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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 235 records · Page 13
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NASA NTRSDate not supplied

Simulating Meteor Ablation at the Hypersonic Materials Environmental Test System

The ablation mechanisms of stony meteorite material and a terrestrial analog were investigated at the Hypersonic Materials Environmental Test System (HyMETS) facility at NASA’s Langley Research Center. The primary analyte (Tamdakht-H5) and arc-jet test conditions were chosen to simulate the entry of an ordinary chondrite through the Earth’s mesosphere. Basalt was selected to compare the meteorite response against material with enhanced polymerization and an elevated concentration of volatile species. The initial ablation process for each material commences with the vaporization of volatile species and germination of a viscous melt layer on the stagnation surface. However, each material exhibited distinct mass loss mechanisms, with basalt recessing at twice the rate of Tamdakht. Inspection of high-speed video and chemical analysis of the post-test melt layer suggests the dominant mode of mass loss of Tamdakht is expressed through the vaporization of volatile compounds. Vaporization rates of Tamdakht are 18x higher than basalt under the most severe test conditions which provides enhanced thermal shielding. Furthermore, Tamdakht produces a relatively stable melt flow, as evidenced by perpetual growth at the sidewall and the exiguous detachment of molten material into the flow. The ablation mechanism of basalt is markedly different from Tamdakht and is governed by volatile species in the virgin material. The dominant mode of mass loss for basalt is attributed to the detachment of large sections of the stagnation surface near the edge radius. An additional but subordinate mode of mass loss is assigned to the removal of melt flow as it passes over the edge radius, where shear forces overcome the rheological properties of the molten matter. Finally, mechanistic details will be discussed in terms of designing future test campaigns, developing meteorite-based materials response models, and impacting the broader scope of the Asteroid Threat Assessment Project (ATAP).

Meteor Ablation↗
NASA NTRSDate not supplied

Identification and Study of Validation Level Test Cases for Computational Modeling of Non-Charring Ablators

Computational modeling of Thermal Protection System (TPS) materials, used for aerospace applications, provides numerous advantages in preliminary selection and design of a heatshield material and shape for atmospheric entry vehicles. However, to serve as a reliable tool for prediction of material thermal and ablative behavior, the modeling approach needs to be validated against real experimental and flight data, preferably at a range of applied conditions. The validation study is typically very complex as it requires reliable measured data not only for the material thermal response and surface recession, but also well characterized environmental conditions. The validation problem becomes even more complex when the material thermal response is dictated by multi-physics effects such as solid conduction, in-depth thermal decomposition, pyrolysis gas flow and chemical reactions. The multi-physics effects complicate not only the modeling effort, but also the experimental measurement for validation of various aspects of the highly coupled problem. In this study, an attempt is made to identify suitable experimental data that could serve as a source for validation of material thermal response modeling tools. To reduce the computational complexity, this study focuses only on non-charring ablators, where the material thermal response could be modeled with a single governing equation for solid conduction and the ablation is limited only to the surface of the material. With a well characterized and publicly available experimental data being sparse, the study is limited in presenting test cases for only three materials: camphor, graphite and FiberForm® in the sequence of increased modeling complexity. Graphite is a commonly used TPS material for aerospace applications, both for leading edges of high-speed vehicles and internal insulation of solid rocket motors. FiberForm® is a porous carbon pre-form used in preparation of the well known PICA material Tran et al. [1996]. Inclusion of camphor into the list is conditioned with the relative simplicity in modeling the material thermal and chemical response and the low-enthalpy flow environment. In addition, camphor has been used as a simple test material for study of flow transition behavior by Stock and Ginoux [1973] and assessment of a heatshield shape change at flight relevant conditions by Rotondi et al. [2022]. In this work, the identified experimental data was extracted from the public literature and test cases that yet have been published. As it was found from the review, not a single test case contains an exhaustive set of data that would validate every aspect of the material physics. However, in the data collected, various aspects of the material behavior can be still validated, such as surface and in-depth temperature, amount of recession and a shape change. The identified experimental data for each case is accompanied with a characterized flow environment and simulated boundary conditions predicted by a Data-Parallel Line Relaxation (DPLR) code Wright et al. [1998]. In addition, material thermal response numerical simulations in each test case are performed with Kentucky Aerothermodynamics and Thermal Response System (KATS-MR) Zibitsker et al. [2022] providing a comparative study and a sanity check for the proposed validation data. Sample results from the performed numerical study are shown below. Figure 1 shows distribution of surface heat flux and pressure values on a hemi-cylinder model made of FiberForm® and tested in HyMETS arc-jet facility. The results are shown for the high pressure condition among the two tests. Flow simulation was performed with DPLR code on a quarter of original geometry. In the figure, the quarter shape was mirrored across zx and xy planes to show the complete distribution. Figure 2 shows the material response results for the high pressure case (7500 Pa), simulated with KATS-MR and a comparison to the experimental data for the surface temperature and shape shape. The simulation was performed on a 2-D slice, extracted in the xy plane at the middle of the sample. Figure 3 shows the material response simulation for the low pressure case (3500 Pa) and a comparison to the experimental data for surface temperature and shape change.

ablation↗
NASA NTRSDate not supplied

Material Response Analysis of PICA-NuSil at the Hypersonic Materials Environmental Test System

Phenolic impregnated carbon ablator (PICA) is a thermal protection system (TPS) that gained heritage during the Stardust mission and is the baseline TPS material for expeditions to Mars (e.g., Mars Science Laboratory and Mars 2020).1 PICA is friable; therefore, a polysiloxane resin (NuSil CV-1144-0) is deposited onto the surface of flight hardware before assembly, test, and launch operations (ATLO) to mitigate particle shedding. Furthermore, the Mars Science Laboratory (MSL) and Mars 2020 heatshields were instrumented with an array of thermocouple plugs (MEDLI Integrated Sensor Plugs or MISP) designed to measure the in-depth thermal response of PICA during flight. Post-flight analysis of MISP data suggests that recession was lower than predicted, and NuSil is suspected as a reasonable cause. NuSil primarily consists of a copolymer blend of dimethyl and diphenyl-substituted polysiloxane resin. Four decades of research in the field of polymer-derived ceramics demonstrate that polysiloxane resins form oxidation-resistant silicon oxycarbide materials at pyrolysis temperatures as low as 800 °C. -2 Furthermore, silicon oxycarbide materials exhibit excellent thermal stability at relatively high-temperatures (< 1200 °C) but eventually decompose via carbothermal reduction. -3 Therefore, it is reasonable to suggest that NuSil forms an oxidation-resistant thermal barrier coating on the TPS surface and influences the material response during atmospheric entry. Evidence for this notion was observed during prior arc-jet testing at both the Aerodynamic Heating Facility (AHF) and the Panel Test Facility (PTF) at the NASA Ames Research Center. Articles of PICA were subjected to testing in airflow, and a temperature discontinuity was recorded at the surface of coupons coated with NuSil. A glassy coating was observed to form at the surface in shear flow configurations (wedge and panel) under moderate heat fluxes. Furthermore, state-of-the-art material response models have yet to account for the underlying physics and chemistry of the temperature discontinuity. To this end, a pathfinder test campaign was executed at the Hypersonic Materials Environmental Test System (HyMETS) to enhance the fundamental understanding of PICA-NuSil ablation phenomena and provide a preliminary data set to aid in the development of material response models.

PICA↗
NASA NTRSDate not supplied

Development of Advanced Conformal and Soft Pica for Future Nasa Missions and Commercial Space

Phenolic Impregnated Carbon Ablator (PICA) is a low-density ablator that has been used as the planetary entry heatshield for several NASA missions since the late 90’s. Its low density and efficient performance characteristics have proven effective for use from Discovery to Flag-ship class missions, from Sample Return missions such as Stardust, OSIRIS-REx to large Mars Lander missions such as MSL and Mars 2020. Continued development of a more mass efficient and compliant versions of PICA that use a carbon felt as the substrate will be presented. The felt based versions of PICA known as Conformal PICA (C-PICA) and Soft PICA (S-PICA), are very comparable in terms of peak heat-flux capabilities compared to standard PICA. The lower density and of C-PICA and S-PICA further show a much higher thermal protection efficiency and hence more mass savings. The compliant nature of these materials allows for use on a wide variety of substrates and therefore makes it very attractive for commercial low earth orbit missions as well as NASA’s aerocapture missions to Ice Giants. NASA is currently working with several commercial partners (Varda and Inversion Space) to Technology Transfer C/S-PICA variants for commercial LEO missions. Thermal, mechanical, and representative environment arc-jet tests have been conducted comparing the performance of Conformal and Soft-PICA materials.

Matthew J Gasch↗
NASA NTRSDate not supplied

An Overview of Experiments in The Entry Systems Modeling Project

The Entry Systems Modeling (ESM) project has invested in experiments designed to enhance understanding of salient interactions between thermal protection materials (TPS) and mission-relevant planetary entry environments. An arc-jet campaign has been carried out at the Aerodynamic Heating Facility (AHF) to investigate the spallation of fiber particles as a function of gas composition and to measure the effect of pyrolysis gas flow on the in-depth temperature response of phenolic impregnated carbon ablator (PICA). Moreover, fundamental insights into the pyrolysis and oxidation mechanisms of the phenolic binding agent of FiberForm will be discussed. Finally, two new apparatus developed at NASA will be presented that were designed to interrogate phenomena associated with the production of gases and particles generated under simulated flight conditions.

Varcum↗
NASA NTRSDate not supplied

Simulating Ordinary Chondrite (Tamdakht) Ablation at the Hypersonic Materials Environmental Test System (HyMETS) Facility.

NASA’s Science Mission Directorate (SMD) created the Asteroid Threat Assessment Project (ATAP) to inform decision-makers of risks associated with Potentially Hazardous Objects (PHOs), which may pose an existential threat to human civilization. ATAP assesses risk, in part, by developing analytical physics-based damage models which draw upon data collected during material property characterization efforts, entry simulations, hazard simulations, and ground-based arc-jet testing. Therefore, a pathfinder test campaign was con-ducted at the Hypersonic Materials Environmental Test System (HyMETS) at the NASA Langley Re-search Center to investigate the ablation mechanisms of an ordinary chondrite (Tamdakht H5) and a terrestrial analog (basalt). The HyMETS facility is a 400 kW constricted arc heater used to screen material performance under simulated aerothermal conditions of hypersonic flow.1 Facility conditions were chosen to simulate Earth entry conditions be-tween the upper-mesosphere and the lower thermo-sphere. The ablation mechanisms of Tamdakht and bas-alt are illustrated with still images collected from high-speed video cameras (fig. 1, Tamdakht). Tamdakht produces a relatively stable melt flow, as evidenced by the perpetual growth of a flange at the sidewall and the exiguous detachment of molten material into the flow. Furthermore, an inspection of high-speed video and chemical analysis of the post-test melt layer suggests that the dominant mode of mass loss for Tamdakht, at these test conditions, is expressed through the vaporization of volatiles (e.g., iron, potassium, sodium, phosphorus, and sulfur). The vaporization rates of Tamdakht are greater than basalt under the most extreme test conditions, which leads to an enhanced blowing layer, in-creased thermal shielding, and reduced recession. The ablation mechanisms of basalt are markedly different from Tamdakht and are attributed to the presence of hydrated minerals dispersed at irregular intervals throughout the silicate matrix. Rapid de-composition of secondary minerals and the subsequent formation of water lead to the ejection of the subsurface and overlying melt layer. Furthermore, the presence of water is suspected of lowering the viscosity of the melt layer resulting in increased mass loss near the edge of the test article where drag forces overcome rheological properties (fig. 1, bas-alt). Finally, the results will be discussed in the broader context of meteorite-based material response model development and the potential impact on the Asteroid Threat Assessment Project (ATAP).

Brody K. Bessire↗
NASA NTRS2023

Coupled Fluid Dynamics and Material Response Simulations for Nitrogen High Enthalpy Flows

The study focuses on the interaction of nitrogen flows with thermal protection systems during atmospheric re-entry for NASA flight missions. The Ares multiphysics coupling tool is employed to investigate the coupling between the fluid (US3D) and material response (Icarus) solvers using various modeling approaches. These approaches include the equilibrium thin-film coefficients approach, a weakly coupled approach with temperature coupling, and an approach considering the full chemical composition of the surface and the transfer of pyrolysis gases. The objective is to understand and accurately represent the mechanisms of nitrogen interaction with the surface, such as nitridation and catalytic recombination. The study aims to assess the accuracy of the different approaches by comparing them to experimental results obtained from NASA arc-jet facilities. By addressing these challenges and improving the understanding of nitrogen-surface interactions, it is expected to enhance the design and performance analysis of thermal protection systems for future missions.

Ablation↗
NASA NTRSDate not supplied

Developments to the Ares Multi-Physics Framework

Increasingly challenging problems in Entry, Descent, and Landing (EDL) have motivated the development of a computational framework that encompasses the advances in high-fidelity modeling and a robust foundation for TPS design in a single software package. This is the objective of the Ares multi-physics solver which, to date, couples the US3D flow solver with Icarus (material response) and Nero (radiation), through detailed time-scale management, while also incorporating the physics of fluid-solid boundaries such as gas-surface interaction chemistry and shape change. Ares, which is currently in the development stage, is being assessed against a variety of EDL relevant problems such as arc-jet tests of varying geometries and materials (Figs. 1 and 2), the earth entry of MSR-EES and the Titan entry of Dragonfly. This presentation will focus on the findings to-date regarding development of the technology as well as its standing with respect to available experimental data and/or reference solutions.

CFD↗
NASA NTRSDate not supplied

Ares: A Coupling Methodology for Ablation Modeling

To enable modeling of complex and coupled ablation problems, a multi-physics framework is developed. A methodology for modeling shape change in coupled systems is presented. The approach taken to model gas-surface interactions and translate coupled surface phenomena to physically meaningful boundary conditions in the distinct solvers is discussed. Particular emphasis is placed on the nature of coupled boundary conditions pertaining to surface energy and mass balances as well as surface chemistry modeling. The developed methodology is used to simulate a shear test in arc-jet conditions in order to assess the validity of the coupled approach as well as the implementation of the relevant physical processes.

EDL↗
NASA NTRSDate not supplied

Ares: A Coupling Methodology for Ablation Modeling

To enable modeling of complex and coupled ablation problems, a multi-physics framework is developed. A methodology for modeling shape change in coupled systems is presented. The approach taken to model gas-surface interactions and translate coupled surface phenomena to physically meaningful boundary conditions in the distinct solvers is discussed. Particular emphasis is placed on the nature of coupled boundary conditions pertaining to surface energy and mass balances as well as surface chemistry modeling. The developed methodology is used to simulate a shear test in arc-jet conditions in order to assess the validity of the coupled approach as well as the implementation of the relevant physical processes.

EDL↗
NASA NTRS2011

Excited State Chemistry in the Free Stream of the NASA IHF Arc Jet Facility Observed by Emission Spectroscopy

Spectroscopic measurements of non-equilibrium emission were made in the free stream of the 60 megawatts Interaction Heating Facility at NASA Ames Research Center. In the visible near infrared wavelength region, the most prominent emission was from molecular N2, and in the ultra violet region, the spectra were dominated by emission from molecular NO. The only atomic lines observed were those of copper (an erosion product of the electrodes). The bands of the 1st Positive system of N2 (if B is true then A is true) differed significantly from spectra computed spectra assuming only thermal excitation, suggesting overpopulation of the high vibrational states of the B state of N2. Populations of these high vibrational levels (peaking at v (sub upper) equals 13) of the N2 B state were determined by scaling simulated spectra; calculations were performed for each upper vibrational state separately. The experimental-theoretical procedure was repeated for several radial positions away from the nozzle axis to obtain spatial distributions of the upper state populations; rotational symmetry of the flow was assumed in simulations. The overpopulation of the high vibrational levels has been interpreted as the effect of inverse pre-dissociation of neutral atoms in the N2 A state, which populates the N2 B state through a level crossing process at v (sub upper) is greater than 10.

arc-jet testing↗
NASA NTRSDate not supplied

CFD Simulations of the Truncated IHF Semi-Elliptical Nozzle Flow: Convective Calibration Plate

This paper reports computational simulations of a high-enthalpy panel test facility at NASA Ames Research Center. The recently developed facility configuration uses a truncated version of an existing semi-elliptical nozzle in the 60-MW Interaction Heating Facility, and it provides testing capability for panel test articles as large as 43.2 cm x 43.2 cm (17 in x 17 in). A water-cooled calibration plate, which is attached to the semi-elliptical nozzle bottom surface and instrumented with twenty Gardon-gage heat flux calorimeters and twelve pressure gages, is used to characterize the convective heating environment over the panel test articles. The present analysis comprises computational fluid dynamics simulations of the nonequilibrium flowfield in the facility nozzle and test box, and flowfield over panel test articles. Both laminar and turbulent simulations are performed, and the computational results are compared with the calibration plate measurements. Comparisons of computed and measured heat fluxes indicate that the boundary layer in the semi-elliptical nozzle is transitional at certain conditions (relatively higher arc-heater pressures or mass flow rates).

Arc-jets↗
NASA NTRSDate not supplied

CFD Simulations of the Truncated IHF Semi-Elliptical Nozzle Flow: Convective Calibration Plate

This paper reports computational simulations of a high-enthalpy panel test facility at NASA Ames Research Center. The recently developed facility configuration uses a truncated version of an existing semi-elliptical nozzle in the 60-MW Interaction Heating Facility, and it provides testing capability for panel test articles as large as 43.2 cm x 43.2 cm (17 in x 17 in). A water-cooled calibration plate, which is attached to the semi-elliptical nozzle bottom surface and instrumented with twenty Gardon-gage heat flux calorimeters and twelve pressure gages, is used to characterize the convective heating environment over the panel test articles. The present analysis comprises computational fluid dynamics simulations of the nonequilibrium flowfield in the facility nozzle and test box, and the flowfields over panel test articles. Both laminar and turbulent simulations are performed, and the computational results are compared with the calibration plate measurements. Comparisons of computed and measured heat fluxes indicate that the boundary layer in the semi-elliptical nozzle is transitional at certain conditions (relatively higher arc-heater pressures or mass flow rates).

Arc-jets↗
NASA NTRSDate not supplied

On Characterization of Laminar to Turbulent Transitional Flow in the Truncated IHF Semi-Elliptical Nozzle

This paper reports computational analysis and experimental data to characterize the laminar to turbulent flow transition in a high-enthalpy panel test facility at NASA Ames Research Center. The recently developed facility configuration uses a truncated version of an existing semi-elliptical nozzle in the 60-MW Interaction Heating Facility, and it provides testing capability for panel test articles as large as 43.2 cm x 43.2 cm (17 in x 17 in). A water-cooled calibration plate, which is attached to the semi-elliptical nozzle bottom surface and instrumented with twenty Gardon-gage heat flux calorimeters and twelve pressure gages, is used to characterize the convective heating environment over the panel test articles. The present analysis comprises computational fluid dynamics simulations of the nonequilibrium flowfield in the facility nozzle and test box, and the flowfields over panel test articles, and comparisons with the measured test data. Both laminar and turbulent simulations are performed. Constant current studies are performed: the measured data are grouped at the same arc current levels with varying mass flow rates, and they are compared with corresponding computations. For all currents studied, these studies indicate that the semi-elliptical nozzle flow is transitional at relatively higher mass flow rates within the facility operating envelope.

Arc-jets↗
NASA NTRSDate not supplied

On Characterization of Laminar to Turbulent Transitional Flow in the Truncated IHF Semi-Elliptical Nozzle

This paper reports computational analysis and experimental data to characterize the laminar to turbulent flow transition in a high-enthalpy panel test facility at NASA Ames Research Center. The recently developed facility configuration uses a truncated version of an existing semi-elliptical nozzle in the 60-MW Interaction Heating Facility, and it provides testing capability for panel test articles as large as 43.2 cm x 43.2 cm (17 in x 17 in). A water-cooled calibration plate, which is attached to the semi-elliptical nozzle bottom surface and instrumented with twenty Gardon-gage heat flux calorimeters and twelve pressure gages, is used to characterize the convective heating environment over the panel test articles. The present analysis comprises computational fluid dynamics simulations of the nonequilibrium flowfield in the facility nozzle and test box, and the flowfields over panel test articles, and comparisons with the measured test data. Both laminar and turbulent simulations are performed. Constant current studies are conducted: the measured data are grouped at the same arc current levels with varying mass flow rates, and they are compared with corresponding computations. For all currents considered, these studies indicate that the semi-elliptical nozzle flow is transitional at relatively higher mass flow rates within the facility operating envelope. An approximate facility map for the transitional flow characterization is developed, showing laminar and transitional to turbulent flow regions.

Arc-jets↗
NASA NTRSDate not supplied

Arc Jet Testing of 3D Mid-Density Carbon Phenolic (3MDCP) for Mars Sample Return

When accounting for the highest-heating trajectory with margin, dispersion, and greatest system mass, MSR-EES is predicted to experience the highest heat flux and pressure (approximately 3300 W/cm2 hot-wall, 200 kPa) of any earth entry vehicle todate. To verify performance requirements are met by the forebody TPS, the material must be tested to validate model predictions and give confidence to stakeholder’s expectation of performance. 3D Mid-Density Carbon Phenolic (3MDCP) is NASA’s baseline material for the forebody heatshield of the MSR-EES. As part of the arc jet campaign to evaluate material performance, recent testing has completed in the Interaction Heating Facility (IHF) using a new facility setting to achieve the necessary environments.

arcjet↗