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At least 253 records · Page 14

Sixty Earth-Days Test of a Prototype Pt/HTCC Alumina Package in Simulated Venus Environment

This paper presents experimental results of a prototype high temperature co-fired ceramic (HTCC) package with Au/Pt metallization in a three-phase harsh environment test that culminated with 60-day demonstration in simulated Venus surface environment of 465 degrees Centigrade with corrosive atmosphere at 90 bars pressure. The prototype package is based on a previously developed and reported HTCC package successfully tested with multiple analog and digital silicon carbide (SiC) high temperatures semiconductor integrated circuits (ICs) at NASA Glenn Research Center in 500 degrees Centigrade Earth air ambient for over ten thousand hours, and short-term tested at temperatures above 800 degrees Centigrade. The three-phase harsh environment test started with 48 hours in 465 degrees Centigrade Earth air, followed by 48 hours in 465 degrees Centigrade nitrogen at 90-bar pressure and 1400 hours in simulated Venus surface environment of 465 degrees Centigrade with corrosive atmosphere at 90 bars. Initial analytical results of the package materials and surfaces after exposure to the Venus environment are discussed to assess the stability of the packaging materials in the tested environments. The test in a simulated Venus environment was implemented in the NASA Glenn Extreme Environment Rig (GEER). The results of this study suggest that an effective encapsulation of areas of surface metallization and vicinities may help to improve electrical performance of a HTCC alumina packaging system in Venus environment.

Chen, Liang-Yu↗

High Density Packaging Technologies for RF Electronics in Small Spacecraft

This paper will describe a few high density packaging technologies which we are currently exploring for use in current and future small spacecraft applications. The three categories of technologies include organic multichip modules (MCMs), ceramic leadless surface mount technology (SMT) and 3D printed waveguide structures. There are many other packaging technologies that currently exist but these three were selected in part due to their long heritage in various commercial, military and space applications along with each having a relatively clear path to flight. For each of these technologies, detailed examples will be included in which hardware has been fabricated and tested for use in RF electronics for spacecraft transponders. The organic MCM example will be described in most detail and it utilizes a packaging technology by the name of CoreEZ which is a trademark of i3 Electronics. This MCM has shrunk a portion of our electronics down to 1/8th of its previous area. The CoreEZ technology has been shown to be rad hard beyond a total ionizing dose (TID) of 300kRad and the MCM which was fabricated has gone through thermal cycling and shown to have no degradation in performance. The ceramic leadless package examples include packages from high reliability manufactures by the name of KCB solutions and Barry Industries. In the case of KCB solutions, we have multiple products that will be described including a hermetic ceramic carrier which houses three microwave monolithic integrated circuits (MMICs) along with small discrete components. Finally, we will discuss the results of our search for a 3D printing process that allows us to reduce the cost and volume of our waveguide filters and diplexers for low cost small satellite applications. We have fabricated a few prototypes using direct metal laser sintering (DMLS) and metal coated plastics. Each of these packaging technology discussions will have a brief overview of its current and future use.

Aquirre, Fernando↗

High Density Packaging Technologies for RF Electronics in Small Spacecraft

This paper will describe a few high density packaging technologies which we are currently exploring for use in current and future small spacecraft applications. The three categories of technologies include organic multichip modules (MCMs), ceramic leadless surface mount technology (SMT) and 3D printed waveguide structures. There are many other packaging technologies that currently exist but these three were selected in part due to their long heritage in various commercial, military and space applications along with each having a relatively clear path to flight. For each of these technologies, detailed examples will be included in which hardware has been fabricated and tested for use in RF electronics for spacecraft transponders. The organic MCM example will be described in most detail and it utilizes a packaging technology by the name of CoreEZ which is a trademark of i3 Electronics. This MCM has shrunk a portion of our electronics down to 1/8th of its previous area. The CoreEZ technology has been shown to be rad hard beyond a total ionizing dose (TID) of 300kRad and the MCM which was fabricated has gone through thermal cycling and shown to have no degradation in performance. The ceramic leadless package examples include packages from high reliability manufactures by the name of KCB solutions and Barry Industries. In the case of KCB solutions, we have multiple products that will be described including a hermetic ceramic carrier which houses three microwave monolithic integrated circuits (MMICs) along with small discrete components. Finally, we will discuss the results of our search for a 3D printing process that allows us to reduce the cost and volume of our waveguide filters and diplexers for low cost small satellite applications. We have fabricated a few prototypes using direct metal laser sintering (DMLS) and metal coated plastics. Each of these packaging technology discussions will have a brief overview of its current and future use.

Schatzel, Donald↗

Determing Degradation Of Fiberboard In The 9975 Shipping Package By Measuring Axial Gap

Currently, thousands of model 9975 transportation packages are in use by the US Department of Energy (DOE); the design of which has been certified by DOE for shipment of Type B radioactive and fissile materials in accordance with Part 71, Title 10 Code of Federal Regulations (CFR), or 10 CFR 71, Packaging and Transportation of Radioactive Material. These transportation packages are also approved for the storage of DOE-STD-3013 containers at the Savannah River Site (SRS). As such, the 9975 has been continuously exposed to the service environment for a period of time greater than the approved transportation service life. In order to ensure the material integrity as specified in the safety basis, an extensive surveillance program is in place in K-Area Complex (KAC) to monitor the structural and thermal properties of the fiberboard of the 9975 shipping packages. The surveillance approach uses a combination of Non-Destructive Examination (NDE) field surveillance and Destructive Examination (DE) lab testing to validate the 9975 performance assumptions. The fiberboard in the 9975 is credited with thermal insulation, criticality control and resistance to crushing. During surveillance monitoring in KAC, an increased axial gap of the fiberboard was discovered on selected items packaged at Rocky Flats Environmental Technology Site (RFETS). Many of these packages were later found to contain excess moisture. Savannah River National Laboratory (SRNL) testing has resulted in a better understanding of the relationship between the fiberboard moisture level and compaction of the fiberboard under storage conditions and during transport. In laboratory testing, the higher moisture content has been shown to correspond to higher total compaction of fiberboard material and compaction rate. The fiberboard height is reduced by compression of the layers. This change is observed directly in the axial gap between the flange and the air shield. The axial gap measurement is made during the pre-use inspection or during the annual recertification process and is a screening measurement for changes in the fiberboard.

42 ENGINEERING↗

TYPE A FISSILE PACKAGING FOR AIR TRANSPORT PROJECT OVERVIEW

This paper presents the project status of the Model 9980, a new Type A fissile packaging for use in air transport. The Savannah River National Laboratory (SRNL) developed this new packaging to be a light weight (<150-lb), drum-style package and prepared a Safety Analysis for Packaging (SARP) for submission to the DOE/EM. The package design incorporates unique features and engineered materials specifically designed to minimize packaging weight and to be in compliance with 10CFR71 requirements. Prototypes were fabricated and tested to evaluate the design when subjected to Normal Conditions of Transport (NCT) and Hypothetical Accident Conditions (HAC). An overview of the design details, results of the regulatory testing, and lessons learned from the prototype fabrication for the 9980 will be presented.

42 ENGINEERING↗

PVAnalytics: A Python Package for Automated Processing of Solar Time Series Data

Multiple publicly available software packages exist that analyze solar time series data, including RdTools and Solar Data Tools, among others. Several of these packages contain their own unique quality assurance (QA) and feature recognition algorithms. The python PVAnalytics package was developed to offer an internally consistent source for these analysis tools, making it easier for the end user to deploy these routines on his or her solar data. The PVAnalytics package currently contains routines for outlier detection, inverter clipping detection, irradiance and temperature checks, orientation checks, and data shift detection, among other functions. These functions have been aggregated from various sources including Solar Forecast Arbiter, RdTools, and the QA process developed by NREL's PV Fleets Initiative. We are continuously adding new functionality to the package, including documentation, examples and algorithms. By bundling QA functionality into a single software package, we hope to make PVAnalytics a comprehensive software library to support analysis of solar metadata and time series data.

data cleaning↗

Cold-Climate Packaged Heat Pumps - Resistance is Futile

The U.S. currently has a large market for room/zonal space conditioning equipment focused primarily on cooling, namely packaged terminal air conditioners (PTACs), packaged terminal heat pumps (PTHPs), and room air conditioners. This equipment largely relies on electric resistance for heating, particularly when outdoor temperatures fall to 40°F or below, presenting a compelling opportunity for energy savings and carbon reductions from reverse cycle heating. This paper provides an overview of cold climate packaged heat pump technologies in the market capable of high output down to outdoor temperatures of 5°F and identifies the technological and market barriers to adoption. For state-of-the-art cold climate packaged heat pumps sold in the retrofit market, defrost meltwater management is the principal barrier to implementation. An energy use analysis is conducted on state-of-the-art cold climate packaged heat pumps for heating and cooling loads by building vintage and climate zone. Potential solutions to defrost meltwater are proposed and modeled for their impact on heating energy efficiency. A national impact assessment estimates the aggregate energy savings and carbon reductions if cold climate packaged heat pumps were to replace existing PTACs and PTHPs in the U.S. building stock. A national, two-track approach is proposed for increasing market adoption in the replacement and new construction markets.

ACEEE Summer Study, cold climate, heat pumps, ccph↗

Conceptual Design of the Package Handling System for the Deep Borehole Engineering Demonstration - 17064

Deep borehole disposal involves drilling one or more boreholes into crystalline basement rock to a depth of about 5 km, emplacing waste packages in the lower 2 km of the borehole, and sealing and plugging the upper 3 km. These depths are several times deeper than for typical mined repositories. A deep borehole field test (DBFT) is proposed to confirm the safety and feasibility of the deep borehole concept. The primary goals are to demonstrate the construction and characterization of deep boreholes, demonstrate the equipment and operations used for safe waste handling and emplacement downhole, study geologic controls on waste form stability and isolation, and evaluate the overall safety and practicality of the concept. The test will be conducted using simulated waste packages; no radioactive wastes will be handled at the deep borehole field test site. A key component of the DBFT is an engineering demonstration of the equipment and operations needed to transport waste packages to the site, move packages between the transportation and emplacement systems, and lower or retrieve packages into or out of the borehole. This paper describes the conceptualization of test package handling, from transportation and receipt through the interface with the borehole. It also describes the use of an integrated test facility to check out equipment prior to deployment at the DBFT site, and performance of the engineering demonstration at the DBFT site. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Standards and Guidelines for the Design of Trunnions of RAM Transport Packages - 17365

Trunnion systems of packages for the transport of radioactive materials have to guarantee the safe handling of package during crane operations (lifting, tilting) and to secure package tie down to the transport vehicle, if the trunnions are used as attachment points during transport. The design of trunnions is based on IAEA Regulations SSR-6, the supporting Advisory Material SSG-26 and further appropriate technical standards and/or guidelines. For package approval procedures in Germany the guideline BAM-GGR 012 has to be applied. If a package is handled inside a german nuclear power plant, the standard KTA 3905 has to be fulfilled additionally. In this paper the requirements of KTA 3905 [4] concerning the trunnion systems as load attaching points (LAP) are discussed in connection with the recommendations in the guideline BAM-GGR 012 [3]. This guideline is prepared at BAM Federal Institute for Materials Research and Testing for analysis and assessment of bolted lid and trunnion systems of Type B(U) transport packages. The quality assurance questions concerning trunnion systems are discussed as well. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

MP197HB; First licensed transportation package with canistered high burnup fuel after dry storage - 15580

AREVA TN has recently received the NRC 10 CFR Part 71 transportation license CoC 9302 Revision 7 for the MP197HB transportation package that allows transportation of canistered high burnup fuel assemblies. The Nuclear Horizontal Modular Storage (NUHOMS{sup R}) system canisters containing high burnup PWR and BWR fuel assemblies are now licensed for transportation as a payload in MP197HB after these canisters were in dry storage at the utility ISFSIs. Enhancements have been made to the MP197HB transportation package to improve thermal performance and also provide superior shielding capabilities. Design features of existing AREVA TN transportation packages such as radial fins, thermal shield, neutron resin and optimized gamma and neutron shielding were used to accommodate transportation of high burnup fuel assemblies with heat loads up to 32 kW. The transportation package is designed for exclusive use by rail, truck or marine transport. State-of-the-art analyses methodologies were used to demonstrate compliance with regulatory requirements of 10 CFR 71.55 for the high burnup fuel after dry storage at any ISFSI. Some of the issues addressed in the license application related to the transportation of high burnup fuel included potential degradation of fuel cladding, uncertainty associated with high burnup fuel cladding material properties, and larger radiation and thermal sources due to higher burnups. Bounding conservative assumptions were made where limited test data was available. AREVA TN's licensing approach did not rely on the cladding integrity of high burnup fuel cladding. Instead, the criticality, thermal and shielding analyses were carried out assuming high burnup fuel reconfiguration. With the approval of this transportation package for PWR and BWR canistered high burnup fuel from dry storage at ISFSIs, the utilities can now transport these canisters which are in dry storage at their sites. This is also a major step forward for the canistered fuel that is currently in dry storage at the shutdown plants because they can use this AREVA TN MP197HB transportation package to ship that fuel to any interim storage facility (ISF) or to a repository when they become available. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Safety analysis report for packaging shielding and nuclear criticality safety courses developed and conducted by Oak Ridge National Laboratory

The US Department of Energy (DOE) Packaging Certification Program, Office of Packaging and Transportation, is offering Safety Analysis Report for Packaging (SARP) Shielding and Nuclear Criticality Safety (NCS) courses for SARP generalists and analysts. The SARP generalist course is designed for project managers, supervisors, NCS/shielding subject matter experts (SME), and SMEs in non-NCS/shielding technical areas (e.g., structural, thermal, package design) who need to better understand how NCS/shielding analyses fit into the broader body of SARP documentation. The generalist course provides an overview of the regulations and guidelines for the criticality and shielding analyses for a SARP and illustrates how the NCS/shielding chapters integrate with the other parts of the SARP. After course material is presented, students in the generalist course will review an actual SARP document to examine key elements of the shielding and criticality analyses. The analyst course provides detailed instructions on the radioactive material package shielding analyses and NCS evaluation fundamentals needed by analysts/practitioners (i.e., safety analysts and/or technical reviewers) to prepare and/or review technical analyses for the SARP documentation. The analyst course also provides an overview of regulations and guidelines, in addition to detailed in-class exercises associated with package shielding and NCS analyses. Analysis teams will be faced with staged SARP examples in which several important decision processes in the generation of a SARP will be demonstrated and discussed. The courses are offered at Oak Ridge National Laboratory's National Transportation Research Center. (authors)

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Fiber-optic sensor packaging assessment and benchmarking for embedded sensing applications

Fiber optic-based sensing for non-destructive evaluation (NDE) and structural health monitoring of various infrastructure and energy assets is an increasingly important sensing scheme. Because of their immunity to electromagnetic interferences, versatility in sensing mechanisms and designs as well as capability for distributed sensing, the fiber optic sensing is of great interest for embedding within infrastructures using advanced manufacturing methods. However, the protection of fiber optic sensors during advanced manufacturing-based embedding is an important aspect for infrastructure monitoring in practice. While successful installation of fiber optic sensors has been accomplished through application of epoxy or adhesives on infrastructure surfaces, there has been only limited investigation of fiber protection packaging schemes which are compatible with in-situ repair techniques such as the metallic cold-spray. With increasing interest and importance of cold spray-based repair processes, the integration of fiber optic sensors simultaneously during the repair is equally important. In this work, we focus our efforts on investigating various types of packaging schemes for their compatibility and integrability on the surfaces of metallic structures such as oil and gas pipelines during an in-situ repair coating. First, we consider sandblasting using silica sand particles of various size for optical fibers on the surface of a metallic coupon as a useful proxy test of sensor packaging stability. Structural damage of packaging is characterized by means of optical microscopy and the optical integrity of embedded fiber optic cables is examined using optical backscatter reflectometry (OBR). In addition, initial investigation of metallic cold-spray embedded fiber optic cables under various packaging on metallic substrates is also considered with early conclusions and future directions.

Fiber-optic sensors, Sensors packaging, Metallic C↗

Development and Demonstration of a Risk Assessment Approach for Approval of a Transportation Package of a Transportable Nuclear Power Plant for Domestic Highway Shipment

The U.S. Department of Defense (DoD) Strategic Capabilities Office (SCO) has tasked PNNL to address the regulatory challenges associated with confirming the safe transport of Transportable Nuclear Power Plants (TNPPs) containing irradiated nuclear fuel. A previous report—Proposed Risk-Informed Regulatory Framework for Approval of Microreactor Transportation Packages (PNNL-31867)—determined that the expected radioactive inventory in the irradiated fuel of a TNPP would likely require shipment in an NRC-approved Type B package (or spent nuclear fuel cask) but that a TNPP “package” is unlikely to meet the entire suite of NRC requirements set forth in Part 71 of Title 10 of the Code of Federal Regulations (CFR) for a Type B package. It was therefore concluded that shipment of this initial TNPP transportation package, as well as possibly others, under existing regulations would likely require NRC approval using the 10 CFR 71.12 (“Specific exemptions”) process that relies on risk-informed decision making supported by quantitative risk assessment (i.e., Probabilistic Risk Assessment).

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Life cycle assessment of a packaging waste recycling system in Portugal

Highlights: • We modeled a real packaging waste recycling system. • The analysis was performed using the life cycle assessment methodology. • The 2010 situation was compared with scenarios where the materials were not recycled. • The “Baseline” scenario seems to be more beneficial to the environment. - Abstract: Life Cycle Assessment (LCA) has been used to assess the environmental impacts associated with an activity or product life cycle. It has also been applied to assess the environmental performance related to waste management activities. This study analyses the packaging waste management system of a local public authority in Portugal. The operations of selective and refuse collection, sorting, recycling, landfilling and incineration of packaging waste were considered. The packaging waste management system in operation in 2010, which we called “Baseline” scenario, was compared with two hypothetical scenarios where all the packaging waste that was selectively collected in 2010 would undergo the refuse collection system and would be sent directly to incineration (called “Incineration” scenario) or to landfill (“Landfill” scenario). Overall, the results show that the “Baseline” scenario is more environmentally sound than the hypothetical scenarios.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

PET based nanocomposite films for microwave packaging applications

In recent years, changes in life standards have promoted the diffusion of Ready to Cook (RTC) and Ready to Eat (RTE) products for microwave ovens. However, the main limits in microwave (MW) ovens usage are often related to the proper choice of packaging materials suitable for such technology. In fact, packages for microwaveable RTC and RTE foods should ensure adequate preservation of the product before cooking/heating such as high barriers to gases and aromas and adequate control of water vapor transmission. In addition, microwaveable packaging material must be transparent to MW, thermally stable and resistant to the mechanical stress induced by the accumulation in the head space of volatile substances produced during the cooking. Polymeric materials are good candidates for microwaveable packaging thanks to their transparency to MW. In the last years a great interest is devoted to developing innovative solution based on the use of additives or systems that act as susceptors or heating enhancers for improving the characteristics of polymers in cooking/heating in MW ovens. The present work was focused on the production and characterization of nanocomposite copolyester based films suitable for microwaveable food packaging applications. The matrices selected consist in two PET copolymers modified with carbon black (ULTRA STD) and with titanium oxide (ULTRA NA). Nanocomposite co-extruded multilayer films were produced using different percentages (0%, 2% and 4%wt/wt) of Cloisite 20A (C20A). Films were analyzed for evaluating the effect of nanofiller on the morphology and barrier properties. Moreover, to verify the effectiveness of the designed systems in reducing the cooking times of meat products, MW heating tests were carried out on pork meat hamburgers in MW oven at varying supplied powers. The cooking tests have pointed out that the selected matrices are efficient in reducing cooking times and that even low concentration of C20A acts as heating enhancers of PET.

77 NANOSCIENCE AND NANOTECHNOLOGY↗

Material Needs and Measurement Challenges for Advanced Semiconductor Packaging: Understanding the Soft Side of Science

This Perspective builds upon insights from the National Institute of Standards and Technology (NIST)-organized workshop, “Materials and Metrology Needs for Advanced Semiconductor Packaging Strategies,” held at the 35th annual Electronics Packaging Symposium in Binghamton, NY, on September 5, 2024. It outlines critical challenges and opportunities related to polymer-based “soft” materials in advanced semiconductor packaging, with emphasis on polymer science, measurement science (metrology), and the strategic development of Research-Grade Test Materials (RGTMs). These efforts, led by the NIST CHIPS team, aim to advance the fundamental understanding of structure-property-processing relationships, promote standardized guidelines and innovative methods for material characterization, and accelerate the development, qualification, and adoption of next-generation packaging materials. The Perspective also distills key insights from the panel discussion with industry experts, emphasizing the need for close collaboration among materials scientists, process engineers, and metrology experts to enable a holistic strategy, further highlighting the importance of cross-sector partnerships among industry, academia, and government to address pressing challenges in packaging materials and processes.

97 MATHEMATICS AND COMPUTING↗

The Model 9977 Radioactive Material Packaging Primer

The Model 9977 Packaging is a single containment drum style radioactive material (RAM) shipping container designed, tested and analyzed to meet the performance requirements of Title 10 the Code of Federal Regulations Part 71. A radioactive material shipping package, in combination with its contents, must perform three functions (please note that the performance criteria specified in the Code of Federal Regulations have alternate limits for normal operations and after accident conditions): Containment, the package must “contain” the radioactive material within it; Shielding, the packaging must limit its users and the public to radiation doses within specified limits; and Subcriticality, the package must maintain its radioactive material as subcritical

42 ENGINEERING↗

Materials Assessment of Insulating Foam in the 9977 Shipping Package for Long-Term Storage - Annual Report

The 9977 shipping package is being evaluated for long-term storage applications in the K-Area Complex (KAC) with specific focus on the packaging foam material. A rigid closed cell polyurethane foam, LAST-A-FOAM® FR-3716, produced by General Plastics Manufacturing Company is sprayed and expands to fill the void between the inner container and the outer shell of the package. The foam is sealed in this annular space and is not accessible. During shipping and storage, the foam experiences higher than ambient temperatures from the heat generated by nuclear material within the package creating the potential for degradation of the foam. A series of experiments is underway to determine the extent of foam degradation. Foam samples of three densities have been aging at elevated temperatures 160 °F, 160 °F + 50% relative humidity (RH), 185 °F, 215 °F, and 250 °F since 2014. Samples were periodically removed and tested. After approximately 80 weeks, samples conditioned at 160 °F, 160 °F + 50% RH, and 185 °F have retained initial property values while samples conditioned at 215 °F have reduced intumescence. Samples conditioned at 250 °F have shown the most degradation, loss of volume, mass, absorbed energy under compression, intumescence, and increased flammability. Based on the initial data, temperatures up to 185 °F have not yet shown an adverse effect on the foam properties and it is recommended that exposure of FR-3716 foam to temperatures in excess of 250 °F be avoided or minimized. Testing will continue beyond the 96 week mark. This will provide additional data to help define the long-term behavior for the lower temperature conditions. Additional testing will be pursued in an attempt to identify transition points (threshold times and temperatures) at the higher temperatures of interest, as well as possible benefits of aging within the relatively oxygen-free environment the foam experiences inside the 9977 shipping package.

36 MATERIALS SCIENCE↗