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At least 217 records · Page 12

Flight Readiness of Mochii S: Portable Spectroscopic Scanning Electron Microscope Facility on the International Space Station (ISS)

The ISS (International Space Station) currently lacks the capability to image and chemically analyze nano-to-micron scale particles from numerous engineering systems. To identify these particles, we must wait for a re-entry vehicle to return them from low earth orbit for ground-based SEM (Scanning Electron Microscope) / EDS (Energy Dispersive X-Ray Spectroscopy) analysis. This may take months, potentially delaying the affected system. Having an EDS-equipped SEM (Mochii S) aboard the ISS will accelerate response time thereby enhancing crew and vehicle safety by rapid and accurate identification of microscopic threats, especially in time-critical situations.The Mochii S payload will be stationed in the Japanese Experiment Module (JEM) powered by 120 VAC (Volts Alternating Current) inverter and connected to station Ethernet and WiFi (Fig. 1). To date the Mochii S payload has undergone testing for command and data handling, power quality, flight vibration, and radiation testing at Johnson Space Center (JSC). Mochii's high-RPM (Revolutions Per Minute) rotating vacuum pumps and high voltage systems have been reviewed to meet safety standards by JSC (Johnson Space Center) Engineering. Topology of the system in the JEM module has been baselined by ISS Safety and JAXA (Japan Space Exploration Agency). Digital controls to and from ISS over Joint Station LAN (Local Area Network) uplink have been simulated and the latencies and data rates have been found to be sufficient for successful operation of the payload from ground.Transporting sensitive electron optical instruments aboard a rocket that sustains 7G acceleration for 8 minutes and then operating it the unique microgravity (micro-g) environment is no trivial matter. To meet strict safety requirements and increase robustness for mission success, over 500 unique verifications must be completed before the payload is certified for spaceflight. Two of which will be discussed in detail are: vibroacoustic testing and magnetic susceptibility shielding and validation.

Mochii↗

Infrared observations of planets

A positive correlation was found between the strength of the 3-micron water feature and the strength of the absorption feature shortward of 0.4 microns. This is similar to what is seen in laboratory spectra of carbonaceous chondrites whose silicate compositions range from hydrated phyllosilicates to anhydrous olivine. Features were found in the IRAS images that appear to be related to solar system objects. Analysis of the data has yielded narrow trails of dust coincident with the orbits of comets Temple 2, Encke, and Gunn. Dust is found both ahead and behind comet orbital positions due to low-velocity ejection of large particles during perihelion passage. The occultation diameters of Ceres and Pallas were used to improve the standard thermal model used in the reduction of thermal IR observations of asteroids.

Lebofsky, L. A.↗

Radiation-induced chromosomal instability in human mammary epithelial cells

Karyotypes of human cells surviving X- and alpha-irradiation have been studied. Human mammary epithelial cells of the immortal, non-tumorigenic cell line H184B5 F5-1 M/10 were irradiated and surviving clones isolated and expanded in culture. Cytogenetic analysis was performed using dedicated software with an image analyzer. We have found that both high- and low-LET radiation induced chromosomal instability in long-term cultures, but with different characteristics. Complex chromosomal rearrangements were observed after X-rays, while chromosome loss predominated after alpha-particles. Deletions were observed in both cases. In clones derived from cells exposed to alpha-particles, some cells showed extensive chromosome breaking and double minutes. Genomic instability was correlated to delayed reproductive death and neoplastic transformation. These results indicate that chromosomal instability is a radiation-quality-dependent effect which could determine late genetic effects, and should therefore be carefully considered in the evaluation of risk for space missions.

NASA Center JSC↗

Investigation of the Internal Electric Field in Cadmium Zinc Telluride Detectors Using the Pockels Effect and the Analysis of Charge Transients

The Pockels electro-optic effect can be used to investigate the internal electric field in cadmium zinc telluride (CZT) single crystals that are used to fabricate room temperature x and gamma radiation detectors. An agreement is found between the electric field mapping obtained from Pockels effect images and the measurements of charge transients generated by alpha particles. The Pockels effect images of a CZT detector along two mutually perpendicular directions are used to optimize the detector response in a dual anode configuration, a device in which the symmetry of the internal electric field with respect to the anode strips is of critical importance. The Pockels effect is also used to map the electric field in a CZT detector with dual anodes and an attempt is made to find a correlation with the simulated electric potential in such detectors. Finally, the stress-induced birefringence effects seen in the Pockels images are presented and discussed.

Groza, Michael↗

Soot Precursor Material: Visualization Via Simultaneous LIF-LII and Characterization Via TEM

Simultaneous combined laser-induced fluorescence and laser-induced incandescence (LIF-LII) images are presented for both a normal and inverse diffusion flame. The excitation wavelength dependence distinguishes the LIF and LII signals in images from the normal diffusion flame while the temporal decay distinguishes the signals in images of the inverse diffusion flame. Each flame presents a minimum in the combined LIF-LII intensity in a region separating the fuel pyrolysis and soot containing regions. Opacity, geometric in definition, and extent of crystallinity measured through both bright and dark field Transmission Electron Microscopy (TEM) characterizes the thermophoretically sampled material from within this minimal LIF-LII intensity region. TEM analysis reveals rather different soot processes occurring within the normal and inverse diffusion flame. In the normal diffusion flame, rapid chemical and physical coalescence of PAHs results in initial formation of soot precursor particles that are highly crystalline and evolve toward fully formed soot. In the inverse diffusion flame, rapid coalescence of pyrolysis products occurs, producing tarlike, globular structures equivalent in size to fully formed soot aggregates but with markedly less crystallinity than normal-appearing soot. These different material properties are interpreted as reflecting different relative rates of chemical and physical coalescence of fuel pyrolysis products versus carbonization. Significantly, these TEM images support qualitative photophysical arguments suggesting that, in general, this 'dark' region observed in the LIF-LII images demarcates a transitional region in which a fundamental change in the material the material chemical/physical properties occurs between solid carbonaceous soot and condensed or gaseous molecular growth material.

VanderWal, Randall L.↗

The detection of earth orbiting objects by IRAS

A systematic examination of 1836 images of the sky constructed from scans made by the Infrared Astronomical Satellite has resulted in the detection of 466 objects which are shown to be in earth orbit. Analysis of the spatial and size distribution and thermal properties of these objets, which may include payloads, rocket bodies and debris particles, is being conducted as one step in a feasibility study for space-based debris detection technologies.

Dow, Kimberly L.↗

The Mars 2001 Athena Precursor Experiment (APEX)

The Athena Precursor Experiment (APEX) is a suite of scientific instruments for the Mars Surveyor Program 2001 (MSP'01) lander. The major elements of the APEX pay load are: (1) Pancam/Mini-TES, a combined stereo color imager and mid-infrared point spectrometer. (2) An Alpha-Proton-X-Ray Spectrometer (APXS) for in-situ elemental analysis. (3) A Mossbauer Spectrometer for in-situ determination of the mineralogy of Fe-bearing rocks and soils. (4) A Magnet Array that can separate magnetic soil particles from non-magnetic ones.

Squyres, S. W.↗

Global Estimates of Average Ground-Level Fine Particulate Matter Concentrations from Satellite-Based Aerosol Optical Depth

Exposure to airborne particles can cause acute or chronic respiratory disease and can exacerbate heart disease, some cancers, and other conditions in susceptible populations. Ground stations that monitor fine particulate matter in the air (smaller than 2.5 microns, called PM2.5) are positioned primarily to observe severe pollution events in areas of high population density; coverage is very limited, even in developed countries, and is not well designed to capture long-term, lower-level exposure that is increasingly linked to chronic health effects. In many parts of the developing world, air quality observation is absent entirely. Instruments aboard NASA Earth Observing System satellites, such as the MODerate resolution Imaging Spectroradiometer (MODIS) and the Multi-angle Imaging SpectroRadiometer (MISR), monitor aerosols from space, providing once daily and about once-weekly coverage, respectively. However, these data are only rarely used for health applications, in part because the can retrieve the amount of aerosols only summed over the entire atmospheric column, rather than focusing just on the near-surface component, in the airspace humans actually breathe. In addition, air quality monitoring often includes detailed analysis of particle chemical composition, impossible from space. In this paper, near-surface aerosol concentrations are derived globally from the total-column aerosol amounts retrieved by MODIS and MISR. Here a computer aerosol simulation is used to determine how much of the satellite-retrieved total column aerosol amount is near the surface. The five-year average (2001-2006) global near-surface aerosol concentration shows that World Health Organization Air Quality standards are exceeded over parts of central and eastern Asia for nearly half the year.

Van Donkelaar, A.↗

Instrumentation for gamma-ray astronomy

The current status of gamma-ray-telescope technology for ground, airborne, and space observations is surveyed and illustrated with drawings, diagrams, and graphs and tables of typical data. For the low- and medium-energy ranges, consideration is given to detectors and detector cooling systems, background-rejection methods, radiation damage, large-area detectors, gamma-ray imaging, data analysis, and the Compton-interaction region. Also discussed are the gamma-ray interaction process at high energies; multilevel automated spark-chamber gamma-ray telescopes; the Soviet Gamma-1 telescope; the EGRET instrument for the NASA Gamma-Ray Observatory; and Cerenkov, air-shower, and particle-detector instruments for the TeV and PeV ranges. Significant improvements in resolution and sensitivity are predicted for the near future.

Bertsch, David L.↗

Coronagraphic Observations of the Lunar Sodium Exosphere Near the Lunar Surface

The sodium exosphere of the Moon was observed using a solar coronagraph to occult the illuminated surface of the Moon. Exceptionally dust-free atmospheric conditions were required to allow the faint emission from sunlight scattered by lunar sodium atoms to be distinguished from moonlight scattered from atmospheric dust. At 0300 UT on April 22, 1994, ideal conditions prevailed for a few hours, and one excellent image of the sodium exosphere was measured, with the Moon at a phase angle of 51 deg, 81 % illuminated. Analysis of the image data showed that the weighted mean temperature of the exosphere was 1280 K and that the sodium column density varied approximately as cosine-cubed of the latitude. A cosine-cubed variation is an unexpected result, since the flux per unit area of solar photons and solar particles varies as the cosine of latitude. It is suggested that this can be explained by a temperature dependence for the sputtering of sodium atoms from the surface. This is a characteristic feature of chemical sputtering, which has been previously proposed to explain the sodium exosphere of Mercury. A possible interaction between chemical sputtering and solar photons is suggested.

Potter, A. E.↗

Measurements to Understand the Flow Mechanisms Contributing to Tandem-Rotor Outwash

Downwash and outwash characteristics of a model-scale tandem-rotor system in the presence of the ground were analyzed by identifying and understanding the physical mechanisms contributing to the observed flow field behavior. A building block approach was followed in simplifying the problem, separating the effects of the fuselage, effects of one rotor on the other, etc. Flow field velocities were acquired in a vertical plane at four aircraft azimuths of a small-scale tandem rotor system using the particle image velocimetry (PIV) technique for radial distances up to 4 times the rotor diameter. Results were compared against full-scale CH-47D measurements. Excellent correlation was found between the small- and full-scale mean flow fields (after appropriate normalization using rotor and wall jet parameters). Following the scalability analysis, the effect of rotor height on the outwash was also studied. Close to the aircraft, an increase in rotor height above ground decreased the outwash velocity at all aircraft azimuths. However, farther away, the longitudinal and lateral axes of the aircraft showed increasing and decreasing outwash velocities, respectively, with increasing rotor height. Measurements also indicated the presence of large-scale (of the size of the rotor height) shear-layer vortical structures along the ground that could be the source of low-frequency (approximately 1 Hz) flow variation observed in the full-scale measurements. Flow visualization studies and PIV measurements were also made on jets of different sizes to complement the observations made on rotors wherever possible. Baseline rotor measurements were made out-of-ground effect to understand the nature of inflow distribution for realistic rotor configurations and their modified characteristics in the presence of ground. Lastly, a feasibility study on applying high-fidelity CFD simulations for outwash study was conducted using Helios to model an isolated rotor configuration IGE at full scale Reynolds number. The results were encouraging and demonstrated the practical challenges associated with predicting rotor outwash.

Measurements↗

Measurements to Understand the Flow Mechanisms Contributing to Tandem-Rotor Outwash

Downwash and outwash characteristics of a model-scale tandem-rotor system in the presence of the ground were analyzed by identifying and understanding the physical mechanisms contributing to the observed flow field behavior. A building block approach was followed in simplifying the problem, separating the effects of the fuselage, effects of one rotor on the other, etc. Flow field velocities were acquired in a vertical plane at four aircraft azimuths of a small-scale tandem rotor system using the particle image velocimetry (PIV) technique for radial distances up to 4 times the rotor diameter. Results were compared against full-scale CH-47D measurements. Excellent correlation was found between the small- and full-scale mean flow fields (after appropriate normalization using rotor and wall jet parameters). Following the scalability analysis, the effect of rotor height on the outwash was also studied. Close to the aircraft, an increase in rotor height above ground decreased the outwash velocity at all aircraft azimuths. However, farther away, the longitudinal and lateral axes of the aircraft showed increasing and decreasing outwash velocities, respectively, with increasing rotor height. Measurements also indicated the presence of large-scale (of the size of the rotor height) shear-layer vortical structures along the ground that could be the source of low-frequency (approximately 1 Hz) flow variation observed in the full-scale measurements. Flow visualization studies and PIV measurements were also made on jets of different sizes to complement the observations made on rotors wherever possible. Baseline rotor measurements were made out-of-ground effect to understand the nature of inflow distribution for realistic rotor configurations and their modified characteristics in the presence of ground. Lastly, a feasibility study on applying high-fidelity CFD simulations for outwash study was conducted using Helios to model an isolated rotor configuration IGE at full-scale Reynolds number. The results were encouraging and demonstrated the practical challenges associated with predicting rotor outwash.

Ramasamy, Manikandan↗

Understanding the Feasibility of MAB Phase Structures for Lunar Applications

During the ten-week internship, my work focused on synthesis, characterization, and tailoring the flowability of the MAB phase powders for improving the surface finish and decreasing porosity of 3D-printed MAB phase structures. My mentor for the project was Dr. Samuel Hocker from NASA Langley and my faculty advisor was Dr. Surojit Gupta from the University of North Dakota. I also collaborated with Daniel Trieff from the University of North Dakota in developing characterization paradigm of 3D printed samples. The microencapsulation was performed via novel solvent casting-based microencapsulation process pioneered in UND, wherein a polymer (PLA, PHA) was dissolved into dichloromethane and precipitated onto the surface of the MoAlB particles. Two 100mL samples of microencapsulated powder was outsourced to Particle Technology Labs for flowability testing along with a 100mL control sample to determine if microencapsulation is a valid method for improving the flowability. The microencapsulated powders were characterized using SEM, Differential Scanning Calorimetry, and optical microscopy. The SEM images showed no change between the pure and microencapsulated powders. The optical microscopy analysis indicated a reduction in reflectivity for the PLA microencapsulated powders as well as hydrophobic properties. Both results suggest that microencapsulation was successful as PLA is a hydrophobic polymer and the change in reflectivity could be a result of the light being dispersed through the polymer coating. A reflectivity analysis will be done to bring more perspective to these observations. If powder flowability is improved, then the project will move forward with testing the printability of the microencapsulated powders and characterizing the structures using the designed characterization protocol. We are waiting for the DSC results. The characterization protocol for the 3D-printed MAB structures included a visual inspection of the plates to rule out any samples that had spalled or delaminated, optical microscopy to document surface features, porosity, and decomposition, and cleaning of the plates using an ultrasonic bath in preparation for SEM, EDS, and profilometry analyses.

MAB Phase↗

Continuing Studies in Support of Ultraviolet Observations of Planetary Atmospheres

This program was a one-year extension of an earlier Planetary Atmospheres program grant, covering the period 1 August 1996 through 30 September 1997. The grant was for supporting work to complement an active program observing planetary atmospheres with Earth-orbital telescopes, principally the Hubble Space Telescope (HST). The recent concentration of this work has been on HST observations of Jupiter's upper atmosphere and aurora, but it has also included observations of Io, serendipitous observations of asteroids, and observations of the velocity structure in the interplanetary medium. The observations of Jupiter have been at vacuum ultraviolet wavelengths, including imaging and spectroscopy of the auroral and airglow emissions. The most recent HST observations have been at the same time as in situ measurements made by the Galileo orbiter instruments, as reflected in the meeting presentations listed below. Concentrated efforts have been applied in this year to the following projects: The analysis of HST WFPC 2 images of Jupiter's aurora, including the Io footprint emissions. We have performed a comparative analysis of the lo footprint locations with two magnetic field models, studied the statistical properties of the apparent dawn auroral storms on Jupiter, and found various other repeated patterns in Jupiter's aurora. Analysis and modeling of airglow and auroral Ly alpha emission line profiles from Jupiter. This has included modeling the aurora] line profiles, including the energy degradation of precipitating charged particles and radiative transfer of the emerging emissions. Jupiter's auroral emission line profile is self-absorbed, since it is produced by an internal source, and the resulting emission with a deep central absorption from the overlying atmosphere permits modeling of the depth of the emissions, plus the motion of the emitting layer with respect to the overlying atmospheric column from the observed Doppler shift of the central absorption. By contrast the airglow emission line, which is dominated by resonant scattering of solar emission, has no central absorption, but displays rapid time variations and broad wings, indicative of a superthermal component (or corona) in Jupiter's upper atmosphere. Modeling of the observed motions of the plumes produced after the impacts of the fragments of Comet S/L-9 with Jupiter in July 1994, from the HST WFPC 2 imaging series.

Clark, John↗

Preconditioning of overcast-to-broken cloud transitions by riming in marine cold air outbreaks

Marine cold air outbreaks (CAOs) commonly form overcast cloud decks that transition into broken cloud fields downwind, dramatically altering the local radiation budget. In this study, we investigate the impact of frozen hydrometeors on these transitions. We focus on a CAO case in the NW Atlantic, the location of the multi-year flight campaign ACTIVATE (Aerosol Cloud meTeorology Interactions oVer the western ATlantic Experiment). We use MERRA-2 (Modern-Era Retrospective analysis for Research and Applications, version 2) reanalysis fields to drive large eddy simulations with mixed-phase two-moment microphysics in a Lagrangian framework. We find that transitions are triggered by substantial rain (rainwater paths >25 g m−2), and only simulations that allow for aerosol depletion result in sustained breakups, as observed. Using a range of diagnostic ice nucleating particle concentrations, Ninp, we find that increasing ice progressively accelerates transitions, thus abbreviating the overcast state. Ice particles affect the cloud-topped boundary layer evolution, primarily through riming-related processes prior to substantial rain, leading to (1) a reduction in cloud liquid water, (2) early consumption of cloud condensation nuclei, and (3) early and light precipitation cooling and moistening below cloud. We refer to these three effects collectively as “preconditioning by riming”. Greater boundary layer aerosol concentrations available as cloud condensation nuclei (CCN) delay the onset of substantial rain. However, cloud breakup and low CCN concentration final stages are found to be inevitable in this case, due, primarily, to liquid water path buildup. An ice-modulated cloud transition speed suggests the possibility of a negative cloud–climate feedback. To address prevailing uncertainties in the model representation of mixed-phase processes, the magnitude of ice formation and riming impacts and, thereby, the strength of an associated negative cloud–climate feedback process, requires further observational evaluation by targeting riming hot spots with in situ imaging probes that allow for both the characterization of ice particles and abundance of supercooled droplets.

Marine cold air outbreaks↗

Effect of aluminum phosphate additions on composition of three-component plasma-sprayed solid lubricant

Image analysis (IA) and electron microprobe X-ray analysis (EMXA) were used to characterize a plasma-sprayed, self-lubricating coating, NASA LUBE PS106, specified by weight percent as 35NiCr-35Ag-30CaF2. To minimize segregation of the powder mixture during the plasma-spraying procedure, monoaluminum phosphate was added to form agglomerate particles. Three concentrations of AlPO4 were added to the mixtures: 1.25, 2.5, and 6.25 percent by weight. Analysis showed that 1.25 wt% AlPO4 yielded a CaF2 deficiency, 2.5 wt% kept the coating closest to specification, and 6.25 wt% yielded excess CaF2 as well as more impurities and voids and a deficiency in silver. Photomicrographs and X-ray maps are presented. The methods of IA and EMXA complement each other, and the reasonable agreement in the results increases the confidence in determining the coating composition.

Jacobson, T. P.↗

Extended atmospheres of outer planet satellites and comets

In the third year of this 3-year project, research accomplishments are discussed and related to the overall objective. In the area of the distribution of hydrogen in the Saturn system, new Voyager UVS data have been discovered and are discussed. The data suggest that both Titan's hydrogen torus and Saturn's hydrogen corona play a major role in the circumplanetary gas source. Modeling analysis of this new data establishes a strong basis for continuing studies to be undertaken in a new NASA-sponsored project. In the area of the cometary atmospheres, observational data for H, O, C, and OH acquired with the Pioneer Venus Orbiter are evaluated and preliminary modeling analysis for some of the hydrogen Lyman-alpha data is presented. In addition, the importance of collisional thermalization in spatial properties and structure of the inner and extended comae of comets has been demonstrated using the recently developed particle trajectory model. The successful simulation by this model of the hydrogen Lyman-alpha image for Comet Kohoutec near perihelion, an extreme case for collisional thermalization, is particularly noteworthy.

Smyth, William H.↗

ELM: Europa Luminescence Microscope

The Europa Luminescence Microscope (ELM) is an automated fluorescence and bright-field microscope designed to meet key objectives defined in the 2016 NASA Europa Lander Study Report, including the identification and characterization of morphological biosignatures. ELM’s heritage stems from a 2U cubesat fluorescence microscope, the Fluorescence Analysis for In situ Research imager, designed and built at NASA Ames Research Center, for the autonomous study of microbial biology in low Earth orbit. For ELM implementation, a sample is autonomously manipulated with a microfluidic system using in-line 10, 1.0, and 0.2 μm pore-size filters to capture successively smaller particles for imaging. For bright-field imaging, ELM uses deep-ultraviolet, ultraviolet and visible light to image organic and inorganic structures with submicron resolution. The ability to detect biosignatures as small as 0.2 μm in size is achieved by imaging native fluorescence and using fluorescence microscopy stains to identify key structural and functional indicators of microbial life (proteins, lipids, nucleic acids). For fluorescence imaging, ELM uses 265, 370, 470, and 530 nm LEDs with five emission bands. The use of multiple excitation and emission wavelengths for native fluorescence imaging enables the detection of a wide range of molecular species and their rough classification. Excitation at 265 nm allows for the detection of smaller polycyclic aromatic hydrocarbons (PAH), aromatic amino acids, and proteins with little to no interference from mineral fluorescence, given proper emission band selection. 370 and 470 nm light excites increasingly larger PAH structures and larger aromatic biomolecules that may be present (e.g., protective pigments). Similarly, inorganic fluorescence can be characterized and separated from organic fluorescence, allowing the recognition and in some cases classification, of minerals and other abiotic particles. ELM is based upon work supported by the NASA COLDTech and ICEE-2 programs.

Richard C Quinn↗