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DOE OSTI2023

Quantification of the light output anistropy in deuterated stilbene

Deuterated stilbene is an organic scintillator that is a desirable material for fast neutron spectroscopy using spectrum unfolding techniques without requiring time-of-flight information. Due to the crystal structure of the material, some anisotropy of the light output exists, which is dependent on the direction of heavy charged particle recoil relative to the crystal structure. The anisotropy of trans-stilbene (hereafter referred to as stilbene) has been well characterized in previous work, but for deuterated stilbene, the anisotropy has only been partially characterized along the a and b crystal axes, while the artificial c' axis, which shows the largest anisotropy in stilbene, has not been characterized until this publication. Here, in this work, two deuterated stilbene crystals were characterized with neutron energies up to 35 MeV at the Los Alamos Neutron Science Center. For one of the crystals, the response is characterized along the a, b, and c' axes. This characterization shows a distinct anisotropy along the axes in deuterated stilbene, which is very similar to that found in regular stilbene, such that the a axis is the brightest, while the b' and c' axes are approximately 3% and 20%–35% lower relative to the a axis.

36 MATERIALS SCIENCE↗

DOE OSTI2026

Upgrade of the CAESium-iodide scintillator ARray (CAESAR) electronics and data acquisition system for optimized performance at FRIB

Here, we report on the upgrade of the electronics and data acquisition (DAQ) of the high-efficiency CAESium-iodide scintillator ARray (CAESAR) at the Facility for Rare Isotope Beams (FRIB). With the on-going capability ramp-up of FRIB, CAESAR is expected to continue to be an in-demand -ray spectrometer owing to its high detection efficiency, compactness, and modularity, enabling easy integration with additional detection and DAQ systems. Within this context, the CAESAR electronics and DAQ were upgraded to remove obsolete modules, enhance the ease of integration with external instruments, and optimize the DAQ live time. We present the comprehensive results from offline (γ-ray sources) and online (in-beam experiment) commissioning, characterizing the performance of CAESAR’s new electronics and DAQ.

CsI(Na) scintillator array↗

NASA NTRS2019

The NANOGrav 12.5 yr Data Set: The Frequency Dependence of Pulse Jitter in Precision Millisecond Pulsars

Low-frequency gravitational-wave experiments require the highest timing precision from an array of the moststable millisecond pulsars. Several known sources of noise on short timescales in single radio pulsar observationsare well described by a simple model of three components: template fitting from a finite signal-to-noise ratio, pulsephase/amplitude jitter from single-pulse stochasticity, and scintillation errors from short-timescale interstellarscattering variations. Currently template-fitting errors dominate, but as radio telescopes push toward higher signalto-noise ratios, jitter becomes the next dominant term for most millisecond pulsars. Understanding the statistics ofjitter becomes crucial for properly characterizing arrival time uncertainties. We characterize the radio frequencydependence of jitter using data on 48 pulsars in the North American Nanohertz Observatory for GravitationalWaves timing program. We detect significant jitter in 43 of the pulsars and test several functional forms for itsfrequency dependence; we find significant frequency dependence for 30 pulsars. We find moderate correlations ofrms jitter with pulse width (R = 0.62) and number of profile components (R = 0.40); the single-pulse rms jitter istypically 1% of pulse phase. The average frequency dependence for all pulsars using a power-law model hasindex 0.42. We investigate the jitter variations for the interpulse of PSR B1937+21 and find no significantdeviations from the main pulse rms jitter. We also test the time variation of jitter in two pulsars and find thatsystematics likely bias the results for high-precision pulsars. Pulsar timing array analyses must properly modeljitter as a significant component of the noise within the detector.

Lam, M. T.↗

NASA NTRS1992

Scintillations of the Uranian kilometric radiation - Implications for the downstream magnetopause

Results are presented of the planetary radio astronomy observations conducted on board Voyager 2, with emphasis placed on the characteristics of the strong (3 to 6 dB) modulations of the broadband smooth Uranian radio emissions recorded from January 27-30, 1986, when the spacecraft was outbound from Uranus. The modulations were characterized by two superposed periods of about 100 sec and about 10 sec. It is suggested that the long-period modulation is due to the magnetopause surface waves, while the short-period modulations are due to the signature of ion cyclotron turbulence above the proton gyrofrequency, related to the magnetopause boundary layer.

Pedersen, B. M.↗

DOE OSTI2020

ANNIE: Neutron multiplicity in neutrino interactions and new technologies

The Accelerator Neutrino Neutron Interaction Experiment (ANNIE) aims at measuring the neutron abundance in the final state of neutrino-nucleus interactions. This measurement will have a direct impact on our understanding of neutrino interactions and will lead to a better reduction of systematic errors and an improvement of signal-background discrimination in future large neutrino detectors, thus impacting long baseline oscillation experiments as well as proton decay searches and supernova detection. With a volume of about 26 tons of pure water doped with gadolinium to enhance neutron tagging efficiency, ANNIE will provide a measurement of the neutron yield of neutrino interactions as a function of the neutrino energy in the well-characterized Booster Neutrino Beam at Fermilab. The modularity of ANNIE will allow it to perform several fundamental tests of new technologies to be used in neutrino detectors, such as a novel kind of photodetectors called Large Area Picosecond Photodetectors and Water-based Liquid Scintillator, a newly-developed detection medium. The technology behind the ANNIE detector will have a noticeable impact on the development of future large water Cherenkov detectors as well as on detection techniques for neutrino physics.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2025

Characterization of dynamics and decay in the St. Benedict Paul trap

The St. Benedict experiment includes a linear Paul trap designed to measure the beta-neutrino angular correlation coefficient 𝑎 𝛽ν of mixed superallowed 𝛽-decay transitions between mirror nuclei via coincidence detection of 𝛽-particles and recoiling ions. The emitted 𝛽 particle and daughter ion are detected with plastic scintillators and micro-channel plate detectors, respectively, allowing for accurate measurements of their time-of-flights. From the shape of the coincidence time-of-flight distribution, a value of 𝑎 𝛽ν can be determined. This manuscript presents detailed simulations of the St. Benedict Paul trap, with a focus on ion cloud dynamics and recoiling daughter trajectories.

Linear Paul trap↗

DOE OSTI2022

Design and Characterization of an Optically Segmented Single Volume Scatter Camera Module

Here, the optically segmented single volume scatter camera (OS-SVSC) aims to image neutron sources for nuclear nonproliferation applications using the kinematic reconstruction of elastic double-scatter events. We report on the design, construction, and calibration of one module of a new prototype. The module includes 16 EJ-204 organic plastic scintillating bars individually wrapped in Teflon tape, each measuring 0.5cx0.5cmx20cm . The scintillator array is coupled to two custom silicon photomultiplier (SiPM) boards consisting of a 2x8 array of SensL J-Series-60035 SiPMs, which are read out by a custom 16 channel DRS4 based digitizer board. The electrical crosstalk between SiPMs within the electronics chain is measured as 0.76%±0.11% among all 16 channels. We report the detector response of one module including interaction position, time, and energy, using two different optical coupling materials: EJ-560 silicone rubber optical coupling pads and EJ-550 optical coupling grease. We present results in terms of the overall mean and standard deviation of the z -position reconstruction and interaction time resolutions for all 16 bars in the module. We observed the 1σz -position resolution for gamma interactions in the 0.3–0.4 MeVee range to be 2.24 cm ± 1.10 cm and 1.45 cm ± 0.19 cm for silicone optical coupling pad and optical grease, respectively. The observed 1σ interaction time resolution is 265 ps ± 29 ps and 235 ps ± 10 ps for silicone optical coupling pad and optical grease, respectively.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗

DOE OSTI2025

UCNProBe NaI Veto System Characterization and Simulation

This paper presents a summary of my research and technical contributions during a summer internship at Los Alamos National Laboratory, supporting the development of the active veto system for the UCNProBe experiment. UCNProBe aims to perform a state-of-the-art measurement of the free neutron lifetime, requiring low-background conditions facilitated by an array of sodium iodide (NaI) scintillators.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗

NASA NTRS1985

Measurements of the angular distribution of auroral-zone bremsstrahlung in the middle atmosphere

The angular distributions of atmospheric electron bremsstrahlung at 45-65 km are determined by analyzing NaI-scintillation-detector measurements of X-rays in energy ranges upward of 5, 10, 20, and 40 keV obtained in two rocket flights over Alaska during March 1978 as part of the Aurorozone II project (Goldberg et al., 1984). The data are presented graphically and characterized, with a focus on periods of post-breakup auroral precipitation events. Findings reported include generally uniform upward and downward intensities, with the upward intensity typically 1-10 percent of the total; a smooth zenith-nadir transition of angular width less than + or - 20 deg at 40 keV; a downward energy spectrum dominated by direct X-rays at 65 km but much less so at lower altitudes (where Compton-scattered X-rays play a greater role); and a completely scattered-X-ray-dominated upward energy spectrum. Reasonable agreement is found when these data are compared with the theoretical bremsstrahlung calculations of Berger and Seltzer (1972).

Barcus, J. R.↗

DOE OSTI2026

3D printed water-stable Cd-doped Cs 4 MnBi 2 Cl 12 /polylactic acid perovskite/polymer composites for high-flux X-ray scintillation

Stable and efficient X-ray scintillators are crucial for medical diagnostics, industrial, and defense applications. However, conventional scintillator technologies face a trade-off between stability, optimal performance, and sustainability. Herein, we introduce 3D-printed Cs 4 MnBi 2 Cl 12 (Pero1) and Cs 4 Cd 0.68 Mn 0.32 Bi 2 Cl 12 (Pero2) perovskite microcrystals embedded within a polylactic acid (PLA) polymer composite as X-ray scintillators, combining efficiency, stability, and sustainability. The orange luminescent perovskite powder phosphors exhibited poor water stability, which was successfully addressed through incorporation into PLA via filament extrusion and fused deposition modeling (FDM) 3D printing. The resulting composite films demonstrated remarkable water stability while maintaining uniform orange emission throughout the polymer matrix, as confirmed by 3D topography scanning and X-ray fluorescence mapping. Structural characterization revealed minimal chemical interaction between the perovskite and PLA matrix, with the composites retaining their crystalline properties. The PLA-Pero2 composite exhibited superior optical properties, with a photoluminescence quantum yield of 47%, nearly 17 times higher than that of PLA-Pero1 (2.8%), attributed to the effective suppression of non-radiative decay pathways through Cd 2+ doping. Under hard X-ray irradiation at synchrotron beamlines, both composites exhibited excellent radioluminescence, with emission peaks at 605 nm, a linear response across a wide X-ray flux range, and remarkable radiation stability, showing less than 3% intensity degradation after 600 seconds of continuous high-dose exposure. The PLA-Pero2 composite achieved a spatial resolution of 5 line pairs per millimeter and a contrast ratio of 0.255. These performance metrics, combined with the polymer's biodegradability and scalability through additive manufacturing, position PLA-based composites as a more sustainable alternative to conventional petroleum-based polymer scintillators for next-generation medical imaging, radiation monitoring, and industrial radiography applications.

3D Printing↗

DOE OSTI2022

Quantifying spatial resolution in a fast neutron radiography system

Neutron imaging is a powerful nondestructive examination modality that has been employed in various applications. Fast neutrons provide advantages over lower energy neutrons, such as examining thicker samples and inducing negligible activation and transmutations. However, fast neutrons interact mostly via elastic scattering with both the neutron detector and the object, causing degradation in spatial resolution. This study explores the quantification of spatial resolution caused by the testing target itself and suggests proper candidate materials for characterizing spatial resolution in terms of modulation transfer function. Knife-edge radiographs of 3 mm, 6 mm, and 5 cm thick Tantalum (Ta) foils, and a 2.54 cm Tungsten (W) cube were acquired using a CCD-based imaging system and a Polyvinyl Toluene (PVT) scintillator at the Ohio State Research Reactor (OSURR)’s fast neutron beam facility. The spatial resolutions calculated were 195 ± 20 μm, 224 ± 22 μm, 248 ± 25 μm, and 435 ± 44 μm for 3 mm, 6 mm, and 5 cm Ta foils, and 2.54 cm W cube, respectively. The results showed a worsening spatial resolution with increasing target thickness. Simulations and calculations estimate that elastic scattering kinematics between neutrons and protons in the PVT medium also limits spatial resolution, and it sets a lower limit of ~44 μm on the spatial resolution for 2 MeV neutrons.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

NASA NTRS1971

Balloon measurements of cosmic ray protons and helium over half a solar cycle 1965-1969.

Evaluation of differential energy spectra for protons and helium covering the energy range from 100 to 260 MeV/nucleon obtained from balloon flights made each summer (1965 to 1969) at Churchill, Manitoba, with the aid of a Geiger-tube hodoscope operated in conjunction with two scintillation elements used to measure dE/dx and E. Supplementary data from balloon flights at Minneapolis, Minn., and Sioux Falls, S. Dak. and from calibration exposures to protons and electrons were used to define backgrounds and to verify the predicted detector response. The observed proton spectra are characterized over a wide range of energy (30 to 300 MeV) by a simple relationship between cosmic-ray intensity J and kinetic energy T: J = AT. The helium spectra also follow this law at solar maximum but rise less steeply near solar minimum. This characteristic behavior can be interpreted in terms of a simple model in which convection is balanced by adiabatic deceleration.-

Rygg, T. A.↗

NASA NTRS1995

Magellan radio occultation measurements of atmospheric waves on Venus

Radio occultation experiments were conducted at Venus on three consecutive orbits of the Magellan spacecraft in October 1991. Each occultation occurred over the same topography (67 deg N, 127 deg E) and at the same local time (22 hr 5 min), but the data are sensitive to zonal variations because the atmosphere rotates significantly during one orbit. Through comparisons between observations and predictions of standard wave theory, we have demonstrated that small-scale oscillations in retrieved temperature profiles as well as scintillations in received signal intensity are caused by a spectrum of vertically propagating internal gravity waves. There is a strong similarity between the intensity scintillations observed here and previous measurements, which pertain to a wide range of locations and experiment dates. This implies that the same basic phenomenon underlies all the observations and hence that gravity waves are a persistent, global feature of Venus' atmosphere. We obtained a fairly complete characterization of a gravity wave that appears above the middle cloud in temperature measurements on all three orbits. The amplitude and vertical wavelength are about 4 K and 2.5 km respectively, at 65 km. A model for radiative damping implies that the wave intrinsic frequency is approximately 2 x 10(exp 4) rad/sec, the corresponding ratio between horizontal and vertical wavelengths is approximately 100. The wave is nearly stationary relative to the surface or the Sun. Radiative attenuation limits the wave amplitude at altitudes above approximately 65 km, leading to wave drag on the mean zonal winds of about +0.4 m/sec per day (eastward). The sign, magnitude, and location of this forcing suggest a possible role in explaining the decrease with height in the zonal wind speed that is believed to occur above the cloud tops. Temperature oscillations with larger vertical wavelengths (5-10 km) were also observed on all three orbits, but we are able unable to interpret these unambiguously.

Hinson, David P.↗

NASA NTRS1996

Preliminary analysis of fluctuations in the received uplink-beacon-power data obtained from the GOLD experiments

Uplink data from recent free-space optical communication experiments carried out between the Table Mountain Facility and the Japanese Engineering Test Satellite are used to study fluctuations caused by beam propagation through the atmosphere. The influence of atmospheric scintillation, beam wander and jitter, and multiple uplink beams on the statistics of power received by the satellite is analyzed and compared to experimental data. Preliminary analysis indicates the received signal obeys an approximate lognormal distribution, as predicted by the weak-turbulence model, but further characterization of other sources of fluctuations is necessary for accurate link predictions.

M. Jeganathan↗

NASA NTRS1996

Preliminary Analysis of Fluctuations in the Received Uplink-Beacon-Power Data Obtained From the GOLD Experiments

Jeganathan, M.↗

DOE OSTI2025

Commission < 5 µm spatial resolution x-ray imager for High Resolution Turbulence experiments

This report presents the successful development, commissioning, and deployment of the Scintillation-Based X-ray Imager (SBXI) for the High-Resolution Turbulence (HRT) campaign at the National Ignition Facility (NIF). The SBXI system was designed to overcome the spatial resolution and efficiency limitations of conventional x-ray imaging detectors. Through careful system engineering, rigorous laboratory characterization, and experimental validation at NIF, the SBXI has demonstrated spatial resolution at the object plane of 5 μm (±0.5 μm) and a detective quantum efficiency (DQE) of 34% at 7.2 keV, both of which surpass the requirements set by the campaign, and meeting the L2 milestone. The system’s deployment enables high-fidelity imaging of fine-scale hydrodynamic instabilities, directly supporting advanced turbulence model validation and future high energy density physics research.

42 ENGINEERING↗

NASA NTRS2007

Micro-Fabricated Solid-State Radiation Detectors for Active Personal Dosimetry

Active radiation dosimetry is important to human health and equipment functionality for space applications outside the protective environment of a space station or vehicle. This is especially true for long duration missions to the moon, where the lack of a magnetic field offers no protection from space radiation to those on extravehicular activities. In order to improve functionality, durability and reliability of radiation dosimeters for future NASA lunar missions, single crystal silicon carbide devices and scintillating fiber detectors are currently being investigated for applications in advanced extravehicular systems. For many years, NASA Glenn Research Center has led significant efforts in silicon carbide semiconductor technology research and instrumentation research for sensor applications under extreme conditions. This report summarizes the technical progress and accomplishments toward characterization of radiation-sensing components for the recommendation of their fitness for advanced dosimetry development.

Wrbanek, John D.↗

DOE OSTI2019

Deployment of magnetometers to monitor stray magnetic fields near the PROSPECT detector

PROSPECT is a reactor antineutrino experiment located in the High Flux Isotope Reactor (HFIR) at Oak Ridge National Laboratory. PROSPECT’s primary goals are to probe short-baseline oscillations and perform a precise measurement of the U-235 reactor antineutrino spectrum. The detector consists of 154 segmented cells filled with 6Li-doped liquid scintillator. Each segment holds two PMTs, one on each end of the cell. The PMTs can be exposed to stray magnetic fields from superconducting magnets operating on the experiment hall one floor below the detector. The monitoring of the magnetic fields is an important part of our background characterization as the magnetic fields can directly influence the energy measurement. This study presents the characterization and monitoring of stray magnetic fields using triple axis magnetometers near the detector.

Gilbert, Corey E.↗