Heat treatment for improved stress-corrosion resistance of 17-7 pH stainless steel
Stress corrosion tests of heat treated austenitic stainless steels
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Stress corrosion tests of heat treated austenitic stainless steels
Aluminum-silicon fluxless brazing process for Apollo coldplate fabrication, noting pressure and corrosion test results
Instrumentation and performance of Rankine cycle corrosion test loop with alkali metal
Corrosion tests of coatings for cobalt and nickel base alloys
Rankine system corrosion test evaluation and fabrication
Alkali metal removal from Rankine corrosion test loop, and leakage investigation
Temperature, pressure, and boiling data of tantalum-alloy Rankine system corrosion tests loop after 2000 hr operation
Outdoor high temperature corrosion tests for aluminum alloys and titanium alloys, and stainless steels
Stress corrosion tests of titanium alloys in fluids
Corrosion testing of tantalum for mercury containment in SNAP 8 boiler
Stress corrosion tests of AISI - H-11 alloy steel plated with nickel-cadmium coating
Operation and evaluation of Rankine system corrosion test loop based on refractory alloys
Metallization systems materials for IC, discussing environmental stability, metals electromigration, electrochemical corrosion tests, etc
Evaluation of T-111 refractory alloy Rankine system corrosion test loop
Design, fabrication, and evaluation of T-111 Rankine system refractory alloy corrosion test loop
A sample of cable described as four inches of TV cable, fabric wrapped, which had been exposed to the atmosphere for an unknown period of time, was subjected to extensive chemical analyses for the various components. The fabric was tested using attenuated total reflectance, chloroform extract, aqueous extraction, pyrolysis infrared, and reflectance spectroscopy. The wire insulation was tested using pyrolysis infrared, pyrolysis gas chromatography, differential thermal analysis, attenuated total reflectance subsurface, and tensile tests. Corrosion was also observed in parts of certain wires.
A two inch diameter stainless steel reactor was designed and built to operate at pressures up to 500 psig for the experimental studies on the hydrochlorination of SiCl4 and metallurgical grade (m.g.) silicon metal to SiHCl3. In order to clearly see the effect of pressure, the experiments were carried out at low reactor pressures of 73 psig and 150 psig, respectively. A large pressure effect on the hydrochlorination reaction was observed between the results of the low pressure experiments and the results of the high pressure experiments. In general, higher pressure produces a higher conversion of SiHCl3, but at a lower reaction rate. The effect of temperature on the reaction rate was studied at 73 psig. Higher reaction temperature gave a higher conversion and a higher reaction rate. Samples of the materials used to construct the hydrochlorination reactor were prepared for corrosion tests.
The supporting research and technology effort is intended to provide technical support to the current engine program and also to investigate advanced concepts for the next generation of Stirling engines. Technical areas represented are: seals, materials, engine experiments, combustion, system analysis, cseramics, and tribology. A collage of more recent work in each area is presented. Under seals, analysis and some experimental data on the effect of wear on rod seal performance is presented. The material work described concerns the effect of water content on hydrogen permeation. Results of experiments with the Philips' Advenco engine are presented. A comparison is made of two combustor nozzles, an air atomizing and an ultrasonic atomizing nozzle. A new venture in systems analysis to provide more rigorous Stirling engine simulation is discussed. The results of hydrogen corrosion tests on silicon carbide are presented. Friction and wear tests on candidate materials for engine hot ring tests are discussed.