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NASA NTRS1980

Cork-resin ablative insulation for complex surfaces and method for applying the same

A method of applying cork-resin ablative insulation material to complex curved surfaces is disclosed. The material is prepared by mixing finely divided cork with a B-stage curable thermosetting resin, forming the resulting mixture into a block, B-stage curing the resin-containing block, and slicing the block into sheets. The B-stage cured sheet is shaped to conform to the surface being insulated, and further curing is then performed. Curing of the resins only to B-stage before shaping enables application of sheet material to complex curved surfaces and avoids limitations and disadvantages presented in handling of fully cured sheet material.

Walker, H. M.↗

NASA NTRS2007

Genesis Concentrator Target Particle Contamination Mapping and Material Identification

The majority of surface particles were found to be < 5 microns in diameter with increasing numbers close to the optical resolution limit of 0.3 microns. Acceleration grid EDS results show that the majority of materials appear to be from the SRC shell and SLA materials which include carbon-carbon fibers and Si-rich microspheres in a possible silicone binder. Other major debris material from the SRC included white paint, kapton, collector array fragments, and Al. Image analysis also revealed that SRC materials were also found mixed with the Utah mud and salt deposits. The EDS analysis of the acceleration grid showed that particles < 1 m where generally carbon based particles. Chemical cleaning techniques with Xylene and HF in an ultrasonic bath are currently being investigated for removal of small particles by the Genesis science team as well as ultra-pure water megasonic cleaning by the JSC team [4]. Removal of organic contamination from target materials is also being investigated by the science team with the use of UV-ozone cleaning devices at JSC and Open University [5]. In preparation for solar wind oxygen analyses at UCLA and Open University [1, 2], surface particle contamination on three Genesis concentrator targets was closely examined to evaluate cleaning strategies. Two silicon carbide (Genesis sample # 60001 and 60003) and one chemical vapor deposited (CVD) 13C concentrator target (60002) were imaged and mosaic mapped with optical microscopes. The resulting full target mosaic images and particle feature maps were subsequently compared with non-flight, but flight-like, concentrator targets and sample return capsule (SRC) materials. Contamination found on the flown concentrator acceleration grid was further examined using a scanning electron microscope (SEM). Energy dispersive X-ray spectroscopy (EDS) for particle identification was subsequently compared with the optical images from the flown targets. Figure 1 show that all three targets imaged in this report are fully intact and do not show any signs of material fractures. However, previous ellipsometry results and overview imaging of both flown SiC targets show a solar wind irradiation gradient from the center focal point to the outer edge [3]. In addition, due to the hard landing, each target has experienced varying degrees of impacts, scratches, and particle debris from the spacecraft and Utah impact site.

Calaway, Michael J.↗

NASA NTRS2021

Insitu Lunar Launch & Landing Pad Construction w/ Regolith and Thermoset Polymers

This CIF project is an extension of materials developed under a previous NASA Innovative Advanced Concepts (NIAC) project titled “Regolith Derived Heat Shield for Planetary Body Entry and Descent Systems with In-Situ Fabrication” by M. Hogue et al. (2012). Launch and landing pads are necessary to mitigate risks to lander/ascent vehicles, surface assets, and orbital assets from rocket plume ejected regolith. At this time, all launching and landing on the lunar surface will be on unprepared surface sites. Though this has been a successful approach for Apollo and other uncrewed missions, significant risks exist for the Artemis Program due to the increased thrust of the vehicles, presence of co-located assets, and potential surface level requirements for tall vehicles. This project developed a thermoset polymer–regolith composite material for use as a launch and landing pad. Test articles were prepared at 20% and 11% polymer mass percent (wt%) and tested under hot fire conditions that simulated large vehicle lunar launch/landing conditions. A minimum polymer wt% of 9% was achieved and both samples successfully mitigated regolith ejecta from plume effects. A concept for emplacing launch/landing pads was successfully tested in laboratory environments using a screw and barrel approach to mixing, conveying and depositing materials. It is recommended that materials and systems be developed to TRL 6 for a small-scale lunar demonstration of emplacement of a launch/landing pad via a Commercial Lunar Payload Services (CLPS) mission to support the Artemis Program.

Nathan Gelino↗

NASA NTRS1985

SCARE: A post-processor program to MSC/NASTRAN for the reliability analysis of structural ceramic components

A computer program was developed for calculating the statistical fast fracture reliability and failure probability of ceramic components. The program includes the two-parameter Weibull material fracture strength distribution model, using the principle of independent action for polyaxial stress states and Batdorf's shear-sensitive as well as shear-insensitive crack theories, all for volume distributed flaws in macroscopically isotropic solids. Both penny-shaped cracks and Griffith cracks are included in the Batdorf shear-sensitive crack response calculations, using Griffith's maximum tensile stress or critical coplanar strain energy release rate criteria to predict mixed mode fracture. Weibull material parameters can also be calculated from modulus of rupture bar tests, using the least squares method with known specimen geometry and fracture data. The reliability prediction analysis uses MSC/NASTRAN stress, temperature and volume output, obtained from the use of three-dimensional, quadratic, isoparametric, or axisymmetric finite elements. The statistical fast fracture theories employed, along with selected input and output formats and options, are summarized. An example problem to demonstrate various features of the program is included.

Gyekenyesi, J. P.↗

NASA NTRS1986

SCARE - A postprocessor program to MSC/NASTRAN for reliability analysis of structural ceramic components

Gyekenyesi, J. P.↗

NASA NTRS1993

Galileo SSI lunar observations: Copernican craters and soils

The Galileo spacecraft completed its first Earth-Moon flyby (EMI) in December 1990 and its second flyby (EM2) in December 1992. Copernican-age craters are among the most prominent features seen in the SSI (Solid-State Imaging) multispectral images of the Moon. The interiors, rays, and continuous ejecta deposits of these youngest craters stand out as the brightest features in images of albedo and visible/1-micron color ratios (except where impact melts are abundant). Crater colors and albedos (away from impact melts) are correlated with their geologic emplacement ages as determined from counts of superposed craters; these age-color relations can be used to estimate the emplacement age (time since impact event) for many Copernican-age craters on the near and far sides of the Moon. The spectral reflectivities of lunar soils are controlled primarily by (1) soil maturity, resulting from the soil's cumulative age of exposure to the space environment; (2) steady-state horizontal and vertical mixing of fresh crystalline materials ; and (3) the mineralogy of the underlying bedrock or megaregolith. Improved understanding of items (1) and (2) above will improve our ability to interpret item (3), especially for the use of crater compositions as probes of crustal stratigraphy. We have examined the multispectral and superposed crater frequencies of large isolated craters, mostly of Eratosthenian and Copernican ages, to avoid complications due to (1) secondaries (as they affect superposed crater counts) and (2) spatially and temporally nonuniform regolith mixing from younger, large, and nearby impacts. Crater counts are available for 11 mare craters and 9 highlands craters within the region of the Moon imaged during EM1. The EM2 coverage provides multispectral data for 10 additional craters with superposed crater counts. Also, the EM2 data provide improved spatial resolution and signal-to-noise ratios over the western nearside.

Mcewen, A. S.↗

NASA NTRS2006

Icy Satellites of the Planets, and the Work of V.I. Moroz

The satellites of the giant planets are highly varied in size and density, indicating a wide range of compositions. The principal components of these satellites are ices of many different compositions (with H2O the most abundant) and varying amounts of silicate rocky material. Many different ices have been found by spectroscopic techniques both from Earth-based observatories and from planetary spacecraft. Three of the Galilean satellites of Jupiter exhibit H2O ice on their surfaces, while small amounts of CO2 are present on Ganymede and Callisto. The volcanic satellite Io has abundant SO2 ice and frost deposits. Saturn s satellites have surfaces dominated by H2O ice, but CO2 is also present on most of them, and in the cases of the low-albedo satellites Iapetus and Phoebe, there is evidence of complex hydrocarbons mixed with the surface materials. The large Uranian satellites also have H2O-dominated surfaces, but CO2 has also been discovered on two of them. Neptune s largest satellite, Triton, show spectroscopic evidence for six different ices, including N2, CH4, CO, CO2, H2O, and C2H6. The latter ice is a photochemical product from the action of sunlight on Triton's atmosphere. Pluto is similar to Triton, although CO2 has not been found. Pluto s large satellite, Charon, shows evidence for an ammonia hydrate on part of its surface. V. I. Moroz was a pioneer in the application of near-infrared detectors to astronomical sources. Using a prism spectrometer he measured the spectra of the Galilean satellites of Jupiter, and in 1966 he published the first near-infrared spectra, noting the appearance of H2O ice as a major component of Europa and Ganymede. This discovery, and the techniques of Moroz measurements help set the stage for the broad extension of the study of planetary, satellite, and asteroid surfaces through reflectance spectroscopy in the near-infrared.

Cruikshank, Dale P.↗

NASA NTRS1990

Approach to SSME health monitoring. II - Exhaust plume emission spectroscopy at the DTF

The Diagnostics Testbed Facility (DTF) located at the Stennis Space Center (SSC) is used for obtaining extensive sets of H2O2 exhaust plume emission spectral data for the SSME critical components related elements and materials. The SSME related elements and materials are simulated by mixing appropriate amounts of compounds of their respective constituent elements in an aqueous solution which is injected into the combustion chamber of the DTFT. Five of the most critical components of the SSME which have experienced very severe wear and tear problems in the past are analyzed. These are high pressure turbopump (HPTP) turbine blades, HPTP turbine disks, HPTP bearing, main injector LOX posts, and the main combustion chamber structural shell. The alloys used in the manufacturing of these components are MAR-M 246 + Hf, Waspaloy X, AISI 440C, Haynes 188, and Inconel 718, respectively. The experimental setup and procedures at the DTF are described; stratospheric data for the five alloys are presented; and strategies for the material identification in the SSME exhaust plume are discussed.

Tejwani, Gopal D.↗

NASA NTRSDate not supplied

Algorithmic Classification of Raman Spectra Biosignatures: Improving Life Detection Confidence

“Agnostic” biosignatures – indicators of life (or the absence of life), independent of a particular biochemistry – are increasingly considered a high standard for life detection. The Ladder of Life Detection (2018) called for investigating how combinations of independent and different potential biosignatures affect confidence. To address this gap, statistical classification of elemental abundances, isotopic fractionation, and reflectance spectroscopy (VNIR) has been implemented. Raman spectroscopy, highly desirable due to its wide availability, has the potential to improve this predictive power. This work implemented biosignature classification algorithms on Raman data alone, in preparation for combination with the other data types. Raman spectroscopy data was collected from published databases and papers as part of a manually curated dataset of “indicative” and “non-indicative of life” samples. These currently include 61 non-indicative samples (meteorites, magnetite); 3 indicative living samples (bacteria); 20 indicative non-living samples (chalk, bone); and 12 indicative mixed (with non-indicative material) samples (soil, microbial mats). Laboratory work is ongoing to characterize additional samples, particularly a greater breadth of mixed systems. Spectra were interpolated, filtered with the Savitzsky-Golay filter, and de-noised. For a preliminary examination, agnostic features were manually extracted including mean intensity, number of peaks, and mean peak width. Different peak prominences and filtering polynomials were used to refine features. Classification algorithms were implemented: k-nearest neighbors (KNN), logistic regression (LR), linear support vector machines (SVM), random forest (RF), Gaussian naïve bayes (GNB). Lastly, Monte Carlo simulations on 1,000 50%-train-test-splits were used to validate classification performance and feature significance. The preliminary feature set achieved its highest AUC of 0.52 with LR, with no strongly discriminatory features. Work to improve feature extraction, such as through deep learning with back propagation, is planned. In future work, the Raman data will be combined with the other data types, and potentially new data types such as enantiomeric excess. This project was partially supported through the NASA Ames Project EXcellence (APEX) incubator program.

Astrobiology↗

NASA NTRS2014

The Bombardment History of 4 Vesta as Told by Sample Geochronology

The Dawn mission showed asteroid 4 Vesta to be an extensively cratered body, ancient in age, with craters in a variety of morphologies and preservation states [1-3]. Tying Vesta's relative crater ages to an absolute impact history can be accomplished through investigations of the HED (howardite, eucrite, diogenite) meteorites. Eucrites are crustal basalts and gabbros, diogenites are mostly orthopyroxenites representing lower crust or upper mantle materials, and howardites are mixed breccias containing both lithologies. Eucrite 53Mn-53Cr systematics show that the HED parent body globally differentiated by ~4.56 Ga and fully crystallized soon afterwards [4]. Much later, many eucrites were brecciated and heated by large impacts into the parent body surface. Disturbance ages in eucrites show that multiple large impacts occurred within 1 Gyr after crystallization, showing a history that largely resembles that of the Moon [5-7]. Dawn images also showed that Vesta is covered with a well-developed regolith that is spectrally similar to howardite meteorites [8]. Howardites are polymict regolith breccias made up mostly of clasts of eucrites and diogenites, but which also contain clasts formed by melting of the regolith by relatively large, energetic impact events. Impact-melt clast ages from howardites extend our knowledge of the impact history of Vesta, expanding on eucrite disturbance ages and helping give absolute age context to the observed crater-counts produced using Dawn data. The distribution of 40Ar-39Ar ages of impact-melt clasts in howardites shows that they formed within the time period 3.3-3.8 Ga [9]. These, and other impact-melted HED materials, have distinct age and compositional characteristics that suggest they formed in discrete impact events. In order to create these crystalline impact-melt products on the surface of Vesta, the impacts during this time period must have had velocities much higher than 5 km/s, the main belt average [10]. This is inconsistent with formation by a normal distribution of impact velocities and points instead to a unique period where high-velocity collisions were more frequent than currently observed. Until now, impact-reset ages in the HED meteorites have been be interpreted under the umbrella of the canonical lunar cataclysm where an increase in the absolute number of bombarding objects is responsible for creating larger absolute amounts of impact-affected and impact-melted rocks, statistically increasing their chances of being found on Earth and dated. However, the distribution of age among the howardite impact-melt clasts may not necessarily result from an increased number of impacts, but rather result from impacts of higher velocity. The changeover from a typical main belt velocity profile to this regime of increased velocity population at Vesta occurs contemporaneously with a similar transition at the Moon, indicating that howardite impact-melt clast ages reinforce the notion of a dynamically unusual episode of bombardment in the inner solar system beginning at around 4.0 Ga.

Cohen, B. A.↗

NASA NTRS2017

The Chemistry of Pluto and its Satellites

Pluto's bulk composition and the composition of the surface layers hold clues to the origin and evolution of a number of other Solar System bodies of comparable size in the region beyond Neptune. The July 14, 2015 flyby of the Pluto system with the New Horizons spacecraft afforded the opportunity to corroborate and greatly improve discoveries about the planet and its satellites derived Earth-based studies. It also revealed extraordinary details of the surface and atmosphere of Pluto, as well as the geology and composition of Charon and two smaller satellites. With a mean density of 1.86 g/sq cm, the bulk composition of Pluto is about two-thirds anhydrous solar composition rocky material and one-third volatiles (primarily H2O in liquid and solid states) by mass, the surface is a veneer of ices dominated by N2, with smaller amounts of CH4 and CO, as well as limited exposures of H2O ice (considered to be "bedrock"). N2, CH4, and CO occur as solid solutions at temperature-dependent mutual concentrations, each component being soluble in the others. Frozen C2H6 as a minor component has also been identified. Sublimation and recondensation of N2, CH4, and CO over seasonal (248 y) and Milankovich-type megaseasons (approx. 3 My) result in the redistribution of these ices over time and with latitude control. Solid N2 is found in glaciers originating in higher elevations and flowing at the present time into a basin structure larger than the State of Texas, forming a convecting lens of N2 that overturns on a timescale of order 10 My. The varied colors of Pluto's landscape arise from the energetic processing of the surface ices in processes that break the simple molecules and reassemble complex organic structures consisting of groups of aromatic rings connected by aliphatic chains. When synthesized in the laboratory by UV or electron irradiation of a Pluto mix of ice, this material, called tholin, has colors closely similar to Pluto. The Pluto ice tholin analog contains carboxylic acids, urea, ketones, aldehydes, amines, and some nitriles. The largest satellite, Charon has density 1.70 g/sq cm and it is about 3/5 anhydrous solar composition rock, with the remainder in H2O ice. The surface H2O ice is infused in some way with NH3, probably as a hydrate, distributed nonuniformly, but to some degree related to geological structures. Pluto's atmosphere is N2, CH4, with CO, C2-hydrocarbons, HCN, and other molecules in trace but detectable amounts. The atmosphere supports a complex haze structure with about 20 discrete layers, and suspected clouds. The haze is presumed to be made of aggregates of complex hydrocarbons (tholins) produced by photolysis of the atmospheric gases, and with similar composition to the ice tholins made on the planet's surface. Urea and a suite of carboxylic acids are of interest for prebiotic and biological chemistries.

SOLAR SYSTEMS↗

NASA NTRS1991

Spectroscopy and multivariate analyses applications related to solid rocket nozzle bondline

Chemical composition and molecular orientation define the properties of materials. Information related to chemical composition and molecular configuration is obtained by various forms of spectroscopy. Software algorithms developed for multivariate analyses, expert systems, and Artificial Intelligence (AI) are used to conduct repetitive operations. The techniques are believed to be of particular significance toward achieving TQM objectives. The objective was to obtain information related to the quality of the bondline in the solid rocket motor, SRM, nozzle. Hysol 934 NA, a room temperature curing epoxide resin, is used as the bonding agent. A good bond requires that the adhesive be placed on a properly prepared metal surface, the adhesives Part A and B be mixed in appropriate ratio from material within shelf life specifications. Spectroscopic data was obtained for surfaces prepared according to specifications, contaminated metal surfaces, samples of the epoxide adhesive at times that represent shelf aging from 3 months to 2 years, several mix ratio of A to B, and curing material. Temperature was found to be a significant factor. The study concentrated on pot life and mix ratio.

Arendale, W. F.↗

NASA NTRS1999

Application of Novel Nonlinear Optical Materials to Optical Processing

We describe wave mixing and interactions in nonlinear photorefractive polymers and disodium flourescein. Higher diffracted orders yielding forward phase conjugation can be generated in a two-wave mixing geometry in photorefractive polymers, and this higher order can be used for image edge enhancement and correlation. Four-wave mixing and phase conjugation is studied using nonlinear disodium floureschein, and the nature and properties of gratings written in this material are investigated.

Banerjee, Partha P.↗

NASA NTRS2003

Electric Field Effects in Self-Propagating High-Temperature Synthesis under Microgravity Conditions

Self-propagating high-temperature synthesis (SHS) has been used to form many materials. SHS generally involves mixing reactants together (e.g., metal powders) and igniting the mixture such that a combustion (deflagration) wave passes though the mixture. The imposition of an electric field (AC or DC) across SHS reactants has been shown to have a marked effect on the dynamics of wave propagation and on the nature, composition, and homogeneity of the product . The use of an electric field with SHS has been termed "field-assisted SHS". Combustion wave velocities and temperatures are directly affected by the field, which is typically perpendicular to the average wave velocity. The degree of activation by the field (e.g., combustion rate) is related to the current density distribution within the sample, and is therefore related to the temperature-dependent spatial distribution of the effective electrical conductivity of reactants and products. Furthermore, the field can influence other important SHS-related phenomena including capillary flow, mass-transport in porous media, and Marangoni flows. These phenomena are influenced by gravity in conventional SHS processes (i.e., without electric fields). As a result the influence of the field on SHS under reduced gravity is expected to be different than under normal gravity. It is also known that heat loss rates from samples, which can depend significantly on gravity, can influence final products in SHS. This research program is focused on studying field-assisted SHS under reduced gravity conditions. The broad objective of this research program is to understand the role of an electric field in SHS reactions under conditions where gravity-related effects are suppressed. The research will allow increased understanding of fundamental aspects of field-assisted SHS processes as well as synthesis of materials that cannot be formed in normal gravity.

Unuvar, C.↗

NASA NTRS1948

Design criteria for and applications of the vortex generator mixing principal

There are at this date numerable projects, in various Divisions of U.A.C., either in progress or contemplated, which are employing the vortex generator mixing principle. This principle is defined as the method which utilises tip vortices generated by low aspect ratio airfoils for the purpose of transverse mixing of the flow of a confined fluid medium where the axis of the vortex is parallel to the direction of flow. To date, vortex generator design criteria have not been published. Therefore, for the assistance of those individuals concerned and in the interest of the vortex mixing principle, the following material (subject to modifications) is presented in this memorandum report.

H D Taylor↗

NASA NTRS1972

The response of a 0.03-cm silicon detector to a mixed neutron and gamma field as a function of shield material and thickness

The neutron and gamma radiation from a MHW-RTG was used to evaluate the total response of a shielded 0.3-mm silicon detector. The generator employs a 2200 W(th) PuO2 heat source concept known as the HELIPAK. The total integrated neutron and gamma ray fluxes at 100 cm away from the source along the radial direction were 1.67 x 1,000 n/sq cm/s and 1.49 x 10,000 gamma sq cm/s, respectively. Experimental values of the response function of the shielded silicon detector were used to determine the total counting rates due to photons at bias energies ranging from 50 to 200 keV. For neutrons, analytically computed response functions were used to determine the total counting rates at the same bias energies. It was found that for an aluminum shield the neutrons are not significant, regardless of the thickness of the shield. However, the magnitude of the total counting rate due to neutrons increases with increased atomic number of the shield and becomes comparable to the counting rate due to photons for a platinum shield thickness of 5 cm.

Taherzadeh, M.↗

NASA NTRS1975

New results from long-term observations of Cyg X-1

Observations of Cyg X-1 between October 1974 and July 1975 reveal a persistent 5.6 day modulation of the 3 to 6 keV X-ray intensity, having a minimum in phase with superior conjunction of the HDE 226868 binary system. The modulation is found to be most pronounced just prior to the April-May 1975 increase of Cyg X-1, after which both the modulation and intensity are at their lowest values for the entire duration of the observations. These data imply that the X-ray emission from Cyg X-1 arises from the compact member of HDE 226868, and that the increase of April-May 1975 may have represented the depletion of accreting material which was not mixed into a cylindrically symmetric accretion disk about the compact member.

Holt, S. S.↗

NASA NTRS1975

Directional-cosine and related pre-processing techniques - Possibilities and problems in earth-resources surveys

The possibilities of using various pre-processing techniques (directional-cosine, ratios and ratio/sum) have been investigated in relation to an urban land-use problem in Marion County, Indiana (USA) and for geologic applications in the San Juan Mountains of Colorado. For Marion County, it proved possible to classify directional-cosine data from September 1972 into different land uses by applying statistics developed with data from a May 1973 ERTS frame, thereby demonstrating the possibilities of using this type of data for signature-extension purposes. In the Silverton (Colorado) area pre-processed data proved superior to original data when extracting useful information in mountainous areas without corresponding ground observations. This approach allowed meaningful classification and interpretation of the data. The main problems encountered as a result of atmospheric effects, mixing of different surface materials, and the performance characteristics of ERTS are elucidated.

Quiel, F.↗