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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 217 records · Page 12

All sources NASA NTRS DOE OSTI

NASA NTRS1970

A Study of the Electrotransport in Thin Films: An Advanced Method for the Study of Electrotransport in Thin Films Using Electrical Resistance Measurements

To date, very little is understood about electrotransport in thin films. One reason for this is the lack of methods in which electromigration can be adequately monitored dynamically. In this thesis, a new nondestructive method for the study of the electrotransport phenomenon in thin aluminum films is presented. This method makes use of electrical resistance measurements of various regions along the test sample to monitor changes in resistance resulting from electromigration. The advantage of this method is that resistance changes can be observed long before void formation can be seen using standard microscopy methods. In order to achieve the best efficiency using this method, special consideration must be given to the design of the sample. Design problems and their respective solutions are given. The results of the electrical resistance measurements are interpreted by means of photographs taken with an scanning electron microscope. The increase in resistance of the aluminum samples is interpreted to be due to void formation. The expected decrease in resistance near the anode was never observed. It is shown that mass accumulation takes on the form of hillocks and whiskers on the surface of the aluminum film, which does not contribute appreciably to conductivity.

Hummel, R. E.↗

NASA NTRS1972

Superconducting rock magnetometer system

A three axis magnetometer system intended for use in the magnetic measurement of lunar rock samples was designed, fabricated and delivered to NASA Manned Spacecraft Center. The system has a four inch diameter room temperature sample access region and is fitted with three orthogonal magnetic field sensors enclosing this region. Two superconducting magnetic shields are incorporated, which are designed to eliminate external magnetic noise from the sense coils. A superconducting solenoid is mounted coaxially with the sample region and this provides axial magnetic fields up to 1,000 gauss. The system was designed for measuring magnetic moments of geophysical samples, especially remanent moments of lunar samples. The sensitivity of the system in all three axes is about 2 x 10 to the -7th power EMU square root HZ peak to peak, measured in the 0 to 1 Hz bandwidth.

Source record↗

NASA NTRS2017

Development of NASA's Sample Cartridge Assembly: Summary of GEDS Design, Development Testing, and Thermal Analyses

Outline: Background of ISS (International Space Station) Material Science Research Rack; NASA SCA (Sample Cartridge Assembly) Design; GEDS (Gravitational Effects in Distortion in Sintering) Experiment Ampoule Design; Development Testing Summary; Thermal Modeling and Analysis. Summary: GEDS design development challenging (GEDS Ampoule design developed through MUGS (Microgravity) testing; Short duration transient sample processing; Unable to measure sample temperatures); MUGS Development testing used to gather data (Actual LGF (Low Gradient Furnace)-like furnace response; Provided sample for sintering evaluation); Transient thermal model integral to successful GEDS experiment (Development testing provided furnace response; PI (Performance Indicator) evaluation of sintering anchored model evaluation of processing durations; Thermal transient model used to determine flight SCA sample processing profiles).

O'Connor, Brian↗

NASA NTRS2019

Initial Developments of a Low Drag Variable Depth Acoustic Liner

The purpose of this study is to assess the acoustic performance and relative drag of a new type of variable depth liner containing pairs of resonators coupled together by shared inlet volumes just below the facesheet. This type of liner has the potential to achieve a targeted impedance with fewer openings in the facesheet, and therefore less drag, than previous designs. To better understand the limitations of the concept, three sets of samples were designed and tested in the NASA Langley normal incidence and grazing flow impedance tubes. Each set of samples consisted of a baseline variable depth liner with straight chambers, and a prototype liner with shared inlet volumes. Measurements conducted in both the normal incidence and grazing flow impedance tubes confirm that the prototype liner can achieve the same impedance as the baseline variable depth liner at discrete frequencies with 50% less open area. This results in a 75% reduction in the drag penalty relative to the baseline design. The proposed concept is not, however, able to achieve a flat, broadband impedance as effectively as the baseline liner. So, while the proposed concept is well suited for multitonal design metrics, tradeoffs must be made between liner drag and acoustic performance when broadband attenuation is required.

Schiller, Noah H.↗

DOE OSTI2025

Physical Testing of The PSEC5 ASIC

The PSEC5 ASIC is a high-speed waveform sampling chip designed for ultra-fast timing detectors, offering up to 40 GSPS sampling with 10-bit resolution. This makes it well-suited for applications requiring fine time resolution, such as MCPs and LGADs. This work focuses on the physical testing and validation of the chip s internal clocking and SPI-controlled registers. Testing began with inspection of schematics and the prototype to identify and resolve design issues. Then, custom firmware was developed for an Arduino controller to interface with the chip via SPI, enabling read and write access to key control registers. Results confirm that the VCO operates between ~3.2 4.0 GHz and remains stable under non-VCOVDD fluctuations. The Division Ratio register enables frequency division by known factors (256, 128, 64, etc.), indicating a pre-division frequency of 3.2 GHz when the digital band is unmodified. While most registers responded correctly, some issues were observed, including unexpected current draw and unstable discriminator behavior. Overall, the chip shows promising functionality, but further work is needed to understand the state of the read only registers and address the existing issues. Continued testing and firmware development will be critical to ensuring reliable integration into detector systems.

Fahey, Alexander [Unlisted, US]↗

NASA NTRS1983

Terminal area automatic navigation, guidance and control research using the Microwave Landing System (MLS). Part 5: Design and development of a Digital Integrated Automatic Landing System (DIALS) for steep final approach using modern control techniques

The design and development of a 3-D Digital Integrated Automatic Landing System (DIALS) for the Terminal Configured Vehicle (TCV) Research Aircraft, a B-737-100 is described. The system was designed using sampled data Linear Quadratic Gaussian (LOG) methods, resulting in a direct digital design with a modern control structure which consists of a Kalman filter followed by a control gain matrix, all operating at 10 Hz. DIALS uses Microwave Landing System (MLS) position, body-mounted accelerometers, as well as on-board sensors usually available on commercial aircraft, but does not use inertial platforms. The phases of the final approach considered are the localizer and glideslope capture which may be performed simultaneously, localizer and steep glideslope track or hold, crab/decrab and flare to touchdown. DIALS captures, tracks and flares from steep glideslopes ranging from 2.5 deg to 5.5 deg, selected prior to glideslope capture. Digital Integrated Automatic Landing System is the first modern control design automatic landing system successfully flight tested. The results of an initial nonlinear simulation are presented here.

Halyo, N.↗

NASA NTRS2014

Development of Genesis Solar Wind Sample Cleanliness Assessment: Initial Report on Sample 60341 Optical Imagery and Elemental Mapping

Since 2005 the Genesis science team has experimented with techniques for removing the contaminant particles and films from the collection surface of the Genesis fragments. A subset of ~40 samples have been designated as "cleaning matrix" samples. These are small samples to which various cleaning approaches are applied and then cleanliness is assessed optically, by TRXRF, SEM, ToF-SIMS, XPS, ellipsometry or other means [1-9]. Most of these sam-ples remain available for allocation, with cleanliness assessment data. This assessment allows evaluation of various cleaning techniques and handling or analytical effects. Cleaning techniques investigated by the Genesis community include acid/base etching, acetate replica peels, ion beam, and CO2 snow jet cleaning [10-16]. JSC provides surface cleaning using UV ozone exposure and ultra-pure water (UPW) [17-20]. The UPW rinse is commonly used to clean samples for handling debris between processing by different researchers. Optical microscopic images of the sample taken before and after UPW cleaning show what has been added or removed during the cleaning process.

Gonzalez, C. P.↗

NASA NTRS2017

Automated Sensitivity Analysis of Interplanetary Trajectories for Optimal Mission Design

This work describes a suite of Python tools known as the Python EMTG Automated Trade Study Application (PEATSA). PEATSA was written to automate the operation of trajectory optimization software, simplify the process of performing sensitivity analysis, and was ultimately found to out-perform a human trajectory designer in unexpected ways. These benefits will be discussed and demonstrated on sample mission designs.

trajectory design↗

NASA NTRS2017

Automated Sensitivity Analysis of Interplanetary Trajectories

trajectory design↗

NASA NTRS2021

Optimal Experimental Design With Fast Neural Network Surrogate Models

Designing optimal experiments minimizes the uncertainty of results and maximizes the efficient use of resources. Herein, machine learning surrogate models and the approximate coordinate exchange (ACE) algorithm are used to determine optimum experimental designs over large or arbitrarily restrictive design spaces. Optimal experimental design is particularly salient in materials science where experiments are expensive and material properties must often be inferred indirectly. The proposed framework is demonstrated by finding optimal experiments with which the hidden constituent properties of composite materials can be most efficiently inferred from observable experimental outcomes. The optimum experimental design is given by an information-theoretic criteria, which maximizes the conditional mutual information between the hidden properties and the expected experimental outcomes. To perform tractable optimization a neural network is trained as a surrogate model to mimic a physics based simulation, which can calculate the expected experimental outcome based on a candidate experimental design and sampled constituent properties. The ACE algorithm is used to optimize over large design spaces with many tests and controlled parameters where an exhaustive search would be intractable even with the surrogate model. Using this approach, optimal experimental designs that are consistent with those produced by heuristic knowledge and established best practices are found; then optimal designs in larger design spaces where heuristic knowledge is unavailable are examined.

machine learning↗

NASA NTRS2019

Implementing CubeSat Avionics Components to Full-Scale Capsule Return Missions

Returning samples from Low Earth Orbit (LEO) is no simple task. Whether the samples are scientific experiments or surveillance footage, engineers must overcome many challenges to achieve mission success. In August of 1960 the first payload recovered from LEO, the Corona capsule, carried “more photographic coverage of the Soviet Union than all previous U-2 missions”. The Corona program proved that re-turning surveillance footage from LEO is possible, the program is still referenced today when designing new sample return missions. Although there are many crucial subsystems that make up a sample return capsule, the avionics subsystem demands the most attention. This paper will discuss how current CubeSat avionics components can be applied to large sample return missions. One advantage of using CubeSat avionics components is that they can fit into a 1.5 U (10x10x15 cm) compartment, leaving more room for the payload. This paper is broken down as follows. First, the reader is introduced to the history of sample return projects. The major design strengths of previous projects are analyzed and applied to the current capsule design. Next, the typical trajectory of a capsule is presented along with mission requirements and operations. During the re-entry phase, the avionics subsystem is responsible for commanding the deployment of the parachute, back shell, and the heat shield. Next, the power subsystem is discussed in detail including a trade study on batteries and voltage regulators. Next, the interface between the Ground Support Equipment (GSE) and the avionics components is discussed. It is important that the capsule is able to provide avionics system state of health to ensure proper functionality before the capsule is launched. Next, an in-depth analysis of current TechEdSat avionics components, with proven flight history, are presented. The various avionics components including the radios, GPS, IMU, temperature sensors, altitude sensors, and ejectors are discussed. The application of cur-rent avionics components to a sample return projects are analyzed. After, the wiring diagram is presented along with a discussion of the design. Next, a summary of how the avionics components are tested and validated is pro-vided. Finally, this article will present current sample return missions TechEdSat avionics components are being applied to. CubeSat Avionics can be applied to almost all sample return missions due to their compact configuration and proven space flight heritage. The TechEdSat team is currently making great progress in returning samples from the International Space Station (ISS) and is excited to present how their avionics components can be applied to a full-scale sample return mission.

Hughes, Z. M.↗

NASA NTRS1992

Microgravity ignition experiment

The purpose of this project is to develop a flight ready apparatus of the microgravity ignition experiment for the GASCan 2 program. This involved redesigning, testing, and making final modifications to the existing apparatus. The microgravity ignition experiment is intended to test the effect of microgravity on the time to ignition of a sample of alpha-cellulose paper. An infrared heat lamp is used to heat the paper sample within a sealed canister. The interior of the canister was redesigned to increase stability and minimize conductive heat transfer to the sample. This design was fabricated and tested and a heat transfer model of the paper sample was developed.

Motevalli, Vahid↗

NASA NTRS2009

Quick-Connect Windowed Non-Stick Penetrator Tips for Rapid Sampling

Standard penetrator sampling systems were designed in order to allow for sampling via penetrators to produce a full set of sample acquisitions including volatile liquids, fine powders, and solid fragments. A gravity harpoon sampler has been designed with a removable tip and a quick coupling. The separation allows for sample handling and eliminates sample cross-contamination. Also, this design allows for multiple use of the penetrator body, which is the largest and heaviest part of the penetrator, while allowing for multiple changes of the light-mass, penetrator tip to avoid sample cross-contamination. The penetrator tip design has been improved by adding a spring trap to retain the sample, as well as a means for connecting to a quick coupling. Quick connect tips have been demonstrated in a sample handling carousel. The penetrator was released and rewound and the tips were released into a circular platter for rotation into instrument stations. The pyro-harpoon sampler was fabricated and tested with a NASA Standard Initiator (NSI) pyrotechnic charge. Initial tests collected cryogenic ice, but removal of the small pyro-harpoon from the ice was difficult. A brass metal sheath was then fitted over the harpoon tip, and removal from the ice was greatly alleviated by leaving the sheath in the ice. Quartz windows in the tips allow direct optical and spectral imaging and gas chromatography-mass spectrometer (GCMS) pyrolysis, and were found to survive impact. All systems were successfully tested by dropping into sand and into cryogenic ice.

Sherritt, Stewart↗

DOE OSTI2025

Autonomous organic synthesis for redox flow batteries via flexible batch Bayesian optimization

Traditional trial-and-error methods for materials discovery are inefficient to meet the urgent demands posed by the rapid progression of climate change. This urgency has driven the increasing interest in integrating robotics and machine learning into materials research to accelerate experimental learning. However, idealized decision-making frameworks to achieve maximum sampling efficiency are not always compatible with high-throughput experimental workflows inside a laboratory. For multi-step chemical processes, differences in hardware capacities can complicate the digital framework by introducing constraints on the maximum number of samples in each step of the experiment, hence causing varying batch sizes in variable selection within the same batch. Therefore, designing flexible sampling algorithms is necessary to accommodate the multi-step synthesis with practical constraints unique to each high-throughput workflow. In this work, we designed and employed three strategies on a high-throughput robotic platform to optimize the sulfonation reaction of redox-active molecules used in flow batteries. Our strategies adapt to the multi-step experimental workflow, where their formulation and heating steps are separate, causing varying batch size requirements. By strategically sampling using clustering and mixed-variable batch Bayesian optimization, we were able to iteratively identify optimal conditions that maximize the yields. Our work presents a flexible approach that allows tailoring the machine learning decision-making to suit the practical constraints in individual high-throughput experimental platforms, followed by performing resource-efficient yield optimization using available open-source Python libraries.

Tamura, Clara [Univ. of Washington, Seattle, WA (U↗

DOE OSTI2025

Identifying Missing Quasars from the DESI Bright Galaxy Survey

The Dark Energy Spectroscopic Instrument (DESI) cosmology survey includes a Bright Galaxy Survey (BGS), which will yield spectra for over 10 million bright galaxies (r < 20.2 AB mag). The resulting sample will be valuable for both cosmological and astrophysical studies. However, the star/galaxy separation criterion implemented in the nominal BGS target selection algorithm excludes quasar host galaxies in addition to bona fide stars. While this excluded population is comparatively rare (∼3–4 per square degrees), it may hold interesting clues regarding galaxy and quasar physics. Therefore, we present a target selection strategy that was implemented to recover these missing active galactic nuclei (AGN) from the BGS sample. The design of the selection criteria was both motivated and confirmed using spectroscopy. The resulting BGS-AGN sample is uniformly distributed over the entire DESI footprint. According to DESI survey validation data, the sample comprises 93% quasi-stellar objects (QSOs), 3% narrow-line AGN or blazars with a galaxy contamination rate of 2%, and a stellar contamination rate of 2%. Peaking around redshift z = 0.5, the BGS-AGN sample is intermediary between quasars from the rest of the BGS and those from the DESI QSO sample in terms of redshifts and AGN luminosities. The stacked spectrum is nearly identical to that of the DESI QSO targets, confirming that the sample is dominated by quasars. We highlight interesting small populations reaching z > 2, which are either faint quasars with nearby projected companions or very bright quasars with strong absorption features including the Lyα forest, metal absorbers, and/or broad absorption lines.

79 ASTRONOMY AND ASTROPHYSICS↗

NASA NTRS2011

Improving the Acquisition and Management of Sample Curation Data

This paper discusses the current sample documentation processes used during and after a mission, examines the challenges and special considerations needed for designing effective sample curation data systems, and looks at the results of a simulated sample result mission and the lessons learned from this simulation. In addition, it introduces a new data architecture for an integrated sample Curation data system being implemented at the NASA Astromaterials Acquisition and Curation department and discusses how it improves on existing data management systems.

Todd, Nancy S.↗

NASA NTRS1994

An unmanned mission to Mars with sample collection and in-situ resource utilization

The design for the Mars Analysis and Return Vehicle with In-Situ Resource Utilization (MARVIN) project is outlined. The MARVIN mission is designed to collect samples of the Martian environment; to produce fuel from local Martian resources; and to use the fuel produced to return the samples to earth. It uses only existing technologies. Exploratory Technologies' mission-design efforts have focused on methods of orbit determination, sample collection, fuel production, power, communications, control, and structural design. Lambert Targeting provided Delta-V's, launch dates, and travel times. The landing site is the Tharsis Plateau, to the southeast of Olympus Mons, chosen for its substantial scientific value. Samples of soil, dust, and atmosphere are collected with lander-based collection devices: the soil sample, with a robotic arm similar to those used in the Viking missions; the atmospheric sample, from a bleed line to the compressor in the fuel-production facility; a dust sample, from the dust-collection container in the fuel-production facility; and a redundant dust sample, with a with a passive filter system, which relies upon neither a power source nor other collection methods. The sample-return capsule (SRC) houses these samples, which are triply contained to prevent contamination. Proven technology can be used to produce methane and oxygen for fuel with relative ease at the landing site: the Sabatier reactor produces methane and water by combining carbon dioxide and hydrogen (brought from earth); the Reverse Water-Gas Shift unit combines carbon dioxide and hydrogen to form carbon monoxide and water; a water-electrolysis unit splits the water into hydrogen and oxygen. The Mars-lander vehicle (MLV) transports the equipment from earth to Mars. The Mars-ascent vehicle (MAV) contains the SRC and the engine, which is the same for both the MLV and the MAV. All equipment that is unnecessary for the Mars-Earth trajectory remains on Mars. This report presents detailed sizing information, for which a spreadsheet has been developed. The trends suggest possibilities for expansion, and suggestions for future work in these areas are offered.

Source record↗

DOE OSTI2026

Bias-Modulated ALD of ZnO: Insights into Precursor-Surface Interactions for ZnO Films

Atomic layer deposition (ALD) is widely used to deposit conformal thin films but is often limited in the tunability of the resulting material’s properties. Substrate bias and electric fields alter precursor-surface interactions and provide means to tune material properties. To explore this, we performed zinc oxide (ZnO) ALD using diethylzinc (DEZ) and water on silicon native oxide substrates at 150 °C in a sample holder designed to create a static electrical field by biasing one plate of a parallel plate capacitor-style sample holder during deposition. ZnO films prepared in an electric field/on a biased sample holder were thinner, changed relative crystalline composition, and contained more carbon compared to samples grown in identical sample holders without bias. The thickness was independent of the magnitude of the eletric field between plates, indicating that the primary driver for the change was substrate biasing not the electric field between plates of the parallel plate capacitor-style sample holder. Density functional theory calculations showed enhanced electron migration between dissociatively adsorbed DEZ molecules and the ZnO (002) facet with increasing force from an electric field at the substrate surface, which strengthens the electronic interactions between the surface and the adsorbate. These models offer a compelling explanation for the inhibited growth, changes in the crystallinity, and increase in carbon content of films grown in an electric field/on biased plates.

Jones, Jessica C. (ORCID:0000000174754620)↗