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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 253 records · Page 14
All sourcesNASA NTRSDOE OSTI
DOE OSTI2025

In-situ neutron radiography of pore-water movement in portland cement mortar under subzero temperature exposure: Insights from D 2 O-H 2 O systems

Neutron radiography was employed in this study to monitor real-time pore water movement in portland cement mortar exposed to subzero temperatures, providing novel insights into freeze-thaw (F-T) damage mechanisms. Deuterated water (D 2 O) was used to hydrate the cement in the mortar specimens, and the pore structure was saturated with water (H 2 O), allowing for a contrast that enabled detailed tracking of water movement predominantly in the pore structure. Furthermore, the mortar sample was placed on a chiller plate set to subzero temperatures, thereby providing a one-dimensional temperature gradient vertically in the sample. Neutron radiography revealed that unfrozen water migrated upward as the freezing front advanced, which can create hydraulic pressure within the mortar microstructure and may contribute to the initiation and propagation of microcracks during F-T cycles. Additional characterization of the concrete made with D 2 O showed a marked contrast to the samples made with H 2 O, including delayed hydration, diminished compressive strength, and greater porosity. Therefore, while mortar made with D 2 O allowed for greater neutron contrast to the pores filled with H 2 O, further study is required to produce mortars with similar properties to those made with H 2 O. In addition, further refinement is needed to the radiography experiment to allow for greater control of temperatures and potential quantification of the water concentration.

Air-void system↗
DOE OSTI2025

Molecular H 2 as the Reducing Agent in Low-Temperature Oxide Reduction Using Calcium Hydride

Low-temperature synthesis is crucial for advancing sustainable manufacturing and accessing novel metastable phases. Metal hydrides have shown great potential in facilitating the reduction of oxides at low temperatures, yet the underlying mechanism—whether driven by H - , H 2 , or atomic H—remains unclear. Here, in this study, we employ in situ electrical transport measurements and first- principles calculations to investigate the CaH 2 -driven reduction kinetics in epitaxial α-Fe 2 O 3 thin films. Intriguingly, samples in direct contact with or separated from CaH 2 powders exhibit similar apparent activation energies for H 2 reduction, although direct contact significantly increases the reduction rate. These findings indicate that molecular H 2 is the dominant reducing species in the low-temperature reduction of oxides using CaH 2 , with a key aspect of the hydrides' superior reducing power attributed to their ability to eliminate residual moisture. This work underscores the critical role of moisture control in enabling effective low-temperature oxide reduction for advanced material synthesis.

Wang, Jiayue [SLAC National Accelerator Laboratory↗
DOE OSTI2024

The Reservoir Temperature Estimator (RTEst): A multicomponent geothermometry tool

The Reservoir Temperature Estimator (RTEst) is a multicomponent geothermometry tool for estimating reservoir geochemical parameters including reservoir temperature, CO 2 fugacity, mass of water lost or gained, and a reaction factor. It estimates these parameters and their associated uncertainties by minimizing an objective function that is the weighted sum of squares of the saturation indices of a user-selected set of minerals believed to be equilibrated with the reservoir fluid. RTEst accomplishes these estimates by combining the geochemical modeling capabilities of The Geochemist’s Workbench® with the optimization/parameter estimation resources of PEST®. An included interface aids the user in selecting plausible mineral phases to comprise the objective function and calculates their weighting factors. The working principles of RTEst are described and its efficacy is illustrated by presenting results of its application to various geothermal fields with known conditions. These examples show RTEst can account for the alteration of ascending reservoir fluid by mineral (calcite) re-equilibration with changes in temperature, reconstruct waters with CO 2 loss, correct for the deficit of water and other volatiles (CO 2,gas , H 2 S gas ) from boiling, and determine the amount of mixing of thermal and non-thermal waters. RTEst can use data with basis species below detection limit, missing, or unreliable either by assuming equilibrium with a controlling mineral (fixed-analyte method) or by treating the analyte concentration as an optimization parameter. The inverse of variance weighting method included in RTEst provides more representative results than either the normalization or unit weighting methods. Finally, the ability of RTEst to calculate reservoir temperatures, gas fugacity, and mixing fractions demonstrates its usefulness as a tool for evaluating geothermal systems.

15 GEOTHERMAL ENERGY↗
NASA NTRS1975

Evaluation and characterization of the methane-carbon dioxide decomposition reaction

A program was conducted to evaluate and characterize the carbon dioxide-methane (CO2-CH4) decomposition reaction, i.e., CO2 + CH4 = 2C + 2H2O. The primary objective was to determine the feasibility of applying this reaction at low temperatures as a technique for recovering the oxygen (O2) remaining in the CO2 which exits mixed with CH4 from a Sabatier CO2 reduction subsystem (as part of an air revitalization system of a manned spacecraft). A test unit was designed, fabricated, and assembled for characterizing the performance of various catalysts for the reaction and ultraviolet activation of the CH4 and CO2. The reactor included in the test unit was designed to have sufficient capacity to evaluate catalyst charges of up to 76 g (0.17 lb). The test stand contained the necessary instrumentation and controls to obtain the data required to characterize the performance of the catalysts and sensitizers tested: flow control and measurement, temperature control and measurement, product and inlet gas analysis, and pressure measurement. A product assurance program was performed implementing the concepts of quality control and safety into the program effort.

Davenport, R. J.↗
NASA NTRS1972

Fabrication, test and demonstration of critical environment monitoring system

Design and performance of an analytical system for the evaluation of certain environmental constituents in critical environmental areas of the Quality Reliability and Assurance Laboratory are reported. Developed was a self-contained, integrated, minimum sized unit that detects, interrogates, and records those parameters of the environment dictated for control in large storage facilities, clean rooms, temporarily curtained enclosures, and special working benches. The system analyzes humidity, temperature, hydrocarbons particle size, and particle count within prescribed clean areas.

Heimendinger, K. W.↗
NASA NTRS1979

Diode step stress program for JANTX1N2970b

Data for the purpose of evaluating the effect of power/temperature step stress was studied when applied to the zener diode JANTX1N2970B manufactured by Siemens and General Semiconductor, Inc. A total of 48 samples from each manufacturer was submitted to the process. In addition, two control sample units were maintained for verification of the electrical parametric testing. The tests for determining power/temperature stresses are described, and test results are discussed. Failure analyses for power stress, and temperature stress are presented.

Source record↗
NASA NTRS1979

Transister step stress testing program for JANTX2N3811

The effect was studied of power/temperature step stress when applied to the dual transistor JANTX2N3811 manufactured by Motorola and National Semiconductor. A total of 48 samples from Motorola and 47 from National Semiconductor was submitted to the processes. In addition, two control sample units were maintained for verification of the electrical parametric testing. The tests for determining power/temperature stresses are described, and test results are discussed. Failure analyses for power stress, and temperature stress are presented.

Source record↗
NASA NTRS1991

A ground test program to support condition monitoring of a spacecraft attitude control propulsion system

The Comet Rendezvous Asteroid Flyby (CRAF) mission involves seven years of flight from 0.6 to 4.57 Astronomical Units (AU), followed by about 915 days of maneuvering around a comet. Ground testing will characterize the very critical attitude control system thrusters' fuel consumption and performance for all anticipated fuel temperatures over thruster life. The ground test program characterization will support flight condition monitoring. A commercial software application hosted on a commercial microcomputer will control ground test operations and data acquisition using a newly designed thrust stand. The data acquisition and control system uses a graphics-based language and features a visual interface to integrate data acquisition and control.

Clark, Douglas J.↗
NASA NTRS1992

Space Station external thermal control system design and operational overview

The driving design requirements and resulting design characteristics for a two-phase ammonia system of the Space Shuttle are reviewed with particular attention given to operational and station assembly issues related to system activation and steady-state operation. Design is described at an overall system level and an orbit replaceable unit level. It is concluded that a system flow network must be designed and ammonia pressures must be controlled to acquire waste heat efficiently from all contributing heat sources at a controlled temperature.

Raetz, John↗
NASA NTRS2012

Design and Operation of the Planetary In-Situ Capillary Electrophoresis System (PISCES)

The PISCES instrument is a portable, miniature, modular instrument designed to analyze organic molecular signatures of life. PISCES uses microcapillary electrophoresis (μCE) with laser-induced fluorescence detection (LIFD) to analyze fluorescently-labeled analytes prepared on a multi-layer microfluidic chip. As a modular instrument composed of five independently functioning units, each module can be easily detached from the system and used for subsystem testing in different environments, e.g. low temperature. The pneumatic module contains mechanical and electrical components necessary to control pneumatically-actuated valves for on-chip sample processing. A prototype LabVIEW program and two custom printed circuit boards (PCBs) operate the pneumatics module using an Arduino microcontroller, and a tentative design for the module’s housing has been developed. The high-voltage module contains circuitry required to apply varying electrical potentials to the electrophoretic channel of the microdevice. Work is currently being done to design the circuit and PCB for this module in collaboration with our SBIR partners at Los Gatos Research. The optical electronics module contains the spectrometer, laser, and laser power supply. The mounting components for the electronics and housing for the module have been designed, assembled, and tested. The optical module contains optical components to focus the laser to a 20μm spot in the center of the electrophoretic channel.The housing for this module has been designed and assembled with the aligned optical components inside.

Willis, Peter A.↗
NASA NTRS2012

Design of a High Temperature Radiator for the Variable Specific Impulse Magnetoplasma Rocket

The Variable Specific Impulse Magnetoplasma Rocket (VASIMR), currently under development by Ad Astra Rocket Company (Webster, TX), is a unique propulsion system that could change the way space propulsion is performed. VASIMR's efficiency, when compared to that of a conventional chemical rocket, reduces the propellant needed for exploration missions by a factor of 10. Currently plans include flight tests of a 200 kW VASIMR system, titled VF-200, on the International Space Station (ISS). The VF-200 will consist of two 100 kW thruster units packaged together in one engine bus. Each thruster core generates 27 kW of waste heat during its 15 minute firing time. The rocket core will be maintained between 283 and 573 K by a pumped thermal control loop. The design of a high temperature radiator is a unique challenge for the vehicle design. This paper will discuss the path taken to develop a steady state and transient-based radiator design. The paper will describe the radiator design option selected for the VASIMR thermal control system for use on ISS, and how the system relates to future exploration vehicles.

Sheth, Rubik B.↗
DOE OSTI2025

Bench-Scale Apparatus for Rapid, Simultaneous, Comprehensive Vapor–Liquid Equilibrium and Kinetic Property Measurements to Advance CO 2 Capture Solvent Technology

We present here, the design, fabrication, and testing of a new "pressure, volume, temperature (PVT)" apparatus that enables rapid standardized testing for viscosity, vapor–liquid equilibria, and kinetics for water-lean carbon capture solvents. This unit is the first of its kind where equilibrium data are collected during operation as a PTx (pressure–temperature–composition) cell while kinetic data are collected simultaneously with an internal mini wetted-wall contactor (WWC) using controlled adjustments of CO 2 injections to allow for measurements of gas flux (in and out of the liquid). Additionally, in situ measurements of viscosity data are also continuously collected while a solvent is in circulation during gas absorption. This cell empowers comprehensive testing of critical CO 2 capture solvent properties in a single measurement, ensuring all data are collected at the same temperature, pressure, and CO 2 loading. This apparatus also expedites screening of materials since less than 50 mL of sample is needed as compared to 2–3 L needed to get similar data from a conventional WWC. In conclusion, we describe here the methodology of data collected on this new PVT cell, nicknamed “Gary” in honor of Professor Gary Rochelle, for multiple water-lean amine solvents, which we compare to data collected from conventional instrumentation for amine testing.

Zheng, Richard [STARS Technology Corporation, Rich↗
NASA NTRSDate not supplied

Thermal Performance Comparison and Lessons Learned for the Thermal Infrared Sensor Instruments 1 & 2

The Thermal Infrared Sensor (TIRS-1) is one of two instruments on the Landsat-8 Mission, which launched in February of 2013 and remains operational. The TIRS-2 instrument was developed for the Landsat-9 Mission, which is scheduled to launch in September of 2021. The TIRS-2 instrument design was adjusted to account for requirements changes and to include key lessons learned from its predecessor. The overall thermal subsystem design of the TIRS Sensor Unit remained comparable from mission to mission, but there were some areas that needed modifications. The general design is comprised of five thermal zones which range in temperature from less than 43 Kelvin to 320 Kelvin. Most zones are proportional heater controlled. A two-stage cryocooler provided by Ball Aerospace is used to cool the cryogenic subsystem, and excess power dissipation is rejected via ammonia transport heat pipes to a dedicated cryocooler radiator with embedded ammonia heat pipes. The cryogenic subsystem includes a series of shells used to radiatively and conductively isolate the cold stage from the warmer surroundings. The Optical System (telescope) is passively cooled to 180-195 Kelvin using a dedicated radiator with embedded dual-bore ethane heat pipes. The warmer end of the instrument includes a Scene Select Mechanism, an on-board Black Body Calibrator with a dedicated radiator, and a Focal Plane Electronics Box, all of which are attached to the Sensor Unit primary structure. The TIRS-1 thermal subsystem design was successfully verified during an extended testing campaign and during more than 8years of on-orbit operations. The TIRS-2 thermal subsystem design was successfully verified during months of ground testing prior to delivery in August of 2019and at the Observatory level in the Spring of 2021. A detailed comparison of the thermal performance of the two instruments has been made with a focus on key lessons learned during each instrument development, and with the benefit of on-orbit data acquired for the TIRS-1 instrument.

Veronica Otero↗
DOE OSTI2025

Experimental demonstration of real-time electron temperature profile control in DIII-D

Future tokamak reactor operation will require the ability to maintain a given plasma scenario for extended periods of time. This will necessitate the capability to react to changes in the plasma state and return the plasma to the target scenario; the principal method to achieve this is through feedback control. Thus, it is necessary to develop and test feedback controllers for the plasma profiles that define a target scenario. In this work, a feedback controller for the electron temperature (Te) profile is tested experimentally in DIII-D. This experiment relied on the ability to ascertain the electron temperature profile in real time, which was achieved using an observer algorithm. The observer relies on both diagnostic data and a predictive model of the electron temperature profile evolution; this predictive model includes contributions from neural network surrogate models. Because of these dependencies, a number of capabilities needed to be added to the real-time PCS for DIII-D in order to support the Te profile control experiment. The neural network surrogates needed to be integrated into the PCS to be called in real time. An observer algorithm for the Te profile needed to be added and connected to the Thomson scattering system to allow access to the current state of the profile in real time. When tested, the observer was shown to produce Te profiles that are consistent with the shape of the Thomson scattering data while rejecting much of the noise in the diagnostic data. Finally, the controller itself was tested in real time. This experiment showed that the controller is capable of tracking the electron temperature target at locations across the spatial profile.

Morosohk, Shira [Oak Ridge Associated Universities↗
DOE OSTI2025

Benchtop-Scale High Temperature Molten Salt Electrochemical Reactors: Experimental Setup and Considerations

Molten salt electrochemical reduction (MSER) is the dominant production method for aluminum and titanium, and emerging technologies for producing other commodity metals with these highly electrified techniques have demonstrated promising results. However, the scale up of MSER of materials such as iron and silicon are limited by the challenging issues of materials compatibility and impurity control. This work describes an experimental MSER setup using both chloride and carbonate salts. This setup is designed for operations outside of a glovebox, which is practical from an industrial perspective, but creates unique challenges. This work serves as a practical guide to discuss some key operational difficulties such as temperature control, air and humidity, material compatibility, developing strong electrical measurements and techniques, and safety.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2022

Cold Climate Heat Pump Evaluation

The use of heat pumps in cold and very cold climates increased by 63% between 2009 and 2015 [1, 2]. This can be attributed to development of heat pumps with higher heating capacity at lower temperatures and increased efficiency. A primary technology driving this trend is the use of variable-speed compressors, which come with an increase in the level of controls in the equipment. Most units with variable-speed compressors also include electronic expansion valves and variable-speed indoor (ID) and outdoor (OD) fans. With the increased complexity of these systems, developing a test procedure that is representative of typical performance and not too burdensome on manufacturers presents a difficult challenge.

32 ENERGY CONSERVATION, CONSUMPTION, AND UTILIZATI↗
DOE OSTI2023

Quantum Computing – Real-Time Data Processing from a Dilution Refrigerator

This poster presents a real-time data visualization system for monitoring and displaying data from a Bluefors control unit connected to a dilution refrigerator. The goal is to provide an aesthetically pleasing and user-friendly web-based interface that continuously updates and displays critical data such as temperature and flow rates at various points within the refrigerator. Leveraging WebSocket technology, the system establishes multiple connections to the dilution refrigerators, enabling simultaneous monitoring of several units. The interactive webpage dynamically updates the data, providing researchers and operators with instant insights into the system's performance. The system's ability to stream and visualize data in real-time enhances the understanding of the dilution refrigerator's behavior, aiding in optimizing its operation and ensuring efficient scientific experiments. The application's web-based nature makes it easily accessible from any device with internet connectivity, promoting seamless collaboration and remote monitoring capabilities. Overall, this poster offers a comprehensive solution for real-time data visualization and analysis of dilution refrigerators, catering to the needs of researchers and scientists working in low-temperature physics and quantum computing fields.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
NASA NTRS1988

Hybrid regenerative fuel cell systems for space applications

This paper describes a hybrid regenerative fuel cell (RFC) system for space application, which is made up of an alkaline fuel cell (Space Shuttle fuel cell) and an acid electrolysis unit (solid polymer electrolyte). In the RFC, gas produced from the acid electrolysis unit and water produced by the alkaline fuel cell are repeatedly reacted in the other unit. The results of RFC's tests indicate that the system is feasible in terms of fluid/unit compatibility. In addition, the fuel cell thermal-control system proved capable of controlling fuel cell temperatures throughout long open-circuit periods. Diagrams of the RFC and its subsystems are included.

Saucier, David R.↗