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NASA NTRS1985

Tough composite materials: Recent developments

The present volume broadly considers topics in composite fracture toughness and impact behavior characterization, composite system constituent properties and their interrelationships, and matrix systems' synthesis and characterization. Attention is given to the characterization of interlaminar crack growth in composites by means of the double cantilever beam specimen, the characterization of delamination resistance in toughened resin composites, the effect of impact damage and open holes on the compressive strength of tough resin/high strain fiber laminates, the effect of matrix and fiber properties on compression failure mechanisms and impact resistance, the relation of toughened neat resin properties to advanced composite mechanical properties, and constituent and composite properties' relationships in thermosetting matrices. Also treated are the effect of cross-link density on the toughening mechanism of elastomer-modified epoxies, the chemistry of fiber/resin interfaces, novel carbon fibers and their properties, the development of a heterogeneous laminating resin, solvent-resistant thermoplastics, NASA Lewis research in advanced composites, and opportunities for the application of composites in commercial aircraft transport structures.

Vosteen, L. F.↗

NASA NTRS1986

Loading rate effect on interlaminar fracture toughness of a thermoplastic composite

A study was undertaken to investigate the loading rate effect on delamination fracture initiation toughness of a thermoplastic composite. For this purpose, double cantilever beam specimens of graphite/PEEK were tested in a displacement controlled mode using an Instron tensile test machine. Specimens were loaded at various crosshead speeds ranging from 0.05 cm/min to 100 cm/min. The interlaminar fracture toughness was found to decrease with increasing loading rate, and this decrease was more than one hundred percent over the five decades of loading rate employed.

Mall, S.↗

NASA NTRS1986

Mode 1 delamination growth in adhesively bonded joints under static and fatigue loads

The objective of this investigation was to characterize the pure mode 1 delamination growth in metal to metal adhesively bonded joints under static and fatigue loading conditions, using FM 73 adhesive. Double cantilever beam specimens (DCB) were used for pure mode 1 tests. Aluminum 2024-T3 adherends were bonded with FM 73 adhesive. Delamination was introduced during fabrication by inserting a Teflon film between the two adherends. The mode 1 strain energy release rate G sub I sub c was obtained directly from static DCB tests conducted in accordance with the ASTM designation D1876-12. Constant amplitude fatigue tests on DCB specimens were conducted to determine the relationship between delamination growth rate da/dN and strain energy release rate G sub I sub c for a pure mode 1 delamination growth. It is found that the debond propagation rate in adhesive joints using FM 73 is more sensitive to errors in design load than is typical crack growth rate in metallic structures.

Biswas, S. C.↗

NASA NTRS1986

The identification of a distributed parameter model for a flexible structure

A computational method is developed for the estimation of parameters in a distributed model for a flexible structure. The structure we consider (part of the RPL experiment) consists of a cantilevered beam with a thruster and linear accelerometer at the free end. The thruster is fed by a pressurized hose whose horizontal motion effects the transverse vibration of the beam. The Euler-Bernoulli theory is used to model the vibration of the beam and treat the hose-thruster assembly as a lumped or point mass-dashpot-spring system at the tip. Using measurements of linear acceleration at the tip, it is estimated that the parameters (mass, stiffness, damping) and a Voight-Kelvin viscoelastic structural damping parameter for the beam using a least squares fit to the data. Spline based approximations to the hybrid (coupled ordinary and partial differential equations) system are considered; theoretical convergence results and numerical studies with both simulation and actual experimental data obtained from the structure are presented and discussed.

Banks, H. T.↗

NASA NTRS1986

Effect of adherend thickness and mixed mode loading on debond growth in adhesively bonded composite joints

Symmetric and unsymmetric double cantilever beam (DCB) specimens were tested and analyzed to assess the effect of: (1) adherend thickness, and (2) a predominantly mode I mixed mode loading on cyclic debond growth and static fracture toughness. The specimens were made of unidirectional composite (T300/5208) adherends bonded together with EC3445 structural adhesive. The thickness was 8, 16, or 24 plies. The experimental results indicated that the static fracture toughness increases and the cyclic debond growth rate decreases with increasing adherend thickness. This behavior was related to the length of the plastic zone ahead of the debond tip. For the symmetric DCB specimens, it was further found that displacement control tests resulted in higher debond growth rates than did load control tests. While the symmetric DCB tests always resulted in cohesive failures in the bondline, the unsymmetric DCB tests resulted in the debond growing into the thinner adherend and the damage progressing as delamination in that adherend. This behavior resulted in much lower fracture toughness and damage growth rates than found in the symmetric DCB tests.

Mangalgiri, P. D.↗

NASA NTRS1987

An evaluation of higher-order model methods for calculating transient structural response

A higher-order modal method proposed by Leung for transient structural analysis entitled the force-derivative method is evaluated. This method repeatedly integrates by parts with respect to time the convolution-integral form of the structural response to produce successively better approximations to the contribution of the higher modes which are neglected in the modal summation. Comparisons are made of the force-derivative, the mode-displacement, and the mode-acceleration methods for several numerical example problems for various times, levels of damping, and forcing functions. The example problems include a tip-loaded cantilevered beam and a simply-supported multispan beam. The force-derivative method is shown to converge to an accurate solution in fewer modes than either the mode-displacement or the mode-acceleration methods. In addition, for problems in which there are a large number of closely-spaced frequencies whose mode shapes have a negligible contribution to the response, the force-derivative method is very effective in representing the effect of the important, but otherwise neglected, higher modes.

Camarda, Charles J.↗

NASA NTRS1987

Structural control by the use of piezoelectric active members

Large Space Structures (LSS) exhibit characteristics which make the LSS control problem different form other control problems. LSS will most likely exhibit low frequency, densely spaced and lightly damped modes. In theory, the number of these modes is infinite. Because these structures are flexible, Vibration Suppression (VS) is an important aspect of LSS operation. In terms of VS, the control actuators should be as low mass as possible, have infinite bandwidth, and be electrically powered. It is proposed that actuators be built into the structure as dual purpose structural elements. A piezoelectric active member is proposed for the control of LSS. Such a device would consist of a piezoelectric actuator and sensor for measuring strain, and screwjack actuator in series for use in quasi-static shape control. An experiment simulates an active member using piezoelectric ceramic thin sheet material on a thin, uniform cantilever beam. The feasibility of using the piezoelectric materials for VS on LSS was demonstrated. Positive positive feedback as a VS control strategy was implemented. Multi-mode VS was achieved with dramatic reduction in dynamic response.

Fanson, J. L.↗

NASA NTRS1987

Micro and macro approaches to tough polymers for composites

The progress to date on the development of techniques to toughen continuous thermoplastic composites is summarized. The work, using the approach of toughening the polycarbonate composite matrix with rubber particles, has focused on determining the differences between Double Cantilever Beam (DCB) samples molded inhouse and those molded by NASA. Specifically, an effort was made to account for the differences in fracture toughness observed between the various specimens. In addition, preliminary results of tensile dilatometry tests are described; these tests suggest that processes leading to increased volume and enhanced shear banding are occurring within the rubber toughened system. The results of the effort using another approach, the preparation of random block copolycarbonates, are presented. The synthetic route to these species was modified so that higher molecular weights of these materials can be obtained. In addition, an attempt is being made to determine the exact block length or the number of functional groups in the oligomers since this procedure also should lead to high molecular weight materials. Dynamic mechanical analysis of the copolymer prepared so far indicates that the scale of cooperative molecular motion of the PBA polycarbonate at sub-Tg temperatures is larger than five monomer units. Efforts to find a suitable rubber-toughener for a thermoset system (bismaleimides) is also discussed. Included is a description of the various tougheners intended for use or currently being used.

Yee, Albert F.↗

NASA NTRS1987

Vibrations and structureborne noise in space station

Analytical models were developed to predict vibrations and structureborne noise generation of cylindrical and rectangular acoustic enclosures. These models are then used to determine structural vibration levels and interior noise to random point input forces. The guidelines developed could provide preliminary information on acoustical and vibrational environments in space station habitability modules under orbital operations. The structural models include single wall monocoque shell, double wall shell, stiffened orthotropic shell, descretely stiffened flat panels, and a coupled system composed of a cantilever beam structure and a stiffened sidewall. Aluminum and fiber reinforced composite materials are considered for single and double wall shells. The end caps of the cylindrical enclosures are modeled either as single or double wall circular plates. Sound generation in the interior space is calculated by coupling the structural vibrations to the acoustic field in the enclosure. Modal methods and transfer matrix techniques are used to obtain structural vibrations. Parametric studies are performed to determine the sensitivity of interior noise environment to changes in input, geometric and structural conditions.

Vaicaitis, R.↗

NASA NTRS1986

Three-dimensional vibrations of twisted cantilevered parallelepipeds

A large number of references dealing with the vibrations of twisted, cantilevered beams and plates exist in the literature. These works show considerable disagreement concerning the effect of twist angle upon frequencies. The present work is the first three-dimensional study of the problem. Displacement components are assumed in the form of algebraic polynomials which satisfy the fixed face conditions exactly, and which are mathematically complete. The Ritz method is then applied. Accurate frequencies are calculated for twisted thick plates and are compared with ones obtained recently by others using beam, shell, and finite element theory.

Leissa, A.↗

NASA NTRS1986

Synthesis of control laws for optimally designed large space structures

In this study, the vibration control of large space structures using the linear quadratic regulator technique is investigated. Emphasis is made on the control of both optimally designed structures and also the original (uniform) structures using the cantilever beam as an example. The open loop and closed loop eigenvalues are compared and the transient responses are obtained to determine the effectiveness of the control system design.

Satyanarayana, K.↗

NASA NTRS1986

The effects of radiation on the interlaminar fracture toughness of a graphite/epoxy composite

An experimental study is made of the effect of electron irradiation (10 to the 10th rad), simulating a 30-year geosynchronous orbit exposure, on the fracture toughness of a graphite/epoxy composite, T300/934. The double cantilever beam (DBC) test is used to determine Mode I (peel) critical strain energy release rate and the edge delamination tension (EDT) test is used to determine mixed Mode I and II (peel and shear) critical strain energy release rate. It is found that the electron interaction of the epoxy matrix material enhances the fracture toughness properties of the composite and that the test temperature has a significant effect on the fracture toughness of both baseline and irradiated material.

Funk, J. G.↗

NASA NTRS1986

Introduction to GRASP - General rotorcraft aeromechanical stability program - A modern approach to rotorcraft modeling

The General Rotorcraft Aeromechanical Stability Program (GRASP), which is a hybrid between finite element programs and spacecraft-oriented multibody programs, is described in terms of its design and capabilities. Numerical results from GRASP are presented and compared with the results from an existing, special-purpose coupled rotor/body aeromechanical stability program and with experimental data of Dowell and Traybar (1975 and 1977) for large deflections of an end-loaded cantilevered beam. The agreement is excellent in both cases.

Hodges, D. H.↗

NASA NTRS1987

Rate-dependent mode I interlaminar crack growth mechanisms in graphite/epoxy and graphite/PEEK

In this paper the mode I fracture behavior of graphite/epoxy and graphite/PEEK composites is examined over four decades of crosshead rates (0.25-250 mm/min). Straight-sided double-cantilever-beam specimens consisting of unidirectional laminates were tested at room temperature. For graphite/epoxy the load-deflection response was linear to fracture, and stable slow crack growth initiating at the highest load level was observed for all rates tested. In contrast, mode I crack growth in the graphite/PEEK material was often unstable and showed stick-slip behavior. Subcritical crack growth occurring prior to the onset of fracture was observed at intermediate displacement rates. A mechanism for the fracture behavior of the graphite/PEEK material (based on viscoelastic, plastic, and microcrack coalescence in the process zone) is proposed and related to the observed rate-dependent phenomena.

Gillespie, J. W., Jr.↗

NASA NTRS1986

Evaluation of several modal methods for transient structural analysis

The convergence properties of three modal methods for solving structural transient response (STR) problems are examined by comparing the accuracy of the total number of modes used to represent the responses. The goal is to identify a method which involves as few degrees of freedom as possible. Two mode superposition methods, the mode displacement method (MDM) and the mode acceleration method (MAM), are fitted with equivalent expressions for damped response. An error norm is employed to compare the accuracies of the methods in calculating displacements, moments, and shear forces for a viscously-damped cantilevered beam experiencing several dynamic loading conditions and levels of damping. The MAM converges quicker and uses fewer dof, mainly because it has a pseudo-static response term which accounts for some of the flexibility of higher modes. A third method, which integrates the convolution integral iteratively over time, generates a higher order approximation to the STR with a reduced number of modes. It converges fastest among the three, but requires definition of an appropriate forcing function. Finally, the MAM and MDM models are applied to study the effects of the forcing frequency and the initial conditions.

Camarda, Charles J.↗

NASA NTRS1987

Matrix resin effects in composite delamination - Mode I fracture aspects

A number of thermoset, toughened thermoset, and thermoplastic resin matrix systems were characterized for Mode I critical strain energy release rates, and their composites were tested for interlaminar critical strain energy release rates using the double cantilever beam method. A clear correlation is found between the two sets of data. With brittle resins, the interlaminar critical strain energy release rates are somewhat larger than the neat resin values due to a full transfer of the neat resin toughness to the composite and toughening mechanisms associated with crack growth. With tougher matrices, the higher critical strain energy release rates are only partially transferred to the composites, presumably because the fibers restrict the crack-tip deformation zones.

Hunston, Donald L.↗

NASA NTRS1987

Rate effects on delamiantion fracture toughness of a toughened graphite/epoxy

The objective of this study was to determine the effects of loading rate on interlaminar fracture toughness of T300/F-185 graphite/epoxy composite, having an elastomer-modified epoxy resin matrix. Mode I interlaminar fracture was investigated by means of uniform width and width-tapered double cantilever beam (DCB) specimens. Hinged tabs were used to insure unrestrained rotation at the free ends. Specimens were loaded at quasi-static deflection rates of up to 8.5 mm/s corresponding to crack extension rates of up to 21 mm/s. Crack extension was monitored by means of strain gages mounted on the surface of the specimen. Continuous records were obtained of load, deflection, and crack extension for determination of the strain energy release rate. The latter was calculated by means of the area method and beam analysis method, and expressed as a power law of the crack extension velocity. Results indicate that the strain energy release rate decreases with crack velocity by over 20 percent over three decades of crack velocity.

Daniel, Isaac M.↗

NASA NTRS1987

Interfacial strength development in thermoplastic resins and fiber-reinforced thermoplastic composites

An experimental program to develop test methods to be used to characterize interfacial (autohesive) strength development in polysulfone thermoplastic resin and graphite-polysulfone prepreg during processing is reported. Two test methods were used to examine interfacial strength development in neat resin samples. These included an interfacial tension test and a compact tension (CT) fracture toughness test. The interfacial tensile test proved to be very difficult to perform with a considerable amount of data scatter. Thus, the interfacial test was discarded in favor of the fracture toughness test. Interfacial strength development was observed by measuring the refracture toughness of precracked compact tension specimens that were rehealed at a given temperature and contact time. The measured refracture toughness was correlated with temperature and contact time. Interfacial strength development in graphite-polysulfone unidirectional composites was measured using a double cantilever beam (DCB) interlaminar fracture toughness test. The critical strain energy release rate of refractured composite specimens was measured as a function of healing temperature and contact time.

Howes, Jeremy C.↗