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DOE OSTI2021

NO PLIF flow visualization and time-resolved temperature distributions in laser induced breakdown plumes

NO planar laser induced fluorescence (PLIF) is used to obtain images of laser-induced breakdown plasma plumes in NO-seeded nitrogen and dry air at near atmospheric pressure. Single-shot PLIF-images show that the plume development 5–50 μs after the breakdown pulse is fairly reproducible shot-to-shot, although the plume becomes increasingly stochastic on longer timescales, 100–500 μs. The stochastic behavior of the plume is quantified using probability distributions of the loci of the plume boundary. Analysis of the single-shot images indicates that the mixing of the plume with ambient gas on sub-ms time scale is insignificant. The induced flow velocity in the plume is fairly low, up to 30 m s –1 , suggesting that laser breakdowns are ineffective for mixing enhancement in high speed flows. The ensemble-averaged PLIF images indicate the evolution of the plume from an initially elongated shape to near-spherical to toroidal shape, with a subsequent radial expansion and formation of an axial jet in the center. Temperature distributions in the plume in air are obtained from the NO PLIF images, using two rotational transitions in the NO(X, v' = 0 → A, v'' = 0) band, J'' = 6.5 and 12.5 of the Q R 12 + Q 2 branch. The results indicate that the temperature in the plume remains high, above 1000 K, for approximately 100 μs, after which it decays gradually, to below 500 K at 500 μs. The residual NO fraction in the plume is ~0.1%, indicating that repetitive laser-assisted ignition may result in significant NO-generation. Furthermore, these measured temperature and velocity distributions can be used for detailed validation of kinetic models of laser-induced breakdown and assessment of their predictive capability.

42 ENGINEERING↗

DOE OSTI2025

Effects of non-equilibrium ionization and excitation on radiation absorption in plasma plumes induced by ablation of metal targets with nanosecond laser pulses

Ionization and radiation absorption in nanosecond laser-induced plasma plumes are routinely modeled using the Saha–Boltzmann equilibrium ionization model (EQM). However, the equilibrium assumption can be inaccurate during the laser pulse when non-equilibrium effects significantly impact radiation absorption. In the present work, the EQM and non-equilibrium collisional-radiative model (CRM) are compared to reveal the effect of plasma non-equilibrium on radiation absorption in non-homogeneous plumes and degree of plasma shielding. Simulations of plume expansion induced by irradiation of a copper target in 1 atm argon background gas with a 10 ns Gaussian pulse at a fluence from 8 Jcm −2 to 14 Jcm −2 are performed with a hybrid computational model that couples a lumped particle direct simulation Monte Carlo method with either CRM or EQM. The simulations show that the EQM strongly underestimates the effects of ionization and radiation absorption compared to CRM and, contrary to the CRM, predict strong ionization of the background gas. The differences between the models are explained by the qualitatively different coupling between plume expansion and dynamics of ionization and exitation processes in the CRM and EQM under conditions when the characteristic times for most radiation- and electron-induced processes are longer than the pulse duration. The CRM-based predictions are also found to agree much better with available experimental data. In conclusion, these results indicate that the model of Saha–Boltzmann equilibrium cannot be used for reliable prediction of the degree of plasma shielding in plumes induced by nanosecond laser pulses or for processing results of spectroscopic measurements at early stages of expansion of such plumes.

Physics - Plasma physics↗

DOE OSTI2022

Measurement of muon-induced neutron yield at the China Jinping Underground Laboratory *

Abstract Solar, terrestrial, and supernova neutrino experiments are subject to muon-induced radioactive background. The China Jinping Underground Laboratory (CJPL), with its unique advantage of a 2400 m rock coverage and long distance from nuclear power plants, is ideal for MeV-scale neutrino experiments. Using a 1-ton prototype detector of the Jinping Neutrino Experiment (JNE), we detected 343 high-energy cosmic-ray muons and (7.86 3.97) muon-induced neutrons from an 820.28-day dataset at the first phase of CJPL (CJPL-I). Based on the muon-induced neutrons, we measured the corresponding muon-induced neutron yield in a liquid scintillator to be μ −1 g −1 cm 2 at an average muon energy of 340 GeV. We provided the first study for such neutron background at CJPL. A global fit including this measurement shows a power-law coefficient of (0.75 0.02) for the dependence of the neutron yield at the liquid scintillator on muon energy.

Zhao, Lin↗

DOE OSTI2021

Advanced assessment of beam-induced background at a muon collider

Renewed international interest in muon colliders motivates the continued investigation of the impacts of beam-induced background on detector performance. This continues the effort initiated by the Muon Accelerator Program and carried out until 2017. The beam-induced background from muon decays directly impacts detector performance and must be mitigated by optimizing the overall machine design, with particular attention paid to the machine detector interface region. In order to produce beam-induced background events and to study their characteristics in coordination with the collider optimization, a flexible simulation approach is needed. To achieve this goal we have chosen to utilize the combination of LineBuilder and Monte Carlo FLUKA codes. We report the results of beam-induced background studies with these tools obtained for a 1.5 TeV center of mass energy collider configuration. Good agreement with previous simulations using the MARS15 code demonstrates that our choice of tools meet the accuracy and performance requirements to perform future optimization studies on muon collider designs.

43 PARTICLE ACCELERATORS↗

DOE OSTI2023

Linking repeat lidar with Landsat products for large scale quantification of fire-induced permafrost thaw settlement in interior Alaska

The permafrost–fire–climate system has been a hotspot in research for decades under a warming climate scenario. Surface vegetation plays a dominant role in protecting permafrost from summer warmth, thus, any alteration of vegetation structure, particularly following severe wildfires, can cause dramatic top–down thaw. A challenge in understanding this is to quantify fire-induced thaw settlement at large scales (>1000 km 2 ). In this study, we explored the potential of using Landsat products for a large-scale estimation of fire-induced thaw settlement across a well-studied area representative of ice-rich lowland permafrost in interior Alaska. Six large fires have affected ~1250 km 2 of the area since 2000. We first identified the linkage of fires, burn severity, and land cover response, and then developed an object-based machine learning ensemble approach to estimate fire-induced thaw settlement by relating airborne repeat lidar data to Landsat products. The model delineated thaw settlement patterns across the six fire scars and explained ~65% of the variance in lidar-detected elevation change. Our results indicate a combined application of airborne repeat lidar and Landsat products is a valuable tool for large scale quantification of fire-induced thaw settlement.

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2021

Genome-wide association of the metabolic shifts underpinning dark-induced senescence in Arabidopsis

Dark-induced senescence provokes profound metabolic shifts to recycle nutrients and to guarantee plant survival. To date, research on these processes has largely focused on characterizing mutants deficient in individual pathways. Here, we adopted a time-resolved genome-wide association-based approach to characterize dark-induced senescence by evaluating the photochemical efficiency and content of primary and lipid metabolites at the beginning, or after 3 or 6 days in darkness. We discovered six patterns of metabolic shifts and identified 215 associations with 81 candidate genes being involved in this process. Among these associations, we validated the roles of four genes associated with glycine, galactinol, threonine, and ornithine levels. We also demonstrated the function of threonine and galactinol catabolism during dark-induced senescence. Intriguingly, we determined that the association between tyrosine contents and TYROSINE AMINOTRANSFERASE 1 influences enzyme activity of the encoded protein and transcriptional activity of the gene under normal and dark conditions, respectively. Moreover, the single-nucleotide polymorphisms affecting the expression of THREONINE ALDOLASE 1 and the amino acid transporter gene AVT 1 B, respectively, only underlie the variation in threonine and glycine levels in the dark. Taken together, these results allow us to present a very detailed model of the metabolic aspects of dark-induced senescence, as well as the process itself.

59 BASIC BIOLOGICAL SCIENCES↗

DOE OSTI2025

Thermodynamic origin of the pressure-induced Invar effect: General criterion and experimental study of Fe 68 ⁢Pd 32

Synchrotron X-ray diffraction measurements were performed on 57 Fe 68 Pd 32 at multiple pressures and two temperatures in a diamond-anvil cell. Between 4 and 11GPa, the thermal expansion was zero or slightly negative. This pressure-induced Invar effect was studied further with 57 Fe nuclear forward scattering and nuclear resonant inelastic X-ray scattering to obtain information on the pressure-induced changes in both the magnetization and the phonon density of states. Magnetic entropy and phonon entropy were obtained from these results, the latter with additional measurements from inelastic neutron scattering to account for the contributions from Pd atoms. The dependencies of these entropies on pressure gave the magnetic and phonon contributions to thermal expansion. These canceled in the region of pressure-induced Invar behavior, even though they individually increased by more than a factor of 2 below the Curie pressure. The behavior of phonons gives evidence for spin-phonon interactions in Fe 68 Pd 32 . A general explanation of the pressure-induced Invar effect is presented, showing that Invar behavior is typically expected at a pressure P* below a magnetic transition at pressure PC. The difference in pressure P C − P* scales with the fractional reduction in magnetic exchange interaction divided by the average Gr¨uneisen parameter.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

DOE OSTI2024

Impact of beam coupling impedance on crab cavity noise induced emittance growth

Crab cavities will be deployed as a part of the High Luminosity Large Hadron Collider (HL-LHC) upgrade to mitigate the luminosity reduction induced by the crossing angle at the main experiments (ATLAS and CMS). Two prototype crab cavities have been installed in the CERN Super Proton Synchrotron (SPS) in 2018 for studies with proton beams. An issue of concern is the transverse emittance growth induced by noise in the crab cavity radio frequency (rf) system, which is anticipated to limit the performance of the HL-LHC. In measurements conducted in the SPS in 2018, the crab cavity noise-induced emittance growth was measured to be a factor of 4 lower than predicted from the existing analytical models. In this paper, it is shown that the observed discrepancy is explained by damping effects from the beam coupling impedance, which were not included in the models up to now. Using the van Kampen mode approach, a new theory is developed, suggesting that the impedance can separate the coherent tune from the incoherent spectrum leading to an effective reduction of the crab cavity rf noise-induced emittance growth. This mechanism is validated in tracking simulations using the SPS impedance model as well as in dedicated experimental measurements conducted in the SPS in 2022. The implications for the HL-LHC project are discussed. Published by the American Physical Society 2024

Physics↗

DOE OSTI2020

Discriminating Uranium Isotopes Based on Fission Signatures Induced by Delayed Neutrons

The use of active interrogation to induce delayed neutron emission is a well-established technique for the characterization of special nuclear materials. Delayed neutrons have isotope-characteristic spectral and temporal signatures, which provide the basis for isotope identification. However, in bulk materials that contain an appreciable fissile (e.g., 235 U or 233 U) fraction, such as highly enriched uranium (HEU), delayed neutrons have a high probability of inducing additional fissions. As a result, the overall delayed neutron signature consists of two distinct components: the “primary” delayed neutrons (emitted directly by fission fragments) and the “secondary prompt” fission neutrons produced in fission induced by primary delayed neutrons. These prompt products differ from “primary” delayed neutrons both in their energy spectra and in the presence of coincident radiation released by the parent fission event. The presence and relative quantity of prompt products from delayed fission depend on the cross section of the material in the energy range of delayed neutrons, which may differ significantly between isotopes, thus providing an exploitable means for isotope differentiation. Here, we demonstrate two experimental approaches for discriminating between 235 U and 238 U isotopes based on the measurement of delayed neutron-induced fission products. First, HEU and depleted uranium objects are differentiated through the detection of high-energy prompt neutrons from delayed fission using both recoil-based organic liquid scintillators and thermalization spectra from a custom-built capture-gated composite detector. Secondly, coincident radiation measurements are used as the basis for discrimination by comparing the overall rates and time evolution of fission events when delayed neutrons are present.

07 ISOTOPE AND RADIATION SOURCES↗

DOE OSTI2021

Evolution of magnetic field induced ordering in the layered quantum Heisenberg triangular-lattice antiferromagnet Ba 3 CoSb 2 O 9

Quantum fluctuations in the effective spin-12 layered triangular-lattice quantum Heisenberg antiferromagnet Ba 3 CoSb 2 O 9 lift the classical degeneracy of the antiferromagnetic ground state in magnetic field, producing a series of novel spin structures for magnetic fields applied within the crystallographic ab plane, including a celebrated collinear “up-up-down” spin ordering with magnetization equal to 1/3 of the saturation magnetization over an extended field range. Theoretically unresolved, however, are the effects of interlayer antiferromagnetic coupling and transverse magnetic fields on the ground states of this system. Additional magnetic field induced phase transitions are theoretically expected and in some cases have been experimentally observed, but details regarding their number, location, and physical character appear inconsistent with the predictions of existing models. Conversely, an absence of experimental measurements as a function of magnetic-field orientation has left other key predictions of these models untested. To address these issues, in this study we have used specific heat, neutron diffraction, thermal conductivity, and magnetic torque measurements to map out the phase diagram as a function of magnetic field intensity and orientation relative to the crystallographic ab plane. For H||ab, we have discovered an additional magnetic field induced phase transition at low temperature and an unexpected tetracritical point in the high-field phase diagram, which coupled with the apparent second-order nature of the phase transitions eliminates several theoretically proposed spin structures for the high-field phases. Our calorimetric measurements as a function of magnetic field orientation are in general agreement with theory for field-orientation angles close to plane parallel (H||a) but diverge at angles near plane perpendicular; a predicted convergence of two phase boundaries at finite angle and a corresponding change in the order of the field induced phase transition are not observed experimentally. Our results emphasize the role of interlayer coupling in selecting and stabilizing field induced phases, provide guidance on the nature of the magnetic order in each phase, and reveal the need for new physics to account for the nature of magnetic ordering in this archetypal two-dimensional spin-12 triangular-lattice quantum Heisenberg antiferromagnet.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

DOE OSTI2024

Medium-induced photon bremsstrahlung in neutrino-nucleus, antineutrino-nucleus, and electron-nucleus scattering from multiple QED interactions

Interactions of charged leptons with nuclei and the naive tree-level kinematics of these processes are affected by radiation of photons induced by the QED nuclear medium. We evaluate cross section modifications at leading orders of the number of correlated interactions inside the nucleus, known as the opacity expansion. We derive results for soft and collinear types of the bremsstrahlung at the first three orders in opacity and generalize them to higher orders. We present the leading in opacity energy spectra of soft and collinear photons and radiative energy loss inside the nucleus for experiments with lepton kinematics in the GeV energy range. At leading power of the Glauber soft-collinear effective field theory, the soft radiation is further resummed to all orders both in opacity and in the electromagnetic coupling constant. We find that the soft and collinear medium-induced radiation is vacuumlike, and additional corrections are power suppressed. Despite the negligible modification to the induced photon spectra, the nuclear medium-induced radiation sizably affects the broadening of charged leptons in the direction orthogonal to their propagation. Published by the American Physical Society 2024

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

DOE OSTI2025

Quasiclassical evaluation of gluon saturation induced helicity effects

At sub-eikonal order in the high-energy limit, helicity dependences are generally contained in the transverse components of the gluon field. In the gluon saturation regime, novel helicity effects arise from the nonlinear interaction between the eikonal-order longitudinal gluon field and the sub-eikonal-order transverse gluon field. We derive this saturation induced helicity-dependent field both by solving the classical Yang-Mills equations and through direct diagrammatic calculations. Our analysis shows that the saturation induced helicity effect is intrinsically a two-particle (or multiparticle) correlation effect, rather than a single-particle distribution effect. Furthermore, we evaluate this effect in the context of double-spin asymmetry for incoherent diffractive dijet production in longitudinally polarized electron-nucleus collisions, using a simplified helicity-extended McLerran-Venugopalan model. We find that the saturation induced helicity effect further suppresses the back-to-back peak in the dijet azimuthal angle correlation, with a magnitude comparable to that of the direct helicity effect. This gluon saturation induced helicity effect may offer a novel avenue to probe gluon saturation in polarized collisions. Published by the American Physical Society 2025

Li, Ming (ORCID:0000000195509691)↗

DOE OSTI2020

Vortex rings drive entrainment and cooling in flow induced by a spark discharge

Spark plasma discharges induce vortex rings and a hot gas kernel. We develop a model to describe the late stage of the spark-induced flow and the role of the vortex rings in the entrainment of cold ambient gas and the cooling of the hot gas kernel. The model is tested in a plasma-induced flow using density and velocity measurements obtained from simultaneous stereoscopic particle image velocimetry and background oriented schlieren. We show that the spatial distribution of the hot kernel follows the motion of the vortex rings, whose radial expansion increases with the electrical energy deposited during the spark discharge. Here, the vortex ring cooling model establishes that entrainment in the convective cooling regime is induced by the vortex rings and governs the cooling of the hot gas kernel, and the rate of cooling increases with the electrical energy deposited during the spark discharge.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

DOE OSTI2020

Exotic silicon phases synthesized through ultrashort laser-induced microexplosion: Characterization with Raman microspectroscopy

Exotic metastable phases of silicon formed under high pressure are expected to have attractive semiconducting properties including narrow band gaps that open up novel technological applications. Confined microexplosions induced by powerful ultrashort laser pulses have been demonstrated as an advanced tool for the creation of new high-pressure phases that cannot be synthesized by other means. Tightly focused laser pulses are used to generate localized modifications inside the material structure, providing the possibility for precise controlled band-gap engineering. In this study, noninvasive Raman spectroscopy was used for analysis of laser-modified zones in silicon and to determine the metastable high-pressure phases contained. Low laser energies induced the formation of amorphous-only silicon, while higher energies led to crystalline silicon polymorphs within the modifications, albeit under considerable residual stress up to 4.5 GPa. The presence of the structurally similar r8-Si, bc8-Si, and bt8-Si phases is revealed, as well as other yet to be identified phases, and the stacking-related 9R Si polytype is evidenced, presumably stress-induced by the highly compressed laser-modified zone. The ab initio random structure searching approach is used to calculate the Raman signatures and to help identify different Si polymorphs. The findings of this study by Raman spectroscopy from ultrashort laser-induced microexplosion sites may yield insights into the local structure and properties of new silicon metastable phases and the prospect of utilizing exotic phases for extending current applications.

36 MATERIALS SCIENCE↗

DOE OSTI2024

Light-Induced Melting of Competing Stripe Orders without Introducing Superconductivity in La 2 − x Ba x CuO 4

The ultrafast manipulation of quantum material has led to many novel and significant discoveries. Among them, the light-induced transient superconductivity in cuprates achieved by melting competing stripe orders represents a highly appealing accomplishment. However, recent investigations have shown that the notion of photoinduced superconductivity remains a topic of controversy, and its elucidation solely through c -axis time-resolved terahertz spectroscopy remains an arduous task. Here, we measure the in-plane and out-of-plane transient terahertz responses simultaneously in the stripe-ordered nonsuperconducting La 2 − x Ba x CuO 4 after near-infrared excitations. We find that although a pump-induced reflectivity edge appears in the c -axis reflectance spectrum, the reflectivity along the CuO 2 planes decreases simultaneously, indicating an enhancement in the scattering rate of quasiparticles. This in-plane transient response is clearly distinct from the features associated with superconducting condensation. Therefore, we conclude the out-of-plane transient responses cannot be explained by an equivalent of Josephson tunneling. Notably, those pump-induced terahertz responses remain consistent even when we vary the near-infrared optical pump wavelengths and hole concentrations. Our results provide critical evidence that transient three-dimensional superconductivity cannot be induced by melting the competing stripe orders with pump pulses whose photon energy is much higher than the superconducting gap of cuprates. Published by the American Physical Society 2024

36 MATERIALS SCIENCE↗

DOE OSTI2025

Allopregnanolone as an Adjunct Therapy to Midazolam is More Effective Than Midazolam Alone in Suppressing Soman‐Induced Status Epilepticus in Male Rats

ABSTRACT Aims Humans and animals acutely intoxicated with the organophosphate soman can develop sustained status epilepticus (SE) that rapidly becomes refractory to benzodiazepines. We compared the antiseizure efficacy of midazolam, a current standard of care treatment for OP‐induced SE, versus combined therapy with midazolam and allopregnanolone (ALLO) in a rat model of soman‐induced SE. Methods Soman‐intoxicated male rats with robust seizure behavior and high‐amplitude electroencephalographic (EEG) activity were administered midazolam (0.65 mg, i.m.) 20 min after seizure initiation and 10 min later either a second dose of midazolam or ALLO (12 or 24 mg/kg, i.m.). Seizure behavior and EEG were monitored for 4 h after treatment. Brains were collected at the end of the monitoring period for histological analyses. Results Animals receiving 2 doses of midazolam exhibited persistent SE. Sequential dosing with midazolam followed by ALLO suppressed electrographic seizure activity. The combination therapy also significantly reduced soman‐induced neurodegeneration and neuroinflammation compared to 2 doses of midazolam. High but not low dose ALLO was associated with transitory and reversible respiratory compromise during the 1 h period after dosing. Conclusions Treatment with midazolam followed by ALLO was more effective than 2 doses of midazolam in suppressing benzodiazepine‐refractory, soman‐induced SE, and in mitigating its acute neuropathological consequences.

Andrew, Peter M. [Department of Molecular Bioscien↗

DOE OSTI2026

Flash electropolishing for TEM: Reducing FIB‐induced defects in tungsten with protocols for new materials

Focused ion beam (FIB) milling has become the dominant approach for site-specific transmission electron microscopy (TEM) specimen preparation; however, FIB damage remains a critical limitation for reliable microstructural characterisation, particularly in radiation effects studies. Tungsten is especially susceptible to FIB damage due to its high nuclear stopping power, which promotes the formation and strong diffraction contrast of FIB-induced ‘black spot’ defects that are indistinguishable from very fine irradiation-induced loops/defects resulting from low to intermediate temperature neutron irradiation. In this work, flash electropolishing is systematically evaluated as a post-FIB treatment for minimising preparation-induced artefacts for TEM analysis of tungsten-based alloys. Using a range of non-, ion-, and neutron-irradiated tungsten materials, the effectiveness of flash electropolishing has been assessed through direct comparison with conventional FIB and plasma-FIB preparation including low-energy Ga, Ar, Xe ion cleaning. The results demonstrate that flash electropolishing effectively removes FIB-damaged layers and ‘black spot’ defects, thereby enabling reliable observation of irradiation-induced dislocation structures. Key processing parameters governing flash electropolishing quality – including lamella thickness, applied voltage, polishing duration, electrolyte chemistry, and cathode geometry – have been systematically evaluated, and clear criteria were established for determining when flash electropolishing is required to ensure reliable microstructural analysis. This work also provides practical guidance for implementing flash electropolishing as an artefact-controlled specimen-preparation approach for TEM characterisation of FIB-produced specimens. The systematic protocol can be extended to other, non-tungsten materials.

TEM sample preparation↗

DOE OSTI2022

The influence of increasing atmospheric CO 2 , temperature, and vapor pressure deficit on seawater-induced tree mortality

We report increasing seawater exposure is killing coastal trees globally, with expectations of accelerating mortality with rising sea levels. However, the impact of concomitant changes in atmospheric CO 2 concentration, temperature, and vapor pressure deficit (VPD) on seawater-induced tree mortality is uncertain. We examined the mechanisms of seawater-induced mortality under varying climate scenarios using a photosynthetic gain and hydraulic cost optimization model validated against observations in a mature stand of Sitka-spruce (Picea sitchensis) trees in the Pacific Northwest, USA, that were dying from recent seawater exposure. The simulations matched well with observations of photosynthesis, transpiration, nonstructural carbohydrates concentrations, leaf water potential, the percentage loss of xylem conductivity, and stand-level mortality rates. The simulations suggest that seawater-induced mortality could decrease by ~16.7% with increasing atmospheric CO 2 levels due to reduced risk of carbon starvation. Conversely, rising VPD could increase mortality by ~5.6% because of increasing risk of hydraulic failure. Across all scenarios, seawater-induced mortality was driven by hydraulic failure in the first two years after seawater exposure began, with carbon starvation becoming more important in subsequent years. Changing CO 2 and climate appear unlikely to have a significant impact on coastal tree mortality under rising sea levels.

54 ENVIRONMENTAL SCIENCES↗