themselves.

Merz, P. L.↗

NASA NTRS1969

Fundamental considerations for future solid lubricants

Properties important to the performance of solid lubricants are discussed. Those properties include shear characteristics, coherence between particles, resistance to cold flow, adherence to the substrate, applicable chemical thermodynamics and kinetics of materials and environments, polymorphism, and rheology. The following generalizations are made: (1) chemical thermodynamics and kinetics are powerful tools for use in determining the useful environments and methods of application for solid film lubricants; (2) the primary requirement for a solid lubricant is low shear strength; (3) the rheology of solid film constituents and formulations is likely to be of vital importance to performance and life; and (4) adherence and mobility of surface films is another primary requirement for long lived solid lubricants.

Johnson, R. L.↗

NASA NTRS1978

Surface temperatures and glassy state investigations in tribology, part 1

The research in this report is divided into two categories: (1) lubricant rheological behavior, and (2) thermal behavior of a simulated elastohydrodynamic contact. The studies of the lubricant rheological behavior consists of high pressure, low shear rate viscosity measurements, viscoelastic transition measurements, by volume dilatometry, dielectric transitions at atmospheric pressure and light scattering transitions. Lubricant shear stress-strain behavior in the amorphous glassy state was measured on several fluids. It appears clear from these investigations that many lubricants undergo viscoplastic transitions in typical EHD contacts and that the lubricant has a limiting maximum shear stress it can support which in turn will determine the traction in the contact except in cases of very low slide-roll ratio. Surface temperature measurements were made for a naphthenic mineral oil and a polyphenyl ether. The maximum surface temperature in these experiments was approximately symmetrical about the zero slide-roll ration except for absolute values of slide-roll ratio greater than about 0.9. Additional surface temperature measurements were made in contacts with rough surfaces where the composite surface roughness was approximately equal to the EHD film thickness. A regression analysis was done to obtain a predictive equation for surface temperatures as a function of pressure, sliding speed, and surface roughness. A correction factor for surface roughness effects to the typical flash temperature analysis was found.

Winer, W. O.↗

NASA NTRS1979

Surface temperatures and glassy state investigations in tribology, part 2

Measurements of lubricant shear rheological behavior in the amorphous solid region and near the liquid solid transition are reported. Elastic, plastic and viscous behavior was observed. The maximum yield shear stress (limiting shear stress) is a function of temperature and pressure and is believed to be the property which determines the maximum traction in elastohydrodynamic contacts such as traction drives. A shear rheological model based on primary laboratory data is proposed for concentrated contact lubrication. The model is Maxwell model modified with a limiting shear stress. Three material properties are required: low shear stress viscosity, limiting elastic shear modulus, and the limiting shear stress the material can withstand. All three are functions of temperature and pressure.

Bair, S. S.↗

NASA NTRS1979

Surface temperatures and glassy state investigations in tribology

The limiting shear stress shear rheological model was applied to property measurements pursuant to the use of the constitutive equation and the application of the constitutive equation to elastrohydrodynamic (EHD) traction. Experimental techniques were developed to subject materials to isothermal compression which is similar to the history the materials were subjected to in EHD contacts. In addition, an apparatus was developed for measuring the shear stress-strain behavior of solid lubricating materials. Four commercially available materials were examined under pressure. They exhibit elastic and limiting shear stress behavior similar to that of liquid lubricants. The application of the limiting shear stress model to traction predictions was extended employing the primary materials properties measured in the laboratory. The shear rheological model was also applied to a Grubin-like EHD inlet analysis for predicting film thicknesses when employing the limiting shear stress model material behavior.

Bair, S.↗

NASA NTRS1980

Surface temperatures and glassy state investigations in tribology, part 3

Research related to the development of the limiting shear stress rheological model is reported. Techniques were developed for subjecting lubricants to isothermal compression in order to obtain relevant determinations of the limiting shear stress and elastic shear modulus. The isothermal compression limiting shear stress was found to predict very well the maximum traction for a given lubricant. Small amounts of side slip and twist incorporated in the model were shown to have great influence on the rising portion of the traction curve at low slide-roll ratio. The shear rheological model was also applied to a Grubin-like elastohydrodynamic inlet analysis for predicting film thicknesses when employing the limiting shear stress model material behavior.

Bair, S.↗

NASA NTRS1980

Influence of excess diamine on properties of PMR polyimide resins and composites

By varying the stoichiometry of the reactants in the preparation of PMR polyimide resin, changes occur in molecular weight distribution which influence the rheological properties and thus the processability of the resin, as well as the mechanical properties of the composite. The influence of 1-10 percent molar excess MDA on the molecular weight distribution and rheological properties of an imidized PMR system were exposed. Molecular weight distribution is characterized by gel permeation chromatography of the imidized molding compound; shear viscosity is related to changes in average molecular weight. The thermo-oxidative stability at 600 F, glass transition temperature, flexural and interlaminar shear properties of PMR polyimide/Celion 6000 graphite fiber composites are compared as a function of the percent excess MDA in the monomer reactant mixture.

Hurwitz, F. I.↗

NASA NTRS1981

Traction contact performance evaluation at high speeds

The results of traction tests performed on two fluids are presented. These tests covered a pressure range of 1.0 to 2.5 GPa, an inlet temperature range of 30 'C to 70 'C, a speed range of 10 to 80 m/sec, aspect ratios of .5 to 5 and spin from 0 to 2.1 percent. The test results are presented in the form of two dimensionless parameters, the initial traction slope and the maximum traction peak. With the use of a suitable rheological fluid model the actual traction curves measured can now be reconstituted from the two fluid parameters. More importantly, the knowledge of these parameters together with the fluid rheological model, allow the prediction of traction under conditions of spin, slip and any combination thereof. Comparison between theoretically predicted traction under these conditions and those measured in actual traction tests shows that this method gives good results.

Tevaarwerk, J. L.↗

NASA NTRS1982

A schematic model of crater modification by gravity

The morphology of craters found on planets and moons of the solar system is examined and a development model which can account for the observed crater characteristics is discussed. The prompt collapse of craters to form flat floors, terraced walls, and central peak structures is considered to be the result of an approximate Bingham plastic rheology of the material surrounding the crater. This rheology is induced dynamically by the strong incoherent acoustic 'noise' accompanying excavation of the crater. Central pits, peak rings, and other multiple symmetric-profile rings originate by oscillation of this fluid. Large craters with transient depths comparable to the lithosphere thickness are subject to collapse by fragmentation of the lithosphere as well as fluidization. The considered concepts are developed mathematically. A model emerges which appears capable of explaining most of the qualitative features of large impact structures.

Melosh, H. J.↗

NASA NTRS1980

Thermal evolution of Ganymede and Callisto - Effects of solid-state convection and constraints from Voyager imagery

The imaging experiments of the Voyager 1 and 2 fly-by missions have provided a large amount of information about the nature of the surfaces of the Galilean satellites. The present investigation is concerned with the development of models regarding the thermal evolution of Ganymede and Callisto, taking into account the approach of parameterized convection. Attention is given to the physical, chemical, and geological data which are available as constraints on the thermal evolution of Ganymede and Callisto. Both satellites appear to possess surfaces composed of silicates and ice. However, their surface features are distinctly different from each other. In the discussion of thermal evolution models, attention is given to ice-dominant rheology, silicate-dominant rheology, and aspects of phase changes and solid-state convection.

Thurber, C. H.↗

NASA NTRS1982

Polymer research at NASA Langley Research Center

Polymer synthesis programs involve the development of Novel thermoplastics, pseudothermoplastics, and thermosets. These systems are prepared to elucidate structure-property relationships involving thermal capabilities, toughness, processability and environmental stability. Easily processable polyimides, solvent-resistant polysulfones and polyphenylquinoxalines, and tougher high and intermediate temperature polymers were developed. Characterization efforts included high pressure liquid chromatography methodology, the development of toughness tests for fiber reinforced composites, a study of electrical properties of metal ion filled polyimides, and a study of the mutagenicity of aromatic diamines. Also the mechanism of cure/degradation of experimental polymers was studied by rheology, mechanical behavior, separation techniques and spectroscopy. The degradative crosslinking of alkyl-containing polyimides, the separation and identification of crosslinked phenylquinoxalines, the rheological behavior of hot-melt polyimides, and the elucidation of the cure of norbornene endcapped imides were also studied.

Terry L. St. Clair↗

NASA NTRS1983

Crustal deformation, the earthquake cycle, and models of viscoelastic flow in the asthenosphere

The crustal deformation patterns associated with the earthquake cycle can depend strongly on the rheological properties of subcrustal material. Substantial deviations from the simple patterns for a uniformly elastic earth are expected when viscoelastic flow of subcrustal material is considered. The detailed description of the deformation pattern and in particular the surface displacements, displacement rates, strains, and strain rates depend on the structure and geometry of the material near the seismogenic zone. The origin of some of these differences are resolved by analyzing several different linear viscoelastic models with a common finite element computational technique. The models involve strike-slip faulting and include a thin channel asthenosphere model, a model with a varying thickness lithosphere, and a model with a viscoelastic inclusion below the brittle slip plane. The calculations reveal that the surface deformation pattern is most sensitive to the rheology of the material that lies below the slip plane in a volume whose extent is a few times the fault depth. If this material is viscoelastic, the surface deformation pattern resembles that of an elastic layer lying over a viscoelastic half-space. When the thickness or breath of the viscoelastic material is less than a few times the fault depth, then the surface deformation pattern is altered and geodetic measurements are potentially useful for studying the details of subsurface geometry and structure. Distinguishing among the various models is best accomplished by making geodetic measurements not only near the fault but out to distances equal to several times the fault depth. This is where the model differences are greatest; these differences will be most readily detected shortly after an earthquake when viscoelastic effects are most pronounced.

Cohen, S. C.↗