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NASA NTRS2003

4-D Model of CO2 Deposition at North and South of Mars from HEND/Odyssey and MOLA/MGS

The first 1.5 year of neutron mapping measurements onboard Mars Odyssey spacecraft are presented based on High Energy Neutron Detector (HEND) observations. HEND instrument is a part of GRS suite responsible for registration of epithermal and fast neutrons originating in Mars subsurface layer. The scattering of fast neutrons in Mars surface caused by primary cosmic rays is strongly sensitive to presence of hydrogen atoms. Even several percents of subsurface water significantly depress epithermal and fast neutron flux. It turns orbit neutron spectroscopy into one of most efficient methods for finding distribution of subsurface water. The Mars Odyssey observations revealed huge water- ice regions above 60N and 60S latitudes. It was founded that distribution of subsurface water has layered structure at these regions. It is thought that more than 50% wt water ice covered by relatively dry layer with different thickness.

M L Litvak↗

NASA NTRS2003

Seasonal CO2 Observations on North and South of Mars as Seen by HEND (Mars Odyssey) and MOLA (MGS)

The first year of neutron mapping measurements from the Mars Odyssey spacecraft are presented based on observations from the High Energy Neutron Detector (HEND). The HEND instrument is a part of GRS suite responsible for registration of epithermal and fast neutrons originating in the Mars subsurface layer. The gamma ray and neutron spectrometers measure the scattering of fast neutrons from the Martian surface, which is caused by bombardment of primary cosmic rays and is strongly sensitive to the presence of hydrogen atoms. Even several percent subsurface hydrogen significantly depresses the flux of epithermal and fast neutrons. The recent Mars Odyssey observations detected a considerable amount of hydrogen, almost certainly corresponding to water ice, in the shallow near surface of the southern and northern hemispheres of Mars.

Litvak, M. L.↗

NASA NTRS2021

Electrolytic Co-deposition Neutron Production Evaluation

Co-deposition electrochemical cells are a simple means to examine novel nuclear reactions. In this study, palladium and deuterium atoms were co-deposited on a cathode at stoichiometric densities, forming dendritic morphologies. Bubble detector neutron dosimeters were used to measure equivalent dose levels during electrolytic deposition. Standard configuration cells expected to produce excess neutrons were denoted as experimental cells and contained an electrolyte consisting of palladium(II) chloride, lithium chloride, and heavy water. The control cells used copper(II) chloride, lithium chloride, and heavy water electrolyte. Experimental and control cells were supplied current, increasing from 0.1 to 100.0 mA over a period of 20 days. For test days 9 through 20, the standard configuration experimental cells exhibited significantly higher average neutron radiation than the controls at a 99% confidence level. Alternative configurations involving more increasing current over a shortened time scale, substitutions of water in place of heavy water or potassium chloride for lithium chloride, as well as inclusion of depleted uranium near the cell cathodes all resulted in inconclusive evidence for promoting neutron production.

neutron↗

DOE OSTI2023

Report on ISR-1 High-Altitude Balloon Flight

To test small technologies at lower cost for space science applications, LANL has developed a small high altitude balloon payload that could, in the future, be regularly and inexpensively launched from LANL. A neutron detector, NEMO, was integrated to evaluate its performance in a space-like mixed-radiation environment and collect neutron data in the atmosphere. In collaboration with EES-14, a high-altitude balloon payload was launched from LANL Technical Area 51 on February 27, 2023 and April 17, 2023. For real-time geolocation, a SAM-M8Q M8 GNSS module was used to get position and time, and an Iridium RockBLOCK 9603 was used to communicate with the ground using the Iridium satellite fleet. These modules were all controlled using an Iteaduino Mega microcontroller board. Finally, a High Altitude Science Eagle Flight Computer with a temperature pressure sensor ran independently, writing data to an SD card. All of these modules were powered by a 5 mAh lithium polymer battery. The battery was attached to the bottom of the payload while the remaining electronics were embedded in the underside of the top of the payload. These modules were wired as seen in Figure 1-2. The Iteaduino Mega microcontroller board was programmed to use the RockBLOCK to send a message once every 10 minutes containing neutron and GPS data read off the NEMO and SAM M8Q, respectively. Once the message send attempt finished, the RockBLOCK would be slept for the rest of the 10 minute interval. The Eagle Flight Computer ran continuously throughout the flight, taking data every 6 seconds. The RockBLOCK message data was set up to be delivered from the Iridium satellite fleet to a website, where it was stored and parsed to create live maps and plots for analysis and balloon retrieval. The RockBLOCK message data was additionally configured to be sent to an email as a fail-safe. The payload was ground-tested successfully for over 50 hours, with multiple revisions occurring to best prepare for conditions at altitude and improve the software and firmware to fix any issues that cropped up with the data pipeline. Additional to the balloon payload, the flight had an attached iMet-4 radiosonde and Garmin T5 GPS Dog Collar. The radiosonde provided GPS and meteorological data. The T5 dog collar is used along with a Garmin Astro 430 to track the balloon at a range of up to 9 miles for retrieval. The balloon itself was initially a 1600 g meteorological balloon with an attached High Altitude Science parachute, both of which can be seen in Figure 1-3. After the first flight, the EES team swapped to a Rocketman parachute.

42 ENGINEERING↗

NASA NTRS2004

Northern and Southern Permafrost Regions on Mars with High Content of Water Ice: Similarities and Differences

The measurements by neutron detectors on Odyssey have revealed two large poleward regions with large depression of flux of epithermal and high energy neutrons [1-3]. The flux of neutrons from Mars is known to be produced by the bombardment of the surface layer by galactic cosmic rays. The leakage flux of epithermal and fast neutrons has regional variation by a factor of 10 over the surface of Mars (e.g. see [3- 5]). These variations are mainly produced by variations of hydrogen content in the shallow subsurface. On Mars hydrogen is associated with water. Therefore, the Northern and Southern depressions of neutron emission could be identified as permafrost regions with very high content of water ice [1-5]. These regions are much larger than the residual polar caps, and could contain the major fraction of subsurface water ice. Here we present the results of HEND neutron data deconvolution for these regions and describe the similarities and differences between them.

Mitrofanov, I. G.↗

NASA NTRS2004

Northern and Southern Permafrost Regions on Mars with High Content of Water Ice: Similarities and Differences

The measurements by neutron detectors on Odyssey have revealed two large poleward regions with large depression of flux of epithermal and high energy neutrons. The flux of neutrons from Mars is known to be produced by the bombardment of the surface layer by galactic cosmic rays. The leakage flux of epithermal and fast neutrons has regional variation by a factor of 10 over the surface of Mars. These variations are mainly produced by variations of hydrogen content in the shallow subsurface. On Mars hydrogen is associated with water. Therefore, the Northern and Southern depressions of neutron emission could be identified as permafrost regions with very high content of water ice. These regions are much larger than the residual polar caps, and could contain the major fraction of subsurface water ice. Here we present the results of HEND neutron data deconvolution for these regions and describe the similarities and differences between them.

Mitrofanov, I. G.↗

DOE OSTI2025

A Ce-Doped LiI Scintillator Film-Based High Rate, High Spatial Resolution Neutron Anger Camera for Neutron Scattering Facilities

The 2-D position sensitive neutron detectors featuring a significantly improved count rate capacity and a sub-mm spatial resolution are in high demand by neutron scattering facilities, especially the next generation high-flux spallation neutron sources (SNSs). They are anticipated to play a crucial role in fully utilizing the unprecedentedly high neutron brightness offered by these sources. In this work, a high rate and high spatial resolution neutron Anger camera has been successfully developed based on a Ce-doped microcolumnar LiI scintillator film and the PETsys TOFPET2 ASIC readout electronics. The performance evaluation was conducted in a standard laboratory environment as well as the High Flux Isotope Reactor (HFIR) at Oak Ridge National Laboratory (ORNL) with regard to light yield, γ-ray sensitivity, neutron detection efficiency, count rate capability, spatial resolution, and position linearity. The LiI:Ce scintillator was found to have a higher light yield and a lower γ-ray sensitivity than GS20 (i.e., 11729 versus 6000 photons/n and 1.67 × 10 −5 versus on the order of 10 −4 ). The neutron detection efficiency was measured to be 63% at 4.2 Å. This camera demonstrated an exceptional count rate capability, up to at least 481 kHz without rate loss. The spatial resolution was as good as 0.47 mm. Here, the position linearity was also enhanced.

High rate↗

DOE OSTI2020

Epithermal Neutron Resonance Analysis Using a Compact D-T Generator

Nuclear material identification and isotopic composition analysis are important capabilities for safeguards and the verification of nuclear arms control and nonproliferation treaties. Epithermal neutron resonance imaging has been proposed for spent fuel assay measurements, and the development of a mobile neutron imaging system could provide such a tool for on-site applications. This technique is highly sensitive to isotopes of interest for safeguards applications (e.g. 235,238 U, 238,239,240 Pu) and yields unique transmission spectra for a target containing actinides and some mid- and high-Z elements. Paired with a position-sensitive neutron detector, such a system could provide spatial information of the target isotopic composition. Recent progress in the development of high intensity neutron sources could make mobile epithermal neutron imaging designs increasingly feasible to serve as a tool for nuclear inspectors. In this work, Monte Carlo (MC) simulations were performed to further optimize a previous design for an epithermal neutron resonance-based analysis apparatus using a D-T portable neutron generator. Additionally, experimental work is being performed to test the feasibility of this method. The MC simulations of moderation time distributions for different moderator compositions and thicknesses were measured to provide a multi-group correction for neutron time-of-flight energy reconstruction.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2023

Numerical Studies of the On-Line Reactivity Monitoring Techniques in Subcritical Systems: Revisit of the Area-Ratio Method, the Neutron Source-Modulation Method, and the Flux-to-Current Ratio Method

In the subcritical systems, the subcriticality level must be monitored continuously to ensure the safe operation of the systems. Techniques such as the neutron source-modulation method and the flux-to-current ratio method have been proposed for on-line reactivity measurements of the subcritical systems. However, the accuracy of these methods is unknown in the actual applications. In this report, the fundamental concepts of these techniques are visited, with numerical simulation techniques developed to validate these on-line reactivity monitoring methodologies. Specifically, the Monte Carlo numerical simulation results show that the neutron source-modulation method is not accurate in determining the reactivity of the subcritical systems. The flux-to-current ratio method can provide on-line reactivity measurements, and its spatial effects have been studied and well understood through the numerical simulations of the fuel loading of the neutron source facility of Ukraine. In addition, a modified version of the area-ratio method is proposed for the on-line measurements of the absolute reactivity of the subcritical systems. Monte Carlo numerical simulations showed that this method can provide the absolute reactivity of the subcritical systems within ~5% error, if the neutron detectors are placed close to the fuel assembly interface with the reflector zone or in the reflector zones away from the neutron source.

22 GENERAL STUDIES OF NUCLEAR REACTORS↗

NASA NTRS2012

Chemical Mapping of Vesta and Ceres

Following successful science operations at Vesta, the Dawn spacecraft is headed for an encounter with Ceres in 2015. What have we learned at Vesta? And, what do we expect to learn by comparing Vesta and Ceres? We will address these questions from the standpoint of geochemistry. Dawn's Gamma Ray and Neutron Detector (GRaND) is sensitive to the elemental composition of surface materials to depths of a few decimeters [1]. Gamma rays and neutrons, produced by the steady bombardment of galactic cosmic rays and by the decay of naturally ]occurring radioisotopes (K, Th, U), provide a chemical fingerprint of the regolith. Analysis of planetary radiation emissions enables mapping of specific elements (such as Fe, Mg, Si, Cl, and H) and compositional parameters (such as average atomic mass), which provide information about processes that shaped the planet1s surface and interior. Dawn has exceeded operational goals for GRaND at Vesta, accumulating an abundance of nadir-pointed data during five months in a 210 km, low altitude mapping orbit around Vesta (265-km mean radius). Chemical information from gamma ray and neutron measurements was used to test the connection between Vesta and the howardite, eucrite, and diogenite (HED) meteorites [2]. Additionally, GRaND searched for evolved, igneous lithologies [3], mantle and upper crustal materials exposed in large impact basins, mesosiderite compositions, and hydrogen in Vesta1s bulk regolith. Results of our analyses and their implications for thermal evolution and regolith-processes will be presented. The possibility of a subcrustal ocean [4, 5] and lack of cerean meteorites makes water-rich Ceres a compelling target of exploration [6]. If Ceres underwent aqueous differentiation, then crustal overturn or gas driven volcanism may have significantly modified its primitive surface; and products of aqueous alteration (e.g. [7]) would detectable by GRaND [1]. For example, the presence of Cl in salts, associated with liquid-water-processes, would have a profound effect on the thermal neutron leakage flux. GRaND is sensitive to H and H-layering, which may be in the form of endogenic water ice or hydrous minerals on Ceres. Ammonia ice (e.g., from recent cryovolcanism) would produce a distinctly different neutron signature than water ice [1]. Prospective results for GRaND at Ceres will be presented in the context of what we have learned about Vesta.

Prettyman, Thomas H.↗

DOE OSTI2021

Characterization of Two Extraordinary AmLi Neutron Sources

Two legacy AmLi sources, MRC-101 and MRC-103, are routinely used for neutron detector characterization and testing campaigns that Pacific Northwest National Laboratory manages for the Defense Threat Reduction Agency within the U.S. Department of Defense. However, applicability of source measurement data has been substantially limited due to the lack of original manufacturer documentation and cross comparison to other sources. This paper summarizes results of the measurement campaign conducted to better quantify source radionuclide content, neutron energy spectrum and emission rate of the AmLi sources. The source characterization study consisted of three major consecutive measurement exercises. First, gamma spectrometry measurements using a high purity germanium detector were used to estimate the radionuclide content and potential impurities of the AmLi sources. Then neutron spectral measurements were taken to determine the unique neutron energy distribution. Finally, assessments of the total neutron yields of the sources were made with measurements in a neutron well counter. The neutron detection efficiency for these measurements was determined via detailed Monte Carlo modeling based on the neutron energy distribution measured with the rotating neutron spectrometer. The most exciting and unexpected finding of the study was a significant contamination of the source material with beryllium, contributing up to 17% to the total neutron emission rate and correspondingly changing the neutron energy spectrum. Also, the obtained lithium-only portion of the measured energy distribution of the sources was compared against several AmLi spectra previously reported by different researchers.

AWCC, AmLi, beryllium contamination, neutron spect↗

DOE OSTI2023

Analysis of WIRE-21 SPND and Optical Fiber Sensor Measurements

The Wireless Instrumented RB Experiment 2021 (WIRE-21) was a highly instrumented experiment designed to test prototype wireless temperature and pressure sensors developed by Westinghouse Electric Corporation (WEC) in the High Flux Isotope Reactor (HFIR). In addition to these sensors, a suite of other sensors was also integrated into the experiment capsule, including various types of distributed optical fiber sensors and self-powered neutron detectors (SPNDs). This report presents an analysis of the data generated by the SPNDs and optical fiber sensors that were tested under the highest reported neutron flux. The distributed optical fiber sensor results demonstrate that F-doped optical fibers, particularly those inscribed with fs fiber Bragg gratings (FBGs), are capable of surviving fast neutron fluences on the order of 1021 n fast /cm 2 at temperatures relevant to light-water reactors (between 200 and 400°C). However, a significant blue-shift in the optical spectra of these sensors was observed over the course of irradiation which cannot be explained based on the current understanding of radiation-induced compaction in fused silica glass. A mechanistic understanding of this drift has not yet been developed and is proposed as future scope under the Advanced Sensors and Instrumentation program. Of the four SPNDs, only one appeared to operate normally during three cycles of irradiation. A radiation transport model of the experiment in HFIR was used to determine time-dependent neutron flux in this SPND and to calculate the neutron sensitivity of the device. Results showed a cycle averaged sensitivity of 1.5 ×10 -22 and 1.4 ×10 -22 A/nν for the first and third cycles of irradiation, respectively. Additional details pertaining to the optical fibers and SPNDs are included herein.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

NASA NTRS2013

Preliminary Iron Distribution on Vesta

The distribution of iron on the surface of the asteroid Vesta was investigated using Dawn's Gamma Ray and Neutron Detector (GRaND) [1,2]. Iron varies predictably with rock type for the howardite, eucrite, and diogenite (HED) meteorites, thought to be representative of Vesta. The abundance of Fe in howardites ranges from about 12 to 15 wt.%. Basaltic eucrites have the highest abundance, whereas, lower crustal and upper mantle materials (cumulate eucrites and diogenites) have the lowest, and howardites are intermediate [3]. We have completed a mapping study of 7.6 MeV gamma rays produced by neutron capture by Fe as measured by the bismuth germanate (BGO) detector of GRaND [1]. The procedures to determine Fe counting rates are presented in detail here, along with a preliminary distribution map, constituting the necessary initial step to quantification of Fe abundances. We find that the global distribution of Fe counting rates is generally consistent with independent mineralogical and compositional inferences obtained by other instruments on Dawn such as measurements of pyroxene absorption bands by the Visual and Infrared Spectrometer (VIR) [4] and Framing Camera (FC) [5] and neutron absorption measurements by GRaND [6].

Mittlefehldt, David W.↗

NASA NTRS2011

Isolation Effects on the Moon: High Topographic Slope Observations from the LRO and LOLA Instruments

The extremely low temperatures in the Moon's polar permanent shadow regions (PSR) has long been considered a unique factor necessary for entrapping volatile Hydrogen (H). However, recent discoveries indicate some H concentrations lie outside PSR, suggesting other geophysical factors may also influence H distributions. In this study we consider insolation and its resulting thermal effects as a loss/redistribution process influencing the Moon's near-surface < 1m volatile H budget. To isolate regional (5deg latitude band) insolation effects we correlate two data sets collected from the ongoing, 1.5 year long mapping mission of the Lunar Reconnaissance Orbiter (LRO). Epithermal neutron mapping data from the Lunar Exploration Neutron Detector (LEND) is registered and analyzed in the context of slope derivations from Lunar topography maps produced by the Lunar Observing Laser Altimeter (LOLA). Lunar epithermal neutrons are inferred to be direct geochemical evidence for near-surface H due to the correlated suppression of surface leakage fluxes of epithermal neutrons with increased H concentration. Regional suppressions of neutrons seen in LEND maps are considered localized evidence of H concentration increase in the upper 1 m of the Lunar surface. To quantify spatially localized insolation effects, LEND data are averaged from sparsely distributed pixels, classed as a function of the LOLA slope derivations.

McClanahan, T. P.↗

NASA NTRS1971

The energy dependence of the cosmic-ray neutron leakage flux in the range 0.01-10 MeV.

Measurement of the cosmic-ray neutron leakage flux and energy spectrum in the range 1 to 10 MeV by a neutron detector on the Ogo 6 satellite from June 7 to Sept. 30, 1969. The same detector simultaneously measured the total leakage flux, having 75% of its response to the leakage flux in the interval from 1 keV to 1 MeV. For a neutron energy spectrum of the form AE to the minus gamma in the range from 1 to 10 MeV, the upper limit to gamma for polar regions was found to be 1.0 and for the equatorial regions was 1.2. For the polar regions, the lower limit to gamma was found to be 0.8. This energy spectrum at 1 to 10 MeV is slightly flatter than Newkirk (1963) predicted.

Jenkins, R. W.↗

NASA NTRS2012

Testing Lunar Permanently Shadowed Regions for Water Ice: LEND Results from LRO

We use measurements from the Lunar Exploration Neutron Detector (LEND) collimated sensors during more than one year of the mapping phase of NASA's Lunar Reconnaissance Orbiter (LRO) mission to make estimates of the epithermal neutron flux within known large Permanently Shadowed Regions (PSRs). These are compared with the local neutron background measured outside PSRs in sunlit regions. Individual and collective analyses of PSR properties have been performed. Only three large PSRs, Shoemaker and Cabeus in the south and Rozhdestvensky U in the north, have been found to manifest significant neutron suppression. All other PSRs have much smaller suppression, only a few percent, if at all. Some even display an excess of neutron emission in comparison to the sunlit vicinity around them. Testing PSRs collectively, we have not found any average suppression for them. Only the group of 18 large PSRs, with area >200 square kilometers, show a marginal effect of small average suppression, approx. 2%, with low statistical confidence. An approx. 2% suppression corresponds to approx. 125 ppm of hydrogen taking into account the global neutron suppression near the lunar poles and assuming a homogeneous H distribution in depth in the regolith. This means that all PSRs, except those in Shoemaker, Cabeus and Rozhdestvensky U craters, do not contain any significant amount of hydrogen in comparison with sunlit areas around them at the same latitude.

LEND↗

NASA NTRS2003

Search for Chemically Bound Water in the Surface Layer of Mars Based on HEND/Mars Odyssey Data

This study is emphasized on search for signatures of chemically bound water in surface layer of Mars based on data acquired by High Energy Neutron Detector (HEND) which is part of the Mars Odyssey Gamma Ray Spectrometer (GRS). Fluxes of epithermal (probe the upper 1-2 m) and fast (the upper 20-30 cm) neutrons, considered in this work, were measured since mid February till mid June 2002. First analysis of this data set with emphasis of chemically bound water was made. Early publications of the GRS results reported low neutron flux at high latitudes, interpreted as signature of ground water ice, and in two low latitude areas: Arabia and SW of Olympus Mons (SWOM), interpreted as 'geographic variations in the amount of chemically and/or physically bound H2O and or OH...'. It is clear that surface materials of Mars do contain chemically bound water, but its amounts are poorly known and its geographic distribution was not analyzed.

Basilevsky, A. T.↗

DOE OSTI2026

Performance assessment of PHITS simulations for the inverse-kinematic p( 7 Li,n) 7 Be reaction based on fast-neutron measurements with a diamond detector

The inverse-kinematics p( 7 Li,n) 7 Be reaction produces forward-focused neutron emission, offering enhanced usable flux and reduced shielding requirements. Reliable simulation of such neutron fields is essential for the development of compact accelerator-based neutron sources. In this study, a PHITS-based simulation framework for the reaction was experimentally assessed using fast-neutron measurements. Forward-directed neutrons were measured with a diamond neutron detector and quantitatively compared with simulations with newly prepared IK-Frag cross-section file based on the proton-induced reaction data in ENDF/B-VIII.1, TENDL-2023, and JENDL-4.0/HE. Measurements and simulations were performed for incident 7 Li 3+ energies ranging from 15.0 to 25.0 MeV using a 50 μm-thick polypropylene target. For all conditions, the PHITS-based simulation framework reproduced the deposited energy spectra at the correct order of magnitude. The comparison of deposited energy spectra in the diamond detector showed high correlation coefficients across all investigated energies, indicating reasonable agreement in spectral shape between simulations and measurements. This work represents an initial step toward establishing a benchmark for PHITS simulations of the inverse kinematic reaction between an incident lithium-ion and a proton target.

43 PARTICLE ACCELERATORS↗