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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 253 records · Page 14

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NASA NTRS1973

The effect of thermal cycling on the structure and properties of a Co, Cr, Ni-TaC directionally solidified eutectic composite

A Co, Cr, Ni-TaC directionally solidified eutectic composite was subjected to thermal fatigue between 427-1093°C. The material suffered degradation in microstructure and elevated temperature mechanical properties. The loss in properties varied with the maximum cycling temperature and number of cycles. This behavior is attributed to the increasing solubility of the TaC in the matrix with temperature from 0.4% at room temperature to 2.2% at 1200°C. During the thermal cycling, the TaC is subjected to solution and reprecipitation which form serrations on the fibers since the easy growth planes of the TaC are not coincident with the fiber faces exposed to the matrix.

Composites↗

NASA NTRS1978

The effect of microstructure on hydrogen embrittlement of the nickel-base superalloy, Udimet 700

Material from a single heat of cast and wrought Udimet 700 was processed and/or heat treated to produce five material conditions with identical chemical compositions but with distinct microstructural variations, and then evaluated for susceptibility to hydrogen embrittlement. Two prealloyed powder conditions exhibited significantly improved resistance to hydrogen embrittlement, as compared to wrought material. No degradation in notch or smooth tensile strengths occurred, and average ductilities of 25 percent reduction of area were determined for 2 hydrogen evaluation procedures. For the most severe hydrogenation procedure, ductility levels were reduced to 15 percent. These improvements were attributed to cleaner grain boundaries and decreases grain size.

Gray, H. R.↗

NASA NTRS1978

The effect of microstructure on hydrogen embrittlement of the nickel base superalloy, Udimet 700

Gray, H. R.↗

NASA NTRS1980

Damage tolerance research on composite compression panels

The damage tolerance of composites was investigated. Results show that severe degradation in material strength may occur due to impact damage and that reduced strain allowables should be considered to compensate for possible impact damage. The mechanisms of failure involved in impact so that local damage will be reduced and arrest of propagating fracture initiated at impact locations are examined. Compression strength reductions for damage due to impact by a 1.27 cm diameter spherical projectile in thick laminates representative of wing skin panels are presented. Also discussed are the results of concepts recently evaluated to improve damage tolerance. These concepts range from improvements at the materials level to advanced structural configurations designed to arrest or limit the growth of propagating fractures. The results indicate that substantial improvements in the damage tolerance of graphite-epoxy composite structures can be achieved through the proper combination of materials and structural design.

Rhodes, M. D.↗

NASA NTRS1986

High-Flux Atomic-Oxygen Source

Beams of pure ground-state oxygen atoms produced. Accelerated electrons strike beam of O2 gas in dissociative-attachment region, producing O- ions. O- ions accelerated to desired final energy and pass through photodetachment region to form 0(3P) atoms. These pass between electric field plates to remove O- and e and strike target. Designed specifically to study degradation of materials and spacecraft glow phenomena in low Earth orbits, used to study gas-phase collision phenomena involving energetic oxygen atoms.

Chutjian, A.↗

NASA NTRS1986

Protecting spacecraft from atomic oxygen

Findings are reported from Space Shuttle flights STS-3, 4, 5, and 8 regarding the degradation of materials exposed to atomic oxygen in low earth orbit. Atomic oxygen, a strong oxidizing agent, is present in low concentrations at such altitudes, and a spacecraft can sweep up considerable volumes of it at orbital velocities of 5 miles/s, especially if mission lifetimes are measured in years or decades. Material loss has been found to be a function of the fluence (the number of oxygen atoms striking a unit area of surface over a given period); fluence is proportional to atmospheric density, orbital velocity, surface attitude relative to velocity vector, and duration of exposure. Atmospheric density depends first on altitude and second on the phase of the 11-year solar activity cycle. Metals, in the experiments, reacted less than nonmetals. Graphs and a table are included, permitting calculation of how far a surface of various organic materials will recede on a spacecraft in low earth orbit. The limited data base on atomic oxygen interactions with materials, using both Shuttle flight experiments and ground-based facilities must be augmented. Space Station design is imminent, and the understanding of such interactions is critical to the success of that design.

Leger, L. J.↗

NASA NTRS1988

Pulsed Source Of Energetic Oxygen Atoms

Apparatus developed that generates high-flux pulses of oxygen atoms to bombard specimens in experiments on aging and degradation of materials in low Earth-orbit environment. Preliminary studies of specimens irradiated with atomic oxygen provided spectral evidence of erosion, in addition to measurable mass loss. Intense atomic oxygen pulses also useful in studies of microfabrication techniques.

Caledonia, George↗

NASA NTRS1988

Probabilistic constitutive relationships for cyclic material strength models

A methodology is developed that provides a probabilistic treatment for the lifetime of structural components of aerospace propulsion systems subjected to fatigue. Material strength degradation models, based on primitive variables, include both a fatigue strength reduction model and a fatigue crack growth model. Probabilistic analysis is based on simulation, and both maximum entropy and maximum penalized likelihood methods are used for the generation of probability density functions. The resulting constitutive relationships are included in several computer programs.

Boyce, L.↗

NASA NTRS1989

Ceramic Wick For Capillary-Pumped Heat Pipe

Fibrous ceramic wick allows choice of working fluid and high-temperature fabrication and/or operation. Wick material resists degradation at temperatures from -195 to +1,500 degrees C. Liquid refrigerant fills bore of silica/alumina wick. After flowing by capillary action through pores of wick, refrigerant evaporates from finned outer surface of wick and enters heat pipe, flowing toward condenser section.

Seidenberg, Benjamin↗

NASA NTRS1988

Plasma interactions monitoring system

The plasma environment around the space station is expected to be different from that environment which occurs naturally at these altitudes because of the unprecedented size of the space station, its orbital motion, and its high power distribution system. Although there are models which predict the environment around the station, they do not take into account changes in configuration, changes in the natural and induced environments, nor interactions between the different environments. There will be unique perturbations associated with the space station, which will vary as the space station is being developed. Even after the developed space station has been completed environmental conditions will change as the payloads are changed and as the station systems and materials undergo degradation and modification. Because the space station will be a point of many varied activities the environment will continually undergo perturbations from effluents resulting from operations of the reboost module, EVA, airlock operations, and vacuum venting. The use of the Mobile Service Center will cause disturbances which cannot, at this time, be predicted. Also, the natural environment will be affected by solar flares. In addition, the operations of attached payloads, (e.g., ASTROMAG) themselves will undoubtedly cause perturbations to the ambient environment. Finally, the natural environment will change as a result of natural perturbations such as solar flares and geomagnetic storms.

Roberts, William T.↗

NASA NTRS1988

Growth of mercuric iodide (HgI2) for nuclear radiation detectors

Mercuric iodide is a material used for the fabrication of the sensing element in solid state X-ray and gamma ray detecting instruments. The operation of the devices is determined to a large degree by the density of structural defects in the single crystalline material used in the sensing element. Since there were strong indications that the quality of the material was degraded by the effects of gravity during the growth process, a research and engineering program was initiated to grow one or more crystals of mercuric iodide in the reduced gravity environment of space. A special furnace assembly was designed which could be accommodated in a Spacelab rack, and at the same time made it possible to use the same growth procedures and controls used when growing a crystal on the ground. The space crystal, after the flight, was subjected to the same evaluation methods used for earth-grown crystals, so that comparisons could be made.

Vandenberg, L.↗

NASA NTRS1991

Meteoroid/space debris impacts on MSFC LDEF experiments

A number of unusual effects are presented that were observed on the TCSE test samples, front cover, and structural components. These include induced UV fluorescence in some materials, the migration and degradation of KRS-5 materials, atomic oxygen (AO), and contaminant texturing and discoloration, and meteoroid and debris impacts. These effects and their causes are discussed.

Zwiener, James M.↗

NASA NTRS1991

Spacecraft thermal control coatings (AO 138-6)

The experiment A0 138-6 was located on the trailing edge of LDEF as part of the Experiment FRECOPA. Material specimens 2 x 2 cm, independently mounted in sample-holders with their surface in the same reference plane, were exposed to space. Materials include paints (conductive or not), SSMs, polymeric films, surface coatings, composite materials, and metals. The results show that for some materials the degradation was higher for samples in the canister than for those directly mounted on the tray; contamination problems were ruled out, the higher temperature experienced by the samples inside the canister probably explains this phenomenon.

Paillous, Alain↗

NASA NTRS1991

Exposure to space radiation of high-performance infrared multilayer filters

The University of Reading experiment exposed IR interference filters and crystal substrates on identical earth facing and leading-edge sites of the Long Duration Exposure Facility (LDEF). Filters mostly comprised multilayer coatings of lead telluride (PbTe)/II-IV on germanium (Ge) and other substrates: crystals comprised CdTe, MgF2, sapphire, quartz, silicon, and some softer materials. Identical control samples were maintained in the laboratory throughout the experiment. The filters were novel in their design, construction and manufacture, and categorized high-performance because of their ability to resolve emission spectra of the important atmospheric gases for various purposes in remote sensing. No significant changes were found in the spectra of the hard-coated filters or in the harder crystals (the softer materials were degraded to an extent). By virtue of this well-documented and long exposure in LDEF, the qualification of the filter type is significantly improved for its future requirements.

Seeley, J. S.↗

NASA NTRS1991

Properties of three graphite/toughened resin composites

Results are presented from an experimental evaluation of IM7/977-2, IM7/F655, and T800/F3900. Data presented include ply-level (unidirectional laminate) strength and moduli, unnotched and notched (open hole) tension and compression properties of quasi-isotropic laminates, and compression-after-impact strengths. These data are compared with properties of other toughened (IM7/8551-7 and IM6/18081) and brittle (T300/5208) graphite-epoxy materials. The IM7/977-2, IM7/F655, and T800/F3900 materials are substantially stronger and more damage tolerant than widely used first generation composite materials such as T300/5208. The T800/F3900 outperforms IM7/977-2 and IM7/F655 materials in tolerance to projectile impacts. Compression-after-impact strengths were found to be dependent on impactor velocity for a given impact energy. The open hole compression properties of all three materials are degraded by the combination of heat and moisture.

Smith, Donald L.↗

NASA NTRS1992

Solar exposure of LDEF experiment trays

Exposure to solar radiation is one of the primary causes of degradation of materials on spacecraft. Accurate knowledge of solar exposure is needed to evaluate the performance of materials carried on the Long Duration Exposure Facility (LDEF) during its nearly 6 year orbital flight. Presented here are tables and figures of calculated solar exposure for the experiment rows, longerons, and end bays of the spacecraft as functions of time in orbit. The data covers both direct solar and earth reflected radiation. Results are expressed in cumulative equivalent sun hours (CESH) or the hours of direct, zero incidence solar radiation that would cause the same irradiance of a surface. Space end bays received the most solar radiation, 14,000 CESH; earth end bays received the least, 4,500 CESH. Row locations received between 6,400 CESH and 11,200 CESH with rows facing either eastward or westward receiving the most radiation and rows facing northward or southward receiving the least.

Bourassa, R. J.↗

NASA NTRS1992

Interaction of atomic oxygen with thin film and bulk copper: An XPS, AES, XRD, and profilometer study

The University of Alabama in Huntsville (UAH) experiment A-0114 was designed primarily to study degradation of material surfaces due to low earth orbital (LEO) atmospheric oxygen. The experiment contained 128 one inch circular samples: metals, polymers, carbons, and semiconductors. Among metal samples, copper has shown some interesting new results. Two types of copper samples, a film sputter coated on fused silica and a bulk piece of OFHC copper, were characterized employing a variety of techniques such as X-ray and Auger electron spectroscopies, X-ray diffraction, and high resolution profilometry. Cu 2p core level spectra were used to characterize the presence of Cu2O and CuO in addition to Cu Auger LMM lines. These results are supported by our recent X-ray diffraction studies which clearly establish the presence of Cu oxides which we were unable to prove in our earlier work. Profilometry showed an increase in thickness of the film sample where exposed to 106.7 +/- 0.5 nm from an initial thickness of 74.2 +/- 1.1 nm. Further studies with SEM and ellipsometry are underway.

Raikar, Genesh N.↗

NASA NTRS1992

Development of static system procedures to study aquatic biofilms and their responses to disinfection and invading species

The microbial ecology facility in the Analytical and Physical Chemistry Branch at Marshall Space Flight Center is tasked with anticipation of potential microbial problems (and opportunities to exploit microorganisms) which may occur in partially closed systems such as space station/vehicles habitats and in water reclamation systems therein, with particular emphasis on the degradation of materials. Within this context, procedures for microbial biofilm research are being developed. Reported here is the development of static system procedures to study aquatic biofilms and their responses to disinfection and invading species. Preliminary investigations have been completed. As procedures are refined, it will be possible to focus more closely on the elucidation of biofilm phenomena.

Smithers, G. A.↗