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At least 253 records · Page 14

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NASA NTRS2012

Spectroscopic Chemical Analysis Methods and Apparatus

This invention relates to non-contact spectroscopic methods and apparatus for performing chemical analysis and the ideal wavelengths and sources needed for this analysis. It employs deep ultraviolet (200- to 300-nm spectral range) electron-beam-pumped wide bandgap semiconductor lasers, incoherent wide bandgap semiconductor lightemitting devices, and hollow cathode metal ion lasers. Three achieved goals for this innovation are to reduce the size (under 20 L), reduce the weight [under 100 lb (.45 kg)], and reduce the power consumption (under 100 W). This method can be used in microscope or macroscope to provide measurement of Raman and/or native fluorescence emission spectra either by point-by-point measurement, or by global imaging of emissions within specific ultraviolet spectral bands. In other embodiments, the method can be used in analytical instruments such as capillary electrophoresis, capillary electro-chromatography, high-performance liquid chromatography, flow cytometry, and related instruments for detection and identification of unknown analytes using a combination of native fluorescence and/or Raman spectroscopic methods. This design provides an electron-beampumped semiconductor radiation-producing method, or source, that can emit at a wavelength (or wavelengths) below 300 nm, e.g. in the deep ultraviolet between about 200 and 300 nm, and more preferably less than 260 nm. In some variations, the method is to produce incoherent radiation, while in other implementations it produces laser radiation. In some variations, this object is achieved by using an AlGaN emission medium, while in other implementations a diamond emission medium may be used. This instrument irradiates a sample with deep UV radiation, and then uses an improved filter for separating wavelengths to be detected. This provides a multi-stage analysis of the sample. To avoid the difficulties related to producing deep UV semiconductor sources, a pumping approach has been developed that uses ballistic electron beam injection directly into the active region of a wide bandgap semiconductor material.

Hug, William F.↗

NASA NTRS1977

Copernicus observations of Nova Cygni 1975

Near-ultraviolet radiation from Nova Cygni 1975 was detected by the Copernicus satellite on five occasions from 1975 September 1 to 1975 September 9. The nova was not seen in the UV after this date. The principal result was the observation of a broad emission feature from the Mg II doublet at 2800 A. The absence of strong UV radiation at shorter wavelengths suggests that these lines are produced by collisional excitation in the outer layers of an expanding shell with electron temperature of approximately 4000 K. The absence of observed emission lines from highly ionized species indicates that the amount of material with log T between 4.4 and 5.7 is less than 0.001 times that which produces the Mg II emission. The continuum flux in the near-UV decreased as the nova evolved, showing that the total luminosity decreased as the nova faded in the visible.

Jenkins, E. B.↗

NASA NTRS1993

Absorption of solar radiation by O2 - Implications for O3 and lifetimes of N2O, CFCl3, and CF2Cl2

An accurate line-by-line model is used to evaluate effects of absorption in the Schumann-Runge bands of O2 on transmission of UV radiation. The model is used to evaluate rates of photolysis for N2O, CFCl3, and CF2Cl2, and to infer global loss rates and instantaneous lifetimes appropriate for 1980. A parameterized version of the line-by-line model enabling rapid evaluation of transmission in the Schumann-Runge region is described. Photochemical calculations employing the parameterization and constrained by data from the Atmospheric Trace Molecule Spectroscopy experiment are used to examine the budget of odd oxygen. Consistent with previous studies, it is shown that photochemical loss of odd oxygen exceeds production by photolysis of O2 for altitudes above 40 km. The imbalance between production and loss is shown to be consistent with a source of odd oxygen proportional to the product of the mixing ratio and photolysis rate of ozone, which suggests that processes involving vibrationally excited O2 may play an important role in production of odd oxygen.

Minschwaner, K.↗

NASA NTRS1974

Extreme ultraviolet spectrometer for space research

A normal incidence spectrometer for use in the wavelength region from 200 to 1270 A has been developed. The design and calibration of the instrument are described in detail. The spectrometer can be employed to detect extreme UV radiation at a minimum flux level of 1 rayleigh with a spectral resolution of 40 A and a spatial resolution of 6 deg. Data on the extreme UV night sky spectrum between 780 and 1270 A obtained with this instrument on a recent rocket flight are presented.

Kumar, S.↗

NASA NTRS1978

Photocatalytic oxidation of organic compounds on Mars

Ultraviolet-stimulated catalytic oxidation is proposed as a mechanism for the destruction of organic compounds on Mars. The process involves the presence of gaseous oxygen, UV radiation, and a catalyst (titanium dioxide), and all three of these have been found to be present in the Martian environment. Therefore it seems plausible that UV-stimulated oxidation of organics is responsible for degrading organic molecules into inorganic end products.

Chun, S. F. S.↗

NASA NTRS1980

On the relationship between secular brightness changes of Titan and solar variability

Titan's geometric albedo varied noticeably from 1972 to 1978, in phase with variations in solar activity (Lockwood and Thompson, 1979). A series of radiative transfer and aerosol formation calculations were made to demonstrate the feasibility of the following scenario for these secular brightness changes. Solar activity changes, especially in the UV output of the sun, result in alterations to the mass production rate of aerosols in Titan's atmosphere, which lead to modifications of their microphysical properties. The latter, in turn, cause the albedo to vary. Current estimates of the change in the solar UV radiation below the dissociation limit of methane imply alterations to the mean radius of the aerosols over an 11-yr solar cycle that are consistent in sign and magnitude with those required to explain the observed secular brightness changes.

Pollack, J. B.↗

NASA NTRS1998

Radiation Induced Degradation of White Thermal Control Paint

This paper details a comparison analysis of the Zinc Oxide pigmented white thermal control paints Z-93 and Z-93P. Both paints were simultaneously exposed to combined space environmental effects and analyzed using an in-vacuum reflectance technique. The dose applied to the paints was approximately equivalent to 5 years in a geosynchronous orbit. This comparison analysis showed that Z-93P is an acceptable substitute for Z-93. Irradiated samples of Z-93 and Z-93P were subjected to additional exposures of ultraviolet (UV) radiation and analyzed using the in-vacuum reflectance technique to investigate UV activated reflectance recovery. Both samples showed minimal UV activated reflectanc6 recovery after an additional 190 Equivalent Sun Hour (ESH) exposure. Reflectance response utilizing nitrogen as a repressurizing gas instead of air was also investigated. This investigation found the rates of reflectance recovery when repressurized with nitrogen are slower than when repressurized with air.

Edwards, D. L.↗

DOE OSTI2021

Preliminary Studies of UV Photolysis of Gas-phase CH3I in Air: Time-resolved Infrared Identification of Methanol and Formaldehyde Products

Halogen-bearing compounds are known to photolyze under UV radiation; analysis of degradation products is of interest for both safety and environmental considerations. Time-resolved infrared spectroscopy was used in the laboratory to study the UV-photolysis of methyl iodide. Photolysis products methanol (CH3OH) and formaldehyde (HCHO) were clearly identified in a time-resolved manner. Preliminary kinetic models predict the formation of both CH3OH and HCHO.

Hughey, Kendall D.↗

NASA NTRS1998

Radiation Induced Degradation of White Thermal Control Paint

This paper details a comparison analysis of the zinc-oxide pigmented white thermal control paints Z-93 and Z-93P. Both paints were simultaneously exposed to combined space environmental effects and analyzed using an in-vacuo reflectance technique. The dose applied to the paints was approximately equivalent to 5 yr in a geosynchronous orbit. This comparison analysis showed that Z-93P is an acceptable substitute for Z-93. Irradiated samples of Z-93 and Z-93P were subjected to additional exposures of ultraviolet (UV) radiation and analyzed using the in-vacuo reflectance technique to investigate UV activated reflectance recovery. Both samples showed minimal UV activated reflectance recovery after an additional 190 equivalent Sun hour (ESH) exposure. Reflectance response utilizing nitrogen as a repressurizing gas instead of air was also investigated. This investigation found the rates of reflectance recovery when repressurized with nitrogen are slower than when repressurized with air.

Edwards, D. L.↗

NASA NTRS1999

Radiation Induced Degradation of White Thermal Control Paint

Edwards, D. L.↗

NASA NTRS2004

Did a Gamma-Ray Burst Initiate the Late Ordovician Mass Extinction?

Gamma-ray bursts (hereafter GRB) produce a flux of radiation detectable across the observable Universe. A GRB within our own galaxy could do considerable damage to the Earth's biosphere; rate estimates suggest that a dangerously near GRB should occur on average several times per billion years. At leastfive times in the history of lfe, the Earth experienced mass extinctions that eliminated a large percentage of the biota. Many possible causes have been documented, and GRB may also have contributed. The late Ordovician mass extinction approximately 440 million years ago may be at least partly the result of a GRB. Due to severe depletion of the ozone layer, intense solar ultraviolet radiation is expected to result from a nearby GRB, and some of the patterns of extinction and survivorship at this time may be attributable to elevated levels of UV radiation reaching the Earth. In addition a GRB could trigger the global cooling which occurs at the end of the Ordovician period that follows an interval of relatively warm climate. Intense rapid cooling and glaciation at that time, previously identijied as the probable cause of this mass extinction, may have resultedfiom a GRB.

Melott, A. L.↗

NASA NTRS1996

Radiation Induced Degradation of the White Thermal Control Paints Z-93 and Z-93P

This paper details a comparison analysis of the zinc oxide pigmented white thermal control paints Z-93 and Z-93P. Both paints were simultaneously exposed to combined space environmental effects and analyzed using an in-vacuo reflectance technique. The dose applied to the paints was approximately equivalent to 5 years in a geosynchronous orbit. This comparison analysis showed that Z-93P is an acceptable substitute for Z-93. Irradiated samples of Z-93 and Z-93P were subjected to additional exposures of ultraviolet (UV) radiation and analyzed using the in-vacuo reflectance technique to investigate UV activated reflectance recovery. Both samples showed minimal UV activated reflectance recovery after an additional 190 equivalent sun hour (ESH) exposure. Reflectance response utilizing nitrogen as a repressurizing gas instead of air was also investigated. This investigation found the rates of reflectance recovery when repressurized with nitrogen are slower than when repressurized with air.

Edwards, D. L.↗

NASA NTRS1974

Ion composition and drift observations in the nighttime equatorial ionosphere

The first in situ measurements of ion composition in the nighttime equatorial E and F region ionospheres (90-300 km) are presented and discussed. These profiles were obtained by two rocket-borne ion mass spectrometers launched from Thumba, India on March 9-10, 1970 at solar zenith angles of 112 deg and 165 deg. Ionosonde data established that the composition was measured at times bounding a period of F region downward drift. During this period the ions O(+) and N(+) were enhanced by one to three orders of magnitude between 220 and 300 km. Below the drift region (200 km), O(+) ceased to be the major ionic constituent, but the concentrations of O(+) and N(+) remained larger than predicted from known radiation sources and loss processes. Here also, both the O2(+) and NO(+) profiles retained nearly the same shape and magnitude throughout the night in agreement with theories assuming scattered UV radiation to be the maintaining source. Light metallic ions including Mg(+), Na(+) and possibly Si(+) were observed to altitude approaching 300 km, while the heavier ions Ca(+) and K(+) were seen in reduced quantity to 200 km. All metal ion profiles exhibited changes which can be ascribed to vertical drifting.

Goldberg, R. A.↗

NASA NTRS1980

Scientific objectives of the Solar Mesosphere Explorer mission

The paper describes the NASA Solar Mesosphere Explorer mission which will study mesospheric ozone and the processes which form and destroy it, measure the ozone density and its altitude distribution from 30 to 80 km, monitor incoming solar UV radiation, and provide a rigorous test of the photochemical equilibrium theory of the mesospheric oxygen-hydrogen system. Five instruments will be carried on the polar-orbiting spacecraft: UV ozone, IR airglow, and visible NO2 programmable Ebert-Fastie spectrometers, a four-channel IR radiometer, and a solar UV spectrometer. Atmospheric measurements will be made of the mesospheric and stratospheric ozone density distribution, water vapor density distribution, temperature profile, ozone photolysis rate, and NO2 density distribution. In addition, the solar UV monitor will measure both the 0.2-0.31 micron spectral region and the Lyman-alpha (0.1216 micron) contribution to the solar irradiance.

Thomas, G. E.↗

NASA NTRS1974

Ion composition and drift observations in the nighttime equatorial ionosphere

The first in situ measurements of ion composition in the nighttime equatorial E- and F-region ionospheres are presented and discussed. These profiles were obtained by two rocket-borne ion mass spectrometers launched from Thumba, India, on March 9-10, 1970. Ionosonde data established that the composition was measured at times bounding a period of F-region downward drift. During this period, the ions O(+) and N(+) were enhanced by 1-3 orders of magnitude between 220 and 300 km. Below the drift region, O(+) ceased to be the major ionic constituent, but the concentrations of O(+) and N(+) remained larger than predicted from known radiation sources and loss processes. Here also, both the O2(+) and the NO(+) profiles retained nearly the same shape and magnitude throughout the night in agreement with theories assuming scattered UV radiation to be the maintaining source.

Goldberg, R. A.↗

NASA NTRS2009

Solar Wind Ablation of Terrestrial Planet Atmospheres

Internal plasma sources usually arise in planetary magnetospheres as a product of stellar ablation processes. With the ignition of a new star and the onset of its ultraviolet and stellar wind emissions, much of the volatiles in the stellar system undergo a phase transition from gas to plasma. Condensation and accretion into a disk is replaced by radiation and stellar wind ablation of volatile materials from the system- Planets or smaller bodies that harbor intrinsic magnetic fields develop an apparent shield against direct stellar wind impact, but UV radiation still ionizes their gas phases, and the resulting internal plasmas serve to conduct currents to and from the central body along reconnected magnetic field linkages. Photoionization and thermalization of electrons warms the ionospheric topside, enhancing Jeans' escape of super-thermal particles, with ambipolar diffusion and acceleration. Moreover, observations and simulations of auroral processes at Earth indicate that solar wind energy dissipation is concentrated by the geomagnetic field by a factor of 10-100, enhancing heavy species plasma and gas escape from gravity, and providing more current carrying capacity. Thus internal plasmas enable coupling with the plasma, neutral gas and by extension, the entire body. The stellar wind is locally loaded and slowed to develop the required power. The internal source plasma is accelerated and heated, inflating the magnetosphere as it seeks escape, and is ultimately blown away in the stellar wind. Bodies with little sensible atmosphere may still produce an exosphere of sputtered matter when exposed to direct solar wind impact. Bodies with a magnetosphere and internal sources of plasma interact more strongly with the stellar wind owing to the magnetic linkage between the two created by reconnection.

Moore, Thomas Earle↗

NASA NTRS2013

The Ultraviolet Radiation Environment around M Dwarf Exoplanet Host Stars

The spectral and temporal behavior of exoplanet host stars is a critical input to models of the chemistry and evolution of planetary atmospheres. Ultraviolet photons influence the atmospheric temperature profiles and production of potential biomarkers on Earth-like planets around these stars. At present, little observational or theoretical basis exists for understanding the ultraviolet spectra of M dwarfs, despite their critical importance to predicting and interpreting the spectra of potentially habitable planets as they are obtained in the coming decades. Using observations from the Hubble Space Telescope, we present a study of the UV radiation fields around nearby M dwarf planet hosts that covers both far-UV (FUV) and near-UV (NUV) wavelengths. The combined FUV+NUV spectra are publicly available in machine-readable format. We find that all six exoplanet host stars in our sample (GJ 581, GJ 876, GJ 436, GJ 832, GJ 667C, and GJ 1214) exhibit some level of chromospheric and transition region UV emission. No "UV-quiet" M dwarfs are observed. The bright stellar Lyman-alpha emission lines are reconstructed, and we find that the Lyman-alpha line fluxes comprise approximately 37%-75% of the total 1150-3100 A flux from most M dwarfs; approximately greater than 10(exp3) times the solar value. We develop an empirical scaling relation between Lyman-alpha and Mg II emission, to be used when interstellar H I attenuation precludes the direct observation of Lyman-alpha. The intrinsic unreddened flux ratio is F(Lyman-alpha)/F(Mg II) = 10(exp3). The F(FUV)/F(NUV) flux ratio, a driver for abiotic production of the suggested biomarkers O2 and O3, is shown to be approximately 0.5-3 for all M dwarfs in our sample, greather than 10(exp3) times the solar ratio. For the four stars with moderate signal-to-noise Cosmic Origins Spectrograph time-resolved spectra, we find UV emission line variability with amplitudes of 50%.500% on 10(exp2)-10(exp3) s timescales. This effect should be taken into account in future UV transiting planet studies, including searches for O3 on Earth-like planets. Finally, we observe relatively bright H2 fluorescent emission from four of the M dwarf exoplanetary systems (GJ 581, GJ 876, GJ 436, and GJ 832). Additional modeling work is needed to differentiate between a stellar photospheric or possible exoplanetary origin for the hot (T(H2) approximately equal to 2000-4000 K) molecular gas observed in these objects.

France, Kevin↗

NASA NTRS1972

Effect of simulated space radiation on selected optical materials.

The effect of simulated Nimbus spacecraft orbital (1100 km, circular, and polar) radiation on wide-band-pass glass filters, narrow-bandpass thin-film interference filters, and several fused silicas was determined by transmittance measurements over the 200-3400-nm wavelength region. No changes were observed in the filters, which were shielded with fused silica during irradiation, after exposure to a 1-yr equivalent orbital dose of electrons, nor were changes observed in the fused silicas after the same electron exposure plus a 1-yr equivalent dose of protons. Exposure to a 1/2-yr equivalent dose of solar uv radiation, however, caused a significant degradation in the transmittance of two uv-transmitting interference filters but had no effect on two colored glass filters that transmitted in the visible and near-ir regions. As a result of the uv exposure, the fused silicas exhibited losses of several percent over the 200-300-nm wavelength region.

Nicoletta, C. A.↗