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At least 217 records · Page 12

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DOE OSTI2022

Many-Body Collective Neutrino Oscillations: Recent Developments

Neutrino flavor transformations in core-collapse supernovae and binary neutron star mergers represent a complex and unsolved problem that is integral to our understanding of the dynamics and nucleosynthesis in these environments. The high number densities of neutrinos present in these environments can engender various collective effects in neutrino flavor transformations, driven either by neutrino-neutrino coherent scattering, or in some cases, through collisional (incoherent) interactions. An ensemble of neutrinos undergoing coherent scattering among themselves is an interacting quantum many-body system -- as such, there is a tantalising prospect of quantum entanglement developing between the neutrinos, which can leave imprints on their flavor evolution histories. Here, in this study, we seek to summarize recent progress that has been made towards understanding this phenomenon.

Hypernuclei↗

DOE OSTI2017

Silk I and Silk II studied by fast scanning calorimetry

Using fast scanning calorimetry (FSC), we investigated the glass transition and crystal melting of samples of B. mori silk fibroin containing Silk I and/or Silk II crystals. Due to the very short residence times at high temperatures during such measurements, thermal decomposition of silk protein can be significantly suppressed. FSC was performed at 2000 K/s using the Mettler Flash DSC1 on fibroin films with masses around 130–270 ng. Films were prepared with different crystalline fractions (ranging from 0.26 to 0.50) and with different crystal structures (Silk I, Silk II, or mixed) by varying the processing conditions. These included water annealing at different temperatures, exposure to 50% MeOH in water, or autoclaving. The resulting crystal structure was examined using wide angle X-ray scattering. Degree of crystallinity was evaluated from Fourier transform infrared (FTIR) spectroscopy and from analysis of the heat capacity increment at the glass transition temperature. Silk fibroin films prepared by water annealing at 25 °C were the least crystalline and had Silk I structure. FTIR and FSC studies showed that films prepared by autoclaving or 50% MeOH exposure were the most crystalline and had Silk II structure. Intermediate crystalline fraction and mixed Silk I/Silk II structures were found in films prepared by water annealing at 37 °C. FSC results indicate that Silk II crystals exhibit endotherms of narrower width and have higher mean melting temperature Tm(II) = 351 ± 2.6 °C, compared to Silk I crystals which melt at Tm(I) = 292 ± 3.8 °C. Films containing mixed Silk I/Silk II structure showed two clearly separated endothermic peaks. Evidence suggests that the two types of crystals melt separately and do not thermally interconvert on the extremely short time scale (0.065 s between onset and end of melting) of the FSC experiment.

59 BASIC BIOLOGICAL SCIENCES↗

DOE OSTI2020

Fast GPU 3D diffeomorphic image registration

3D image registration is one of the most fundamental and computationally expensive operations in medical image analysis. Here, we present a mixed-precision, Gauss–Newton–Krylov solver for diffeomorphic registration of two images. Our work extends the publicly available CLAIRE library to GPU architectures. Despite the importance of image registration, only a few implementations of large deformation diffeomorphic registration packages support GPUs. Our contributions are new algorithms to significantly reduce the run time of the two main computational kernels in CLAIRE: calculation of derivatives and scattered-data interpolation. Additionally, we deploy (i) highly-optimized, mixed-precision GPU-kernels for the evaluation of scattered-data interpolation, (ii) replace Fast-Fourier-Transform (FFT)-based first-order derivatives with optimized 8th-order finite differences, and (iii) compare with state-of-the-art CPU and GPU implementations. As a highlight, we demonstrate that we can register clinical images in less than 6 s on a single NVIDIA Tesla V100. This amounts to over 20 speed-up over the current version of CLAIRE and over 30 speed-up over existing GPU implementations.

97 MATHEMATICS AND COMPUTING↗

DOE OSTI2017

Polyamorphism in Yb-based metallic glass induced by pressure

The Yb 62.5 Zn 15 Mg 17.5 Cu 5 metallic glass is investigated using synchrotron x-ray total scattering method up to 38.4 GPa. The polyamorphic transformation from low density to high density with a transition region between 14.1 and 25.2 GPa is observed, accompanying with a volume collapse reflected by a discontinuousness of isothermal bulk modulus. This collapse is caused by that distortional icosahedron short range order precedes to perfect icosahedron, which might link to Yb 4f electron delocalization upon compression, and match the result of in situ electrical resistance measurement under high pressure conditions. Furthermore, this discovery in Yb-based metallic glass, combined with the previous reports on other metallic glass systems, demonstrates that pressure induced polyamorphism is the general behavior for typical lanthanide based metallic glasses.

36 MATERIALS SCIENCE↗

DOE OSTI2016

A spatial light modulator that uses scattering in a cholesteric liquid crystal

When a cholesteric liquid crystal (helical pitch: 5 μm) was sandwiched between two glass plates with no alignment coating (gap: 20 μm), a random-domain texture appeared and a strong light scattering took place. This translucent texture turned to a transparent homeotropic phase when an electric voltage of 20 V was applied to the liquid crystal layer. This phase transition was used for constructing a spatial light modulator that needed no polarizers. Indium-tin-oxide electrodes (0.8 mm square) were arranged on a glass substrate to create a 20 × 20 pixel array (20 mm square). The liquid crystal was injected into a gap (20 μm thickness) between this substrate and another glass plate with a uniform electrode (ground). The transmittance of the pixels was originally below 10% and decreased to 0% by 7 V application because of increase in the scattering loss. As the voltage was raised, the transmittance increased gradually in the 7–17 V range and then rapidly in the 17–20 V range, attaining 40% at 27 V. Various transmittance distributions or gray-scale images were attainable by applying a suitable voltage (7–27 V) to each pixel. The transmission range of this spatial light modulator extended from ultraviolet (350 nm) to infrared wavelengths (>800 nm). Owing to this wide transmission range as well as capability of the polarizer-free operation, this spatial light modulator is useful to control a lamp spectrum in spectroscopic measurements.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2016

Electric dipole polarizability from first principles calculations

The electric dipole polarizability quantifies the low-energy behavior of the dipole strength and is related to critical observables such as the radii of the proton and neutron distributions. Its computation is challenging because most of the dipole strength lies in the scattering continuum. In our paper we combine integral transforms with the coupled-cluster method and compute the dipole polarizability using bound-state techniques. Furthermore, employing different interactions from chiral effective field theory, we confirm the strong correlation between the dipole polarizability and the charge radius, and study its dependence on three-nucleon forces. Finally, we find good agreement with data for the 4 He, 40 Ca, and 16 O nuclei, and predict the dipole polarizability for the rare nucleus 22 O.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗

DOE OSTI2021

Nonreciprocal Frequency Domain Beam Splitter

The canonical beam splitter—a fundamental building block of quantum optical systems—is a reciprocal element. It operates on forward- and backward-propagating modes in the same way, regardless of direction. The concept of nonreciprocal quantum photonic operations, by contrast, could be used to transform quantum states in a momentum- and direction-selective fashion. In this study, we demonstrate the basis for such a nonreciprocal transformation in the frequency domain through intermodal Bragg scattering four-wave mixing (BSFWM). Since the total number of idler and signal photons is conserved, the process can preserve coherence of quantum optical states, functioning as a nonreciprocal frequency beam splitter. We explore the origin of this nonreciprocity and find that the phase-matching requirements of intermodal BSFWM produce an enormous asymmetry ( 76 × ) in the conversion bandwidths for forward and backward configurations, yielding ~ 25 dB of nonreciprocal contrast over several hundred GHz. We also outline how the demonstrated efficiencies ( ~ 10 – 4 ) may be scaled to near-unity values with readily accessible powers and pumping configurations for applications in integrated quantum photonics.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

NASA NTRS1981

Wave direction measured by four different systems

A March 1977 wave direction measurement experiment is reported in which four systems were used to provide offshore wave-direction information: (1) synthetic aperture radar (SAR), (2) a coastal imaging radar, (3) an offshore pressure-gage array, and (4) aerial photography. From the coastal radar images and aerial photographs, the direction and length of the principal wavetrains were measured by a manual analysis. The SAR images were processed using fast Fourier transform to give two-dimensional wave spectra. Scatter diagrams are presented which intercompare the measurements of all four systems, and show good agreement among all imaging systems. It is concluded that aerial photography and SAR will prove more useful when wave measurements are needed over a large area or when there are rapidly changing wave characteristics.

Mattie, M. G.↗

NASA NTRS1981

Limiting cases of the small-angle scattering approximation solutions for the propagation of laser beams in anisotropic scattering media

The propagation of photons in a medium with strongly anisotropic scattering is a problem with a considerable history. Like the propagation of electrons in metal foils, it may be solved in the small-angle scattering approximation by the use of Fourier-transform techniques. In certain limiting cases, one may even obtain analytic expressions. This paper presents some of these results in a model-independent form and also illustrates them by the use of four different phase-function models. Sample calculations are provided for comparison purposes

Box, M. A.↗

NASA NTRS1986

Large reflector antenna study

In some applications, the wires used to construct the grids are plated over with highly conducting materials such as gold or silver. In those cases, depending on the frequency of operation, the coating may not be thick enough to prevent currents from flowing in the substrate. The conjugate gradient method, in conjunction with the fast Fourier transform is employed to solve the problem of scattering from such rectangular grids. An internal impedance is utilized to account for the effects of the substrate conductivity on the induced current densities. Calculated values of the reflection coefficient and induced currents from different coating thicknesses, angles of incidence and polarizations are presented and discussed.

Christodoulou, C. G.↗

NASA NTRS2012

Rainbow Fourier Transform

We present a novel technique for remote sensing of cloud droplet size distributions. Polarized reflectances in the scattering angle range between 135deg and 165deg exhibit a sharply defined rainbow structure, the shape of which is determined mostly by single scattering properties of cloud particles, and therefore, can be modeled using the Mie theory. Fitting the observed rainbow with such a model (computed for a parameterized family of particle size distributions) has been used for cloud droplet size retrievals. We discovered that the relationship between the rainbow structures and the corresponding particle size distributions is deeper than it had been commonly understood. In fact, the Mie theory-derived polarized reflectance as a function of reduced scattering angle (in the rainbow angular range) and the (monodisperse) particle radius appears to be a proxy to a kernel of an integral transform (similar to the sine Fourier transform on the positive semi-axis). This approach, called the rainbow Fourier transform (RFT), allows us to accurately retrieve the shape of the droplet size distribution by the application of the corresponding inverse transform to the observed polarized rainbow. While the basis functions of the proxy-transform are not exactly orthogonal in the finite angular range, this procedure needs to be complemented by a simple regression technique, which removes the retrieval artifacts. This non-parametric approach does not require any a priori knowledge of the droplet size distribution functional shape and is computationally fast (no look-up tables, no fitting, computations are the same as for the forward modeling).

Alexandrov, Mikhail D.↗

DOE OSTI2022

MENUS—Materials engineering by neutron scattering

Materials engineering by neutron scattering (MENUS) at the second target station will be a transformational high-flux, versatile, multiscale materials engineering diffraction beamline with unprecedented new capabilities for the study of complex materials and structures. It will support both fundamental and applied materials research in a broad range of fields. MENUS will combine unprecedented long-wavelength neutron flux and unique detector coverage to enable real-time studies of complex structural and functional materials under external stimuli. The incorporated small angle neutron scattering and transmission/imaging capabilities will extend its sensitivity to larger length scales and higher spatial resolution. Multimodal MENUS will provide crystallographic and microstructure data to the materials science and engineering community to understand lattice strain/phase transition/microstructure/texture evolution in three orthogonal directions in complex material systems under combined extreme applied conditions. Finally, the capabilities of MENUS will open new scientific opportunities and meet the research needs for science challenges to enable studies of a range of phenomena and answer the key questions in material design/exploration, advanced material processing, transformative manufacturing, and material operations of national impacts in our daily life.

47 OTHER INSTRUMENTATION↗

NASA NTRS2022

Characterization of Aerogel Scattering Filters for Astronomical Telescopes

We have developed a suite of novel infrared-blocking filters made by embedding scattering particles in a polymer aerogel substrate. Our developments allow us to tune the spectral performance of the filters based on both the composition of the base aerogel material and the properties of the scattering particles. Our filters are targeted for use in a variety of applications, from ground-based CMB experiments to planetary science probes. We summarize the formulations we have fabricated and tested to date, including several polyimide base aerogel formulations incorporating a range of size distributions of diamond scattering particles. We also describe the spectral characterization techniques used to measure the filters’ optical properties, including the development o fa mm-wave Fourier transform spectrometer testbed.

aerogel, filter, blocking, scattering, Fourier Tra↗

DOE OSTI2019

Pressure-Induced Transformations of Three-Component Heterostructural Nanocrystals with CdS–Au 2 S Janus Nanoparticles as Hosts and Small Au Nanoparticles as Satellites

Heterostructural nanocrystals (HNCs) have drawn enormous attention because of the combined and synergistic properties inherited from their individual components and interactions. In this paper, we design a three-component CdS-Au 2 S-Au Janus-satellite HNC to study the pressure process of HNC superlattices (HNC-SLs). In situ small/wide-angle X-ray scattering shows that the HNC-SLs can undergo structural transformations at both atomic and meso scales. At the same time, CdS-Au 2 S-Au Janus-satellite HNCs can morphologically transform into CdS-Au 2 S-Au heterotrimer HNCs through intraparticle migration and coalescence of Au satellites. Our results demonstrate that pressure can be employed as a clean and efficient way to fabricate complex heterostructural nanomaterials suitable for potential applications in photocatalysis and theranostics.

77 NANOSCIENCE AND NANOTECHNOLOGY↗

DOE OSTI2024

Massive twistor worldline in electromagnetic fields

We study the (ambi-)twistor model for spinning particles interacting via electromagnetic field, as a toy model for studying classical dynamics of gravitating bodies including effects of both spins to all orders. We compute the momentum kick and spin kick up to one-loop order and show precisely how they are encoded in the classical eikonal. The all-orders-in-spin effects are encoded as a dynamical implementation of the Newman-Janis shift, and we find that the expansion in both spins can be resummed to simple expressions in special kinematic configurations, at least up to one-loop order. We confirm that the classical eikonal can be understood as the generator of canonical transformations that map the in-states of a scattering process to the out-states. We also remark that cut contributions for converting worldline propagators from time-symmetric to retarded amount to the iterated action of the leading eikonal at one-loop order.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗

DOE OSTI2020

X-ray scattering signatures of early-time accelerations in iodine dissociation

Ultrafast time-resolved x-ray scattering (TRXS) from a photoexcited molecular ensemble measures a distribution $S(Q, τ)$ of the x-ray momentum transfer Q and pump-probe delay τ in which all modes of motion induced by the excitation overlap. Frequency-resolved x-ray scattering (FRXS) based on $\tilde {S}\left(Q,\omega \right)$ separates each oscillation and dissociation channel in the TRXS data, enabling measurements of vibrational frequencies and phases, and dissociation velocities and time shifts. In this work, we extend FRXS analysis to study early-time accelerations as well. We show how these appear as diffuse scattering patterns with characteristic phase evolution in FXRS and we develop a set of transformations that isolate individual channels to measure the early-time accelerated motion. This procedure is used to analyze diatomic iodine x-ray scattering data with multiple dissociations, and the ability of this technique to characterize early-time accelerations of one dissociation channel even in the presence of another dissociation is demonstrated.

74 ATOMIC AND MOLECULAR PHYSICS↗

DOE OSTI2019

Synergistic Doping and Intercalation: Realizing Deep Phase Modulation on MoS 2 Arrays for High-Efficiency Hydrogen Evolution Reaction

A synergistic N doping plus PO 4 3- intercalation strategy is used to induce high conversion (ca. 41%) of 2H-MoS 2 into 1T-MoS, which is much higher than single N doping (ca. 28 %) or single PO 4 3- intercalation ca. 10%). A scattering mechanism is proposed to illustrate the synergistic phase transformation from the 2H to the 1T phase, which was confirmed by synchrotron radiation and.spherical aberration TEM. To further enhance reaction kindies, the designed (N, PO 4 3- )-MoS 2 nanosheds are combined with conductive vertical graphene (VG) skeleton forming binder-free arrays fir high efficiencyhydrogen evolution reaction (HER). Owing 10 the decreased band gap, lower d-band censer, and smaller hydrogen adsorption/desorption energy, the designed (NPO 4 3- )-MoSJVG electrode shows excellent HER perfor mance with a lower Tafel slope and overpotential than N-MoS 2 /VG, PO 4 3- -MoS 2 /VG counterparts, and other Mo-base catalysts in the literature.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

DOE OSTI2026

Tuning the Mechanical Properties of Crosslinked Copolymers via Sequence and Solvent‐Selective Swelling for Vat Photopolymerization

Block copolymers (BCPs) offer distinct advantages for vat photopolymerization by enabling mechanically programmable network structures through microphase-separated morphologies that can be kinetically trapped during curing, yielding properties unattainable in homogeneous resins. However, the respective roles of repeat-unit sequence and solvent environment, together with their interplay in directing network formation and mechanical performance, remain unclear. Here, we synthesize a series of CO 2 -based polycarbonate copolymers comprising a crosslinkable glassy poly(vinyl cyclohexene carbonate) (PVCHC, A block) and a non-crosslinkable soft poly(propylene carbonate) (PPC, B block). The polymer sequence is systematically varied (ABA, BAB, and statistical), and solvent choice controls block-selective swelling to jointly control gelation behavior, microphase morphology, and mechanical response through changes in the accessibility and local environment of photocrosslinkable vinyl groups during network formation, as revealed by photorheology and small angle x-ray scattering. By tuning polymer sequence and curing solvent, we transform nominally identical formulations from brittle to highly ductile materials, achieving a three-orders-of-magnitude range in toughness (0.003 to 9.1 MJ m −3 ). These results establish clear structure–processing–property relationships and identify polymer sequence and selective solvation as powerful strategies for programming both printability and performance of block copolymer resins for additive manufacturing.

additive manufacturing↗