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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 235 records · Page 13
All sourcesNASA NTRSDOE OSTI
NASA NTRSDate not supplied

Analysis of Crack Propagation Transients in Accelerated Fatigue Characterization of Adhesives

The characterization of the rates of crack propagation by means of a Paris law is intended for steady-state fatigue conditions. While rates of crack propagation are primarily driven by 𝐽𝐽𝑚𝑚𝑚𝑚𝑚𝑚, in the presence of evolving process zones and fiber bridging they also depend on the crack propagation length: cracks with fully formed process zones propagate more slowly. Analyses of the rates of crack propagation in laminates secondarily bonded with AF163-2K film adhesive were conducted to identify the rate transients that occur during the formation of the process zone in the adhesive and during the evolution of bridging of the adhesive’s carrier knit across the crack faces. Dávila's CF22 cohesive fatigue damage model was used in finite element analyses of the double cantilever beam test to explain discrepancies in experimental rates of propagation obtained from tests conducted with either increasing or decreasing 𝐽max. The results indicate that the analyses accurately reproduce transient and steady-state rates of propagation observed in the experimental results, as well as the threshold of propagation. Transient rates of propagation always exceed those in steady state, which underscores the need to understand transients and account for them in fatigue characterization. The results also highlight that a Paris curve for steady-state propagation can be obtained most quickly using a decreasing load function, but that this curve consists of an unconservative bound to the rates of propagation. A lateral shift in the Paris curve is proposed for a conservative characterization that removes the effect of bridging and other R-curve effects.

fracture mechanics; delamination; J-integral↗
NASA NTRS1976

Stagnation region gas film cooling for turbine blade leading edge applications

An experimental investigation was conducted to model the film-cooling performance for a turbine-vane leading edge using the stagnation region of a cylinder in cross flow. Experiments were conducted with a single row of spanwise-angled coolant holes for a range of the coolant blowing ratio with a freestream-to-wall temperature ratio of about 2.1 and a Reynolds number of 170,000, characteristic of the gas-turbine environment. Data from local heat-flux measurements are presented for coolant-hole injection angles of 25, 35, and 45 deg with the row of holes located at three positions relative to the stagnation line on the cylinder. Results show the spanwise (hole-to-hole) variation of heat-flux reduction due to film cooling and indicate conditions for the optimum film-cooling performance.

Luckey, D. W.↗
NASA NTRS1993

Evaluation of scramjet nozzle configurations and film cooling for reduction of wall heating

Experiments on relaminarization, or reverse transition of turbulent flow, have been conducted with a scramjet combustor and nozzle model. The Mach-2.7 direct-connect scramjet combustor employed swept-ramp fuel injectors, and the entering flow simulated Mach-6 to Mach-7 flight conditions. Tests were also conducted without combustor fuel to produce a higher nozzle entrance Mach number and lower pressures. Additional tests were conducted to evaluate the effectiveness of film cooling on the cowl region. At each test condition studied, the entrance radius had no significant effect on the measured downstream wall heating rates. Analysis of the data when fuel was injected into the combustor shows good agreement with turbulent theory; for the tests without fuel injection and combustion, the data downstream of the nozzle entrance radius are intermediate to the calculated turbulent and laminar solutions. Results of film-cooling tests, conducted with both hydrogen and nitrogen injectants, showed that, per unit mass, the hydrogen was approximately three to four times more effective than nitrogen in reducing the downstream wall heating rates.

Baker, N. R.↗
NASA NTRS1981

Tribological properties and thermal stability of various types of polyimide films

Thermal exposure experiments at 315 and 350 C were conducted on seven different types of polyimide films to determine which was the most thermally stable and adherent. The polyimides were ranked according to the rate at which they lost weight and how well they adhere to the metallic substrate. Friction and wear experiments were conducted at 25 C (room temperature) on films bonded to 440C HT stainless steel. Friction, film wear rates, wear mechanisms, and transfer films of the seven films were investigated and compared. The polyimides were found to fall into two groups as far as friction and wear properties were concerned. Group one had lower friction but an order of magnitude higher film wear rate than did group two. The wear mechanism was predominately adhesive, but the size of the wear particles were larger for group one polyimides.

Fusaro, R. L.↗
NASA NTRS1981

Tribological properties and thermal stability of various types of polyimide films

Thermal exposure experiments at 315 and 350 C were conducted on seven different types of polyimide films to determine which was the most thermally stable and adherent. The polyimides were ranked according to the rate of which they lost weight and how well they adhered to the metallic substrate. Friction and wear experiments were conducted at 25 C (room temperature) on films bonded to 440C HT stainless steel. Friction, film wear rates, wear mechanisms, and transfer films of the seven films were investigated and compared. The polyimides were found to fall into two groups as far as friction and wear properties were concerned. Group I had lower friction but an order of magnitude higher film wear rate than did group II. The wear mechanism was predominately adhesive, but the size of the wear particles was larger for group I polyimides.

Fusaro, R. L.↗
NASA NTRS2004

Polyimide/Carbon Nanotube Composite Films for Electrostatic Charge Mitigation

Low color, space environmentally durable polymeric films with sufficient electrical conductivity to mitigate electrostatic charge (ESC) build-up have potential applications on large, deployable, ultra-light weight Gossamer spacecraft as thin film membranes on antennas, solar sails, thermal/optical coatings, multi-layer insulation blankets, etc.. The challenge has been to develop a method to impart robust electrical conductivity into these materials without increasing solar absorptivity (alpha ) or decreasing optical transparency or film flexibility. Since these spacecraft will require significant compaction prior to launch, the film portion of the spacecraft will require folding. The state-of-the-art clear, conductive coating (e.g. indium-tin-oxide, ITO) is brittle and cannot tolerate folding. In this report, doping a polymer with single-walled carbon nanotubes (SWNTs) using two different methods afforded materials with good flexibility and surface conductivities in the range sufficient for ESC mitigation. A coating method afforded materials with minimal effects on the mechanical, optical, and thermo-optical properties as compared to dispersal of SWNTs in the matrix. The chemistry and physical properties of these nanocomposites are discussed.

Smith, Joseph G., Jr.↗
NASA NTRS2003

Hot Films on Ceramic Substrates for Measuring Skin Friction

Hot-film sensors, consisting of a metallic film on an electrically nonconductive substrate, have been used to measure skin friction as far back as 1931. A hot film is maintained at an elevated temperature relative to the local flow by passing an electrical current through it. The power required to maintain the specified temperature depends on the rate at which heat is transferred to the flow. The heat transfer rate correlates to the velocity gradient at the surface, and hence, with skin friction. The hot-film skin friction measurement method is most thoroughly developed for steady-state conditions, but additional issues arise under transient conditions. Fabricating hot-film substrates using low-thermal-conductivity ceramics can offer advantages over traditional quartz or polyester-film substrates. First, a low conductivity substrate increases the fraction of heat convected away by the fluid, thus increasing sensitivity to changes in flow conditions. Furthermore, the two-part, composite nature of the substrate allows the installation of thermocouple junctions just below the hot film, which can provide an estimate of the conduction heat loss.

Noffz, Greg↗
NASA NTRS1977

Effect of ion-plated films of germanium and silicon on friction, wear, and oxidation of 52100 bearing steel

Friction and wear experiments were conducted with ion plated films of germanium and silicon on the surface of 52100 bearing steel both dry and in the presence of mineral oil. Both silicon and germanium were found to reduce wear, with germanium being more effective than silicon. An optimum film thickness of germanium for minimum wear without surface crack formation was found to be approximately 400 nanometers (4000 A). The presence of silicon and germanium on the 52100 bearing steel surface improved resistance to oxidation.

Buckley, D. H.↗
NASA NTRS1994

Experimental studies of shock-wave/wall-jet interaction in hypersonic flow

Experimental studies have been conducted to examine slot film cooling effectiveness and the interaction between the cooling film and an incident planar shock wave in turbulent hypersonic flow. The experimental studies were conducted in the 48-inch shock tunnel at Calspan at a freestream Mach number of close to 6.4 and at a Reynolds number of 35 x 10(exp 6) based on the length of the model at the injection point. The Mach 2.3 planar wall jet was generated from 40 transverse nozzles (with heights of both 0.080 inch and 0.120 inch), producing a film that extended the full width of the model. The nozzles were operated at pressures and velocities close to matching the freestream, as well as at conditions where the nozzle flows were over- and under-expanded. A two-dimensional shock generator was used to generate oblique shocks that deflected the flow through total turnings of 11, 16, and 21 degrees; the flows impinged downstream of the nozzle exits. Detailed measurements of heat transfer and pressure were made both ahead and downstream of the injection station, with the greatest concentration of measurements in the regions of shock-wave/boundary layer interaction. The major objectives of these experimental studies were to explore the effectiveness of film cooling in the presence of regions of shock-wave/boundary layer interaction and, more specifically, to determine how boundary layer separation and the large recompression heating rates were modified by film cooling. Detailed distributions of heat transfer and pressure were obtained in the incident shock/wall-jet interaction region for a series of shock strengths and impingement positions for each of the two nozzle heights. Measurements were also made to examine the effects of nozzle lip thickness on cooling effectiveness. The major conclusion from these studies was that the effect of the cooling film could be readily dispersed by relatively weak incident shocks, so the peak heating in the recompression region was not significantly reduced by even the largest levels of film cooling. For the case studies in the absence of film cooling, the interaction regions were unseparated. However, adding film cooling resulted in regions of boundary layer separation induced in the film cooling layer -- the size of which regions first increased and then decreased with increased film cooling. Surprisingly, the size of the separated regions and the magnitude of the recompression heating were not strongly influenced by the thickness of the cooling film, nor by the point of shock impingement relative to the exit plane of the nozzles. The lip thickness was found to have little effect on cooling effectiveness. Measurements with and in the absence of shock interaction were compared with the results of earlier experimental studies and correlated in terms of the major parameters controlling these flows.

Holden, Michael S.↗
NASA NTRS1994

Experimental studies of shock-wave/wall-jet interaction in hypersonic flow, part A

Experimental studies have been conducted to examine slot film cooling effectiveness and the interaction between the cooling film and an incident planar shock wave in turbulent hypersonic flow. The experimental studies were conducted in the 48-inch shock tunnel at Calspan at a freestream Mach number of close to 6.4 and at a Reynolds number of 35 x 10(exp 6) based on the length of the model at the injection point. The Mach 2.3 planar wall jet was generated from 40 transverse nozzles (with heights of both 0.080 inch and 0.120 inch), producing a film that extended the full width of the model. The nozzles were operated at pressures and velocities close to matching the freestream, as well as at conditions where the nozzle flows were over- and under-expanded. A two-dimensional shock generator was used to generate oblique shocks that deflected the flow through total turnings of 11, 16, and 21 degrees; the flows impinged downstream of the nozzle exits. Detailed measurements of heat transfer and pressure were made both ahead and downstream of the injection station, with the greatest concentration of measurements in the regions of shock-wave/boundary layer interaction. The major objectives of these experimental studies were to explore the effectiveness of film cooling in the presence of regions of shock-wave/boundary layer interaction and, more specifically, to determine how boundary layer separation and the large recompression heating rates were modified by film cooling. Detailed distributions of heat transfer and pressure were obtained in the incident-shock/wall-jet interaction region for a series of shock strengths and impingement positions for each of the two nozzle heights. Measurements were also made to examine the effects of nozzle lip thickness on cooling effectiveness. The major conclusion from these studies was that the effect of the cooling film could be readily dispersed by relatively weak incident shocks, so the peak heating in the recompression region was not significantly reduced by even the largest levels of film cooling. For the case studies in the absence of film cooling, the interaction regions were unseparated. However, adding film cooling resulted in regions of boundary layer separation induced in the film cooling layer, the size of which regions first increased and then decreased with increased film cooling. Surprisingly, the size of the separated regions and the magnitude of the recompression heating were not strongly influenced by the thickness of the cooling film, nor by the point of shock impingement relative to the exit plane of the nozzles. The lip thickness was found to have little effect on cooling effectiveness. Measurements with and in the absence of shock interaction were compared with the results of earlier experimental studies and correlated in terms of the major parameters controlling these flows.

Holden, Michael S.↗
NASA NTRS1975

Effect of free-stream turbulence on film cooling

Film-cooling experiments were conducted at four levels of free-stream turbulence to test the hypothesis that the film-cooling effectiveness is inversely related to the free-stream turbulence level. The hot-gas operating conditions were held constant at a temperature of 590 K, a pressure of 1 atmosphere, and a velocity of 62 m/sec. The film-cooling air was at ambient inlet temperature, and the film-cooling flow rates were 2.5, 5.0, 7.5, and 10.0 percent of the total airflow. Blockage plates with blockage areas of 0, 52, 72, and 90 percent were placed upstream of the film-cooling slot and produced axial turbulence intensities of 7, 14, 23, and 35 percent, respectively. The film-cooling effectiveness decreased as much as 50 percent as the freestream turbulence intensity was increased from 7 to 35 percent. The value of the turbulent mixing coefficient used in previous work was compared with the axial turbulence intensity. The turbulent mixing coefficient was found to be 10 to 40 percent of the axial turbulence intensity.

Marek, C. J.↗
NASA NTRS1998

Method of Forming a Hot Film Sensor System on a Model

A method of forming a hot film sensor directly on a model is provided. A polyimide solution is sprayed onto the model. The model so sprayed is then heated in air. The steps of spraying and heating are repeated until a polyimide film of desired thickness is achieved on the model. The model with the polyimide film thereon is then thoroughly dried in air. One or more hot film sensors and corresponding electrical conducting leads are then applied directly onto the polyimide film.

Tran, Sang Q.↗
NASA NTRS2003

Experimental Evaluation of Hot Films on Ceramic Substrates for Skin-Friction Measurement

An investigation has been performed on the use of low-thermal conductivity, ceramic substrates for hot films intended to measure skin friction. Hot films were deposited on two types of ceramic substrates. Four hot films used composite-ceramic substrates with subsurface thermocouples (TCs), and two hot films were deposited on thin Macor(R) substrates. All six sensors were tested side by side in the wall of the NASA Glenn Research Center 8-ft by 6-ft Supersonic Wind Tunnel (SWT). Data were obtained from zero flow to Mach 1.98 in air. Control measurements were made with three Preston tubes and two boundary-layer rakes. The tests were repeated at two different hot film power levels. All hot films and subsurface TCs functioned throughout the three days of testing. At zero flow, the films on the high-thermal conductivity Macor(R) substrates required approximately twice the power as those on the composite-ceramic substrates. Skin-friction results were consistent with the control measurements. Estimates of the conduction heat losses were made using the embedded TCs but were hampered by variability in coating thicknesses and TC locations.

Noffz, Gregory K.↗
NASA NTRSDate not supplied

Multiphysics Computational Analysis of a Perforated Plate Cooling Flow

A multiphysics analysis of a film cooling flow was conducted using a computational fluid dynamics (CFD) solver in conjunction with a conjugate heat transfer (CHT) solver. The film cooling problem consisted of a square nozzle producing a heated subsonic jet over a perforated plate with three sections of 45 cooling holes each. Results from the multiphysics analysis were compared to a CFD-only approach and experimental results. Reynolds-averaged Navier-Stokes (RANS) computations were employed first, with and without the CHT solver. The multiphysics approach provided much closer agreement with experimentally measured plate temperatures than the CFD-only approach. Comparisons of computed velocities and temperatures were also made with experimental data. Hybrid RANS-large eddy simulation calculations employing the Delayed Detached Eddy Simulation (DDES) approach were also conducted within the multiphysics framework. The DDES approach was unable to resolve turbulent structures in the near wall regions. Hence, the RANS part of the DDES model was used in near wall regions, and produced surface temperatures along with velocity and temperature profiles close to the wall that were very similar to the RANS results. The DDES approach did resolve structures in the outer portion of the boundary layer especially near the end of the plate where the boundary layer was thicker. The key result was the improved surface temperatures produced by the multiphysics approach employing CHT over the fluid-only approach.

Computational Fluid Dynamics↗
NASA NTRS2000

p-n Junction Diodes Fabricated on Si-Si/Ge Heteroepitaxial Films

A set of photolithographic masks was designed for the fabrication of diodes in the Si-Si/Ge material system. Fabrication was performed on samples obtained from two different wafers: (1) a complete HBT structure with an n (Si emitter), p (Si/Ge base), and an n/n+ (Si collector/sub-collector) deposited epitaxially (MBE) on a high resistivity p-Si substrate, (2) an HBT structure where epitaxial growth was terminated after the p-type base (Si/Ge) layer deposition. Two different process runs were attempted for the fabrication of Si-Si/Ge (n-p) and Si/Ge-Si (p-n) junction diodes formed between the emitter-base and base-collector layers, respectively, of the Si-Si/Ge-Si HBT structure. One of the processes employed a plasma etching step to expose the p-layer in the structure (1) and to expose the e-layer in structure (2). The Contact metallization used for these diodes was a Cu-based metallization scheme that was developed during the first year of the grant. The plasma-etched base-collector diodes on structure (2) exhibited well-behaved diode-like characteristics. However, the plasma-etched emitter-base diodes demonstrated back-to-back diode characteristics. These back-to back characteristics were probably due to complete etching of the base-layer, yielding a p-n-p diode. The deep implantation process yielded rectifying diodes with asymmetric forward and reverse characteristics. The ideality factor of these diodes were between 1.6 -2.1, indicating that the quality of the MBE grown epitaxial films was not sufficiently high, and also incomplete annealing of the implantation damage. Further study will be conducted on CVD grown films, which are expected to have higher epitaxial quality.

Das, K.↗
NASA NTRS1987

CuInSe2/ZnSe solar cells using reactively sputter-deposited ZnSe

Results on CuInSe2/ZnSe thin-film heterojunction photovoltaic devices are presented. By the use of reactive magnetron cosputtering of Zn and In dopant in Ar/H2Se, ZnSe thin films have been deposited on glass and conducting SnO2-coated glass substrates with resistivity as low as 20 ohm-cm at deposition temperatures as low as 120 C. Preliminary ZnSe depositions onto CuInSe2 films supplied by industrial laboratories are encouraging. Reactive-sputter-deposition parameters for ZnSe have yet to be optimized for CuInSe2 substrates; however, open-circuit voltages as high as 430 mV were obtained. The highest short-circuit current density, as determined by spectral response weighted for AM1.5 global insulation, was 37.4 mA/sq cm. In all cases, a highly conductive ZnO film was overcoated onto the ZnSe to reduce the overall sheet resistance.

Nouhi, A.↗