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At least 271 records · Page 15

Acoustic emission testing of composite vessels under sustained loading

Acoustic emissions (AE) generated from Kevlar 49/epoxy composite pressure vessels subjected to sustained load-to-failure tests were studied. Data from two different transducer locations on the vessels were compared. It was found that AE from vessel wall-mounted transducers showed a wide variance from those for identical vessels subjected to the same pressure loading. Emissions from boss-mounted transducers did, however, yield values that were relatively consistent. It appears that the signals from the boss-mounted transducers represent an integrated average of the emissions generated by fibers fracturing during the vessel tests. The AE from boss-mounted transducers were also independent of time for vessel failure. This suggests that a similar number of fiber fractures must occur prior to initiation of vessel failure. These studies indicate a potential for developing an AE test procedure for predicting the residual service life or integrity of composite vessels.

Lark, R. F.↗

Rb-Sr ages and initial Sr-87/Sr-86 for Apollo 17 basalts and KREEP basalt 15386

The Rb-Sr data reported for Apollo 17 mare basalts and for KREEP basalt 15386 is used to determine mineral isochrons. The weighted average age of four Apollo 17 basalts is 3.76 + or - 0.06 AE, while the age determined for 15386 is 3.94 + or - 0.04 AE. The isotopic data for the Apollo 17 basalts are discussed in the context of Sm and Eu data for the same samples. The Sr-isotopic data are fit best by a three-stage model evolution involving evolution of Sr-87/Sr-86 in an environment with Rb/Sr greater than in the basalts, production of mare basalt source regions of lower but variable Rb/Sr sometime in the interval 4.6 to 3.75 AE ago, and extraction of lavas from these sources 3.75 AE ago. Other possibilities are considered.

Nyquist, L. E.↗

Fracture modes and acoustic emission of composite materials

Unidirectional fibrous composite material laminae are the construction material of a laminate. Four failure modes can occur in this material, and the identification of these modes is as important as the identification of onset of fracture. Acoustic emission (AE) pulses, generated by the change in the stress field resulting from cracking in a material, have a unique pattern of amplitude distribution that depends only on the mode of fracture and the type of material. By using a tapered double-cantilever beam as grips for the unidirectional lamina, a crack with a constant stress intensity factor was induced, thus eliminating the factor of the stress level. Placing the lamina in different directions relative to the grips imposed a different failure mode. By plotting the log of the relative number of AE pulses above some level versus the log of the relative level, a single constant coefficient can be measured for each material and mode of fracture. The AE energy is proportional to the energy released by the cracking; this proportionality depends on the medium where the AE waves have to travel, and not on the cracking mode.

Rotem, A.↗

Lead isotope systematics of mare basalt 75075

Uranium, thorium and isotopic lead data are reported for two bulk samples and separated pyroxene, ilmenite and plagioclase from basalt 75075. In a concordia diagram the whole rock, ilmenite and four pyroxene samples define a chord intersecting the concordia curve at approximately 4.25 and 2.8 AE. Three plagioclase samples plot distinctly off the chord. The crystallization age of 75075 is accurately determined at 3.74 AE by Rb-Sr, Sm-Nd and K-Ar measurements from other laboratories. It is not possible to adjust the isotopic composition of initial lead so as to reconcile the U-Pb data with a crystallization age of 3.74 AE. The data therefore indicate some type of post-crystallization disturbance of the U-Pb system that is not detected by the other systems. The 75075 data are one of the few examples of this type of age pattern found on the moon. If the disturbance was a single event, it probably occurred around 2.8 AE ago, the time indicated by the pyroxene, whole rock and ilmenite data.

Chen, J. H.↗

Characterization of delamination and transverse cracking in graphite/epoxy laminates by acoustic emission

Efforts to characterize and differentiate between two major failure processes in graphite/epoxy composites - transverse cracking and Mode I delamination are described. Representative laminates were tested in uniaxial tension and flexure. The failure processes were monitored and identified by acoustic emission (AE). The effect of moisture on AE was also investigated. Each damage process was found to have a distinctive AE output that is significantly affected by moisture conditions. It is concluded that AE can serve as a useful tool for detecting and identifying failure modes in composite structures in laboratory and in service environments.

Garg, A.↗

A proposal for the proper use of pseudopotentials in molecular orbital cluster model studies of chemisorption

The interaction of CO with Cu5, Ni5, and Al4 are treated as model systems for molecular adsorption on metal surfaces. The effect of the use of pseudopotentials for the metal atoms is studied by considering three types of clusters. In the first case, all of the metal electrons are explicitly included in the wave function; an all electron (AE) treatment. In the second case, the metal atom which directly interacts with the CO is described by AE but the remaining metal atoms include a pseudopotential for their core electrons. Finally, in the third case, all of the metal atoms in the cluster have a pseudopotential treatment for the core electrons. The AE cluster results are taken as reference values for the two pseudopotential treatments. The mixed cluster results are in excellent agreement with those of the all AE clusters; however, the results for the all pseudopotential cluster of Ni5CO or of Cu5CO are qualitatively different. The pseudopotential treatment for all of the metal atoms often leads to results that contain serious errors and it is not a reliable approach.

Bagus, P. S.↗

Characterization of delamination and transverse cracking in graphite/epoxy laminates by acoustic emission

Efforts to characterize and differentiate between two major failure processes in graphite/epoxy composites - transverse cracking and Mode I delamination - are described. Representative laminates were tested in uniaxial tension and flexure. The failure processes were monitored and identified by acoustic emission (AE). The effect of moisture on AE was also investigated. Each damage process was found to have a distinctive AE output that is significantly affected by moisture conditions. It is concluded that AE can serve as a useful tool for detecting and identifying failure modes in composite structures in laboratory and in service environments.

Garg, A.↗

Failure during thermal cycling of plasma-sprayed thermal barrier coatings

The thermal cycling behavior of plasma-sprayed ZrO2-12 wt pct Y2O3 coatings was studied. Coatings were produced with and without bond coats of Ni-Cr-Al-Zr and in some cases the substrates were heated to above the optimum temperature prior to spraying. The coatings (attached to the substrate) were thermal cycled to 1200 C and their cracking behavior was followed by acoustic emission (AE) techniques. It was possible to examine the failure mechanisms by statistical analysis of the AE data and to evaluate the influence of preheating and bond coating. It is shown that the AE spectrum changes when a bond coat is used because of the presence of microcracks which, in turn, dissipate energy and improve the coating integrity. The preheating effect is reflected by a decrease in the peak count rate and an increase in the temperature at which AE activity is initiated.

Berndt, C. C.↗

Global large scale structures in the F region

Measurements of neutral densities, temperatures and ion density and temperature by the Atmosphere Explorer C and E satellites exhibit fluctuations made up of coherent waves of scale size from hundreds to thousands of kilometers. The fluctuations in the AE-C data are found at times of low magnetic activity to extend from the auroral region in one hemisphere across the equator to the corresponding region in the other hemisphere with little change in apparent wavelength. The fluctuations in the AE-E data similarly exhibit at times of low magnetic activity nearly uniform wave structure encircling the equatorial belt. Typical examples of waves of more than 1000 km apparent wavelength in both the AE-C and AE-E data are presented. These observations during quiet times may be explained by a system of quasi-stationary waves excited by the auroral belts that are distributed about the Earth possibly with tidal or sub-tidal periods and scale lengths determined by the structure of the belts. According to this interpretation, Traveling Ionospheric Disturbance (TID's) are manifestations of transient wave systems moving past a ground observatory that result from changes in magnetic activity with periods and scale sizes associated with the regions of enhanced auroral activity. Some evidence suggesting tidal-like stationary waves from the Millstone Hill incoherent scatter radar is presented.

Gross, S. H.↗

Punch stretching process monitoring using acoustic emission signal analysis. II - Application of frequency domain deconvolution

The coloring effect on the acoustic emission signal due to the frequency response of the data acquisition/processing instrumentation may bias the interpretation of AE signal characteristics. In this paper, a frequency domain deconvolution technique, which involves the identification of the instrumentation transfer functions and multiplication of the AE signal spectrum by the inverse of these system functions, has been carried out. In this way, the change in AE signal characteristics can be better interpreted as the result of the change in only the states of the process. Punch stretching process was used as an example to demonstrate the application of the technique. Results showed that, through the deconvolution, the frequency characteristics of AE signals generated during the stretching became more distinctive and can be more effectively used as tools for process monitoring.

Liang, Steven Y.↗

Interplanetary Alfven waves and auroral (substorm) activity - IMP 8

Almost 1 year of IMP 8 interplanetary magnetic field and plasma data (days 1-312, 1979) have been examined to determine the interplanetary causes of geomagnetic AE activity. The nature of the interplanetary medium (Alfvenic or non-Alfvenic) and the B(s) correlation with AE were examined over 12-hour increments throughout the study. It is found that Alfvenic wave intervals are present over 60 percent of the time, and the southward component of the Alfven waves is well correlated with AE (average peak correlation coefficient 0.62), with a median lag of 43 min. From this statistical study, no major differences in the magnetospheric response to Alfvenic and non-Alfvenic intervals were obvious. The high-intensity long-duration continuous AE activity (HILDCAA) events discussed previously by Tsurutani and Gonzales (1987) are demonstrated to be caused by the southward components of the Alfven waves, presumably through the process of magnetic reconnection.

Tsurutani, Bruce T.↗

Burst prediction by acoustic emission in filament-wound pressure vessels

Acoustic emission in 51-cm diameter graphite/epoxy pressure vessels was monitored during pressurization (hydrotesting). Several vessels were subjected to impact by a blunt impactor, but only after the vessels had been proofed; that is, pressurized to 80 percent of nominal burst pressure as determined from control (unimpacted) vessels. AE activity was then monitored throughout a series of successively higher pressure cycles ranging from 10 to 60 percent of ultimate. Each cycle included a ramp up to pressure followed by a 4-min hold period and then pressure unload. The event rate was high, and especially modified AE analyzers had to be used to acquire the data. This paper presents the AE event count versus pressure history of these tests and demonstrates the ability of the AE technique to monitor the growth of damage and to estimate the effect on ultimate strength. The number of events that occurred during pressure holds proved to be a reasonable estimator of vessel performance.

Gorman, Michael R.↗

Acoustic emission monitoring of low velocity impact damage in graphite/epoxy laminates during tensile loading

An acoustic emission (AE) system was set up in a linear location data acquisition mode to monitor the tensile loading of eight-ply quasi-isotropic graphite/epoxy specimens containing low velocity impact damage. The impact damage was induced using an instrumented drop weight tower. During impact, specimens were supported by either an aluminum plate or a membrane configuration. Cross-sectional examinations revealed that the aluminum plate configuration resulted in primarily matrix cracking and back surface fiber failure. The membrane support resulted in only matrix cracking and delamination damage. Penetrant enhanced radiography and immersion ultrasonics were used in order to assess the amount of impact damage in each tensile specimen. During tensile loading, AE reliably detected and located the damage sites which included fiber failure. All specimens with areas of fiber breakage ultimately failed at the impact site. AE did not reliably locate damage which consisted of only delaminations and matrix cracking. Specimens with this type of damage did not ultimately fail at the impact site. In summary, AE demonstrated the ability to increase the reliability of structural proof tests; however, the successful use of this technique requires extensive baseline testing.

Parker, Bradford H.↗

Acoustic emission from a solidifying aluminum-lithium alloy

Physical phenomena associated with the solidification of an AA2090 Al-Li alloy have been characterized by AE methods. Repeatable patterns of AE activity as a function of solidification time are recorded and explained for ultrahigh-purity (UHP) aluminum and an Al-4.7 wt pct Cu binary alloy, in addition to the AA2090 Al-Li alloy, by the complementary utilization of thermal, AE, and metallographic methods. One result shows that the solidification of UHP aluminum produces one discrete period of high AE activity as the last 10 percent of solid forms.

Henkel, D. P.↗

Electron spectroscopy analysis

The Surface Science Laboratories at the University of Alabama in Huntsville (UAH) are equipped with x-ray photoelectron spectroscopy (XPS or ESCA) and Auger electron spectroscopy (AES) facilities. These techniques provide information from the uppermost atomic layers of a sample, and are thus truly surface sensitive. XPS provides both elemental and chemical state information without restriction on the type of material that can be analyzed. The sample is placed into an ultra high vacuum (UHV) chamber and irradiated with x-rays which cause the ejection of photoelectrons from the sample surface. Since x-rays do not normally cause charging problems or beam damage, XPS is applicable to a wide range of samples including metals, polymers, catalysts, and fibers. AES uses a beam of high energy electrons as a surface probe. Following electronic rearrangements within excited atoms by this probe, Auger electrons characteristic of each element present are emitted from the sample. The main advantage of electron induced AES is that the electron beam can be focused down to a small diameter and localized analysis can be carried out. On the rastering of this beam synchronously with a video display using established scanning electron microscopy techniques, physical images and chemical distribution maps of the surface can be produced. Thus very small features, such as electronic circuit elements or corrosion pits in metals, can be investigated. Facilities are available on both XPS and AES instruments for depth-profiling of materials, using a beam of argon ions to sputter away consecutive layers of material to reveal sub-surface (and even semi-bulk) analyses.

Gregory, John C.↗

Acoustic emission measurements of aerospace materials and structures

A development status evaluation is given for aerospace applications of AE location, detection, and source characterization. Attention is given to the neural-like processing of AE signals for graphite/epoxy. It is recommended that development efforts for AE make connections between the material failure process and source dynamics, and study the effects of composite material anisotropy and inhomogeneity on the propagation of AE waves. Broadband, as well as frequency- and wave-mode selective sensors, need to be developed.

Sachse, Wolfgang↗

An investigation of theories of failure for ceramic matrix composites

This final report is comprised of the abstract of a masters thesis research grant. The abstract of the thesis, 'An Investigation of Acoustic Emission Techniques for the Discrimination of Damage Mechanisms in Ceramic Matrix Composites', is as follows: In order to further advance the understanding of the mechanical behavior of ceramic matrix composites (CMS's), acoustic emission (AE) techniques were implemented to monitor and identify damage mechanisms in CMC's under tensile loading. In addition to real-time AE monitoring techniques, a data acquisition system was developed and implemented in order to capture AE waveforms resulting from stress-induced damage. Waveforms were inspected for multiple events, separated in distinct events, and then analyzed to determine waveform characteristics in the time and frequency domains. Waveform characteristics included peak amplitude, event duration, MARSE, energy, and dominant and centroidal frequency. In addition to conventional methods for determining a damage discrimination criteria, a study of the distribution and correlation of the waveform characteristics criteria and a study of the distribution and correlation of the waveform characteristics were performed to aid in the determination of a damage discrimination criteria. The damage discrimination criteria was tested for 'uniqueness', i.e., the effectiveness of the criteria to identify and monitor damage independent of the stress-strain relationship. Insitu radiography was used to substantiate the damage accumulation. A simulation test was also performed over the loading history to study the changes in the waveform characteristics of the system response from a constant excitation. This thesis demonstrates the use of waveform analysis to study the AE activity resulting from stress-induced damage in CMC's in conjunction with other nondestructive evaluation techniques to investigate the mechanical behavior of CMC's.

Hemann, John H.↗

Neural Network Burst Pressure Prediction in Graphite/Epoxy Pressure Vessels from Acoustic Emission Amplitude Data

Acoustic emission (AE) data were taken during hydroproof for three sets of ASTM standard 5.75 inch diameter filament wound graphite/epoxy bottles. All three sets of bottles had the same design and were wound from the same graphite fiber; the only difference was in the epoxies used. Two of the epoxies had similar mechanical properties, and because the acoustic properties of materials are a function of their stiffnesses, it was thought that the AE data from the two sets might also be similar; however, this was not the case. Therefore, the three resin types were categorized using dummy variables, which allowed the prediction of burst pressures all three sets of bottles using a single neural network. Three bottles from each set were used to train the network. The resin category, the AE amplitude distribution data taken up to 25 % of the expected burst pressure, and the actual burst pressures were used as inputs. Architecturally, the network consisted of a forty-three neuron input layer (a single categorical variable defining the resin type plus forty-two continuous variables for the AE amplitude frequencies), a fifteen neuron hidden layer for mapping, and a single output neuron for burst pressure prediction. The network trained on all three bottle sets was able to predict burst pressures in the remaining bottles with a worst case error of + 6.59%, slightly greater than the desired goal of + 5%. This larger than desired error was due to poor resolution in the amplitude data for the third bottle set. When the third set of bottles was eliminated from consideration, only four hidden layer neurons were necessary to generate a worst case prediction error of - 3.43%, well within the desired goal.

Hill, Eric v. K.↗