The use of graphite in high and ultrahigh vacuum - A review
Graphite properties in high and ultrahigh vacuum, suggesting use as electrode material in vacuum gages and residual gas analyzers
Beitel, G. A.↗
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Vacuum MOCVD fabrication of high efficience cells
Vacuum metal-organic-chemical-vapor-deposition (MOCVD) is a new fabrication process with improved safety and easier scalability due to its metal rather than glass construction and its uniform multiport gas injection system. It uses source materials more efficiently than other methods because the vacuum molecular flow conditions allow the high sticking coefficient reactants to reach the substrates as undeflected molecular beams and the hot chamber walls cause the low sticking coefficient reactants to bounce off the walls and interact with the substrates many times. This high source utilization reduces the materials costs power device and substantially decreases the amounts of toxic materials that must be handled as process effluents. The molecular beams allow precise growth control. With improved source purifications, vacuum MOCVD has provided p GaAs layers with 10-micron minority carrier diffusion lengths and GaAs and GaAsSb solar cells with 20% AMO efficiencies at 59X and 99X sunlight concentration ratios. Mechanical stacking has been identified as the quickest, most direct and logical path to stacked multiple-junction solar cells that perform better than the best single-junction devices. The mechanical stack is configured for immediate use in solar arrays and allows interconnections that improve the system end-of-life performance in space.
Partain, L. D.↗
Lubricant life tests on ball bearings for space applications Final report
Ball bearing life tests in vacuum using molybdenum sulfide solid films with high vacuum oils as lubricants
BALL BEARING↗
Improved process for making thin-film sodium niobate capacitors
Sodium niobate, formed by high vacuum, flash, and reactive evaporations, has a high dielectric constant and is used as a thin film dielectric in microelectronic capacitors. High purity films are formed from relatively inexpensive, pure starting materials. Crystalline sodium niobate films can be formed on amorphous or crystalline materials.
Micka, E. Z.↗
Calculated reflectance of aluminum-overcoated iridium in the vacuum ultraviolet from 500 angstrom units to 2000 angstrom units.
High vacuum UV reflectance of opaque iridium overcoated with thin aluminum film, noting possible application in satellite spectrography
Hass, G.↗
MAARSS: Magnet Architectures and Active Radiation Shielding Study
Protecting humans from space radiation is a major hurdle for human exploration of the solar system and beyond. Like on Earth, large magnetic fields surrounding a spaceship would deflect charged particles away from the habitat region and reduce the radiation dose to acceptable limits. The objective of this study is to determine the feasibility of current state of the art (SOA) high temperature superconducting (HTS) magnets as a means to protect crew from space radiation exposure on long duration missions beyond Low Earth Orbit (LEO). The study will look at architecture concepts to deflect high energy Galactic Cosmic Radiation (GCR) and Solar Proton Events (SPEs). Mass, power, and shielding efficiency will be considered and compared with current passive shielding capabilities. This report will walk the reader through several designs considered over the one year study and discuss the multiple parameters that should be evaluated for magnetic shielding. The study team eventually down-selects to a scalable light weight solenoid architecture that is launchable and then deployable using magnetic pressure to expand large diameter coils. Benefitting from the low temperature and high vacuum environment of deep space, existing high-temperature superconductors make such radiation shields realistic, near-term technical developments.
Westover, Shayne C.↗
Relationship between LIBS Ablation and Pit Volume for Geologic Samples: Applications for in situ Absolute Geochronology
In planetary sciences, in situ absolute geochronology is a scientific and engineering challenge. Currently, the age of the Martian surface can only be determined by crater density counting. However this method has significant uncertainties and needs to be calibrated with absolute ages. We are developing an instrument to acquire in situ absolute geochronology based on the K‐Ar method. The protocol is based on the laser ablation of a rock by hundreds of laser pulses. Laser Induced Breakdown Spectroscopy (LIBS) gives the potassium content of the ablated material and a mass spectrometer (quadrupole or ion trap) measures the quantity of 40Ar released. In order to accurately measure the quantity of released 40Ar in cases where Ar is an atmospheric constituent (e.g., Mars), the sample is first put into a chamber under high vacuum. The 40Arquantity, the concentration of K and the estimation of the ablated mass are the parameters needed to give the age of the rocks. The main uncertainties with this method are directly linked to the measures of the mass (typically some μg) and of the concentration of K by LIBS (up to 10%). Because the ablated mass is small compared to the mass of the sample, and because material is redeposited onto the sample after ablation, it is not possible to directly measure the ablated mass. Our current protocol measures the ablated volume and estimates the sample density to calculate ablated mass. The precision and accuracy of this method may be improved by using knowledge of the sample's geologic properties to predict its response to laser ablation, i.e., understanding whether natural samples have a predictable relationship between laser energy deposited and resultant ablation volume. In contrast to most previous studies of laser ablation, theoretical equations are not highly applicable. The reasons are numerous, but the most important are: a) geologic rocks are complex, polymineralic materials; b) the conditions of ablation are unusual (for example, variable vacuum pressure), and c) the ablation is made with hundreds of successive laser pulses. In this work, we aim to understand the effects that occur on LIBS spectra when a homogeneous rock or a mineral is ablated under high vacuum. Understanding these effects is important to define best practices for LIBS measurements and may lead to improved measurement (or possibly prediction) of the ablated volume. We will describe our laboratory approach and first results, and discuss its utility for situ absolute geochronology campaigns.
Devismes, D.↗
Vacuum effects on fatigue properties of magnesium and two magnesium alloys.
High vacuum environment and vacuum outgassing time effects on magnesium alloys fatigue properties under constant load and reversed bending
Sumsion, H. T.↗
Cryogenic connector for vacuum use Patent
Leakproof soft metal seal for use in very high vacuum systems operating at cryogenic temperatures
Kitts, W. T.↗
Silicon source for vacuum deposition
Device using two independent silicon sources for ultra-high-vacuum deposition on large substrates can deposit P and N types of silicon simultaneously. Efficient water cooled copper shield supports and cools structure and isolates two filaments.
Racette, G. W.↗
Ion Storage Tests with the High Performance Antimatter Trap (HiPAT)
The NASA/Marshall Space Flight Centers (NASA/MSFC) Propulsion Research Center (PRC) is evaluating an antiproton storage system, referred to as the High Performance Antiproton Trap (HiPAT). This interest stems from the sheer energy represented by matter/antimatter annihilation process with has an energy density approximately 10 order of magnitude above that of chemical propellants. In other terms, one gram of antiprotons contains the equivalent energy of approximately 23 space shuttle external tanks or ET's (each ET contains roughly 740,000 kgs of fuel and oxidizer). This incredible source of stored energy, if harnessed, would be an enabling technology for deep space mission where both spacecraft weight and propulsion performance are key to satisfying aggressive mission requirements. The HiPAT hardware consists of a 4 Tesla superconductor system, an ultra high vacuum test section (vacuum approaching 10(exp -12) torr), and a high voltage confinement electrode system (up to 20 kvolts operation). The current laboratory layout is illustrated. The HiPAT designed objectives included storage of up to 1 trillion antiprotons with corresponding lifetimes approaching 18 days. To date, testing has centered on the storage of positive hydrogen ions produced in situ by a stream of high-energy electrons that passes through the trapping region. However, due to space charge issues and electron beam compression as it passes through the HiPAT central field, current ion production is limited to less then 50,000 ions. Ion lifetime was determined by counting particle populations at the end of various storage time intervals. Particle detection was accomplished by destructively expelling the ions against a micro-channel plate located just outside the traps magnetic field. The effect of radio frequency (RF) stabilization on the lifetime of trapped particles was also examined. This technique, referred to as a rotating wall, made use of a segmented electrode located near the center of the trap on which various phases of a particular frequency were applied. Various experiments were performed illustrating the ability of an RF drive to both prolong and reduced the lifetimes of various ion species depending on the selected frequency. HiPAT is now being reconfigured for testing with an ion source that will provide both positive and negative hydrogen ions from an external source. This ion system shall provide higher fill capacity (order of million of ions per shot), stacking of multiple shots, and injection schemes typical of a realistic antiproton delivery system.
Martin, James J.↗
Compound Walls For Vacuum Chambers
Proposed compound-wall configuration enables construction of large high-vacuum chambers without having to use thick layers of expensive material to obtain necessary strength. Walls enclose chambers more than 1 m in diameter and several kilometers long. Compound wall made of strong outer layer of structural-steel culvert pipe welded to thin layer of high-quality, low-outgassing stainless steel.
Frazer, Robert E.↗
Solid-film lubricant is effective at high temperatures in vacuum
Calcium fluoride with a suitable inorganic binder forms a stable solid-film lubricant when fused to the surface to be lubricated. It is effective in environments at elevated temperatures and gas pressures ranging from atmospheric to high vacuum. It is not stable in reducing atmospheres.
Sliney, H. E.↗
Housing protects laser in vacuum
Airtight housing encloses laser for easy alinement and operation in high-vacuum chamber. Beam is transmitted through window into vacuum chamber. Flexible line runs through vacuum chamber to outside, maintaining laser enclosure at atmospheric pressure.
Canali, V. G.↗
Laser Induced Rotation of a Levitated Sample in Vacuum
A method of systematically controlling the rotational state of a sample levitated in a high vacuum using the photon pressure is described. A zirconium sphere was levitated in the high-temperature electrostatic levitator and it was rotated by irradiating it with a narrow beam of a high power laser on a spot off the center of mass.
laser induced rotation electrostatic levitator↗
Vacuum in the wake of space vehicles
Vacuum conditions to be encountered in the wakes of high altitude unmanned space vehicles are calculated in order to demonstrate possibilities for conducting experiments using the high pumping speeds and very high vacuum (down to 10 to the -15th torr) attainable. The flux of ambient particles backscattered by emissions from spacecraft surfaces is modelled for an idealized Long Duration Exposure Facility spacecraft structure in an orbit of 550 km altitude. The total backscattered fluxes are found to be between 3 x 10 to the 4th and 3 x 10 to the 5th per sq cm sec for H and between 10 to the 6th and 10 to the 7th per sq cm sec for He and O, depending on the angle with respect to the wake axis. It is found that the direct ambient hydrogen flux is an order of magnitude greater than the backscattered flux, while the backscattered fluxes of He and O are greater than the direct fluxes. It is pointed out that care should be taken in designing space experiments to enable these theoretical conditions to be met.
Oran, W. A.↗
Testing Long-Term Exposure To Vacuum
Facility for studying long-term effects of vacuum on materials described in report. Vacuum storage system maintains specimens at constant temperature and high vacuum. Enables specimens to be removed easily and safely for analysis. Nitrogen storage system maintains specimens at 77 degree F in pure, dry nitrogen gas under gauge pressure of 2 to 4 psi. Enables comparison of control specimens with specimens exposed to vacuum. Instrumentation-and-control system measures and records operating parameters and generates control signals and alarm indications as necessary.
Clark, D. L.↗
Fluid Dynamics of Small, Rugged Vacuum Pumps of Viscous-Drag Type
The need to identify spikes in the concentration of hazardous gases during countdowns to space shuttle launches has led Kennedy Space Center to acquire considerable expertise in the design, construction, and operation of special-purpose gas analyzers of mass-spectrometer type. If such devices could be miniaturized so as to fit in a small airborne package or backpack them their potential applications would include integrated vehicle health monitoring in later-generation space shuttles and in hazardous material detection in airports, to name two examples. The bulkiest components of such devices are vacuum pumps, particularly those that function in the low vacuum range. Now some pumps that operate in the high vacuum range (e.g. molecular-drag and turbomolecular pumps) are already small and rugged. The present work aims to determine whether, on physical grounds, one may or may not adopt the molecular-drag principle to the low-vacuum range (in which case viscous-drag principle is the appropriate term). The deliverable of the present effort is the derivation and justification of some key formulas and calculation methods for the preliminary design of a single-spool, spiral-channel viscous-drag pump.
Russell, John M.↗