Development of nondestructive testing techniques for honeycomb heat shields Annual program report, 1 Jul. 1964 - 30 May 1965
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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.
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Energy transfer in reacting flow of pyrolysis products through char layer of nylon-phenolic resin charring ablator
Energy transfer in pyrolysis product flow through char layer of nylon phenolic resin ablator
Dispersion strengthened TD-NiCr alloy for space shuttle reentry shields
Improvements in the processes and design to reduce the manufacturing costs for low density ablative panels for the space shuttle are discussed. The areas that were studied included methods of loading honeycomb core, alternative reinforcement concepts, and the use of reusable subpanels. A review of previous studies on the fabrication of low-cost ablative panels and on permissible defects that do not affect thermal performance was conducted. Considerable differences in the quoted prices for ablative panels, even though the various contractors had reported similar fabrication times were discovered. How these cost differences arise from different estimating criteria and which estimating assumptions and other costs must be included in order to arrive at a realistic price are discussed.
The goal of the ablation technology program is to bring ablation research and development to a high state of readiness for application to space shuttle vehicles. Some recent results and current work in the areas of materials, designs, and refurbishment for ablative TPS are reported. Future research and development needs are also presented.
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Results are presented of a program of research to develop a reliable, high performance, fused slurry silicide coating for the Ta-10W alloy. The effort was directed toward developing new and improved formulations for use at 2600 to 2800 F (1700 to 1811 K) in an atmospheric reentry thermal protection system with a 100-mission capability. Based on a thorough characterization of isothermal and cyclic oxidation behavior, bend transition temperatures, room- and elevated-temperature tensile properties, and creep behavior, a 2.5 Mn-33Ti-64.5Si coating (designated MTS) provides excellent protection for the Ta-10W alloy in simulated reentry environments. An extensive analysis of the oxidation behavior and characteristics of the MTS coating in terms of fundamental mechanisms also is presented.
The experimental and coating process details are presented. The process specifications which were developed for the formulation and application of the R-512E fused slurry silicide coating using either an acrylic or nitrocellulose base slurry system is also discussed.
Description of the formulation and evaluation of low-density elastomeric ablative compounds and low-cost techniques for fabricating and installing ablative panels being considered for the Space Shuttle orbiter's thermal protection system. Sixteen large panels, both flat and contoured, were successfully fabricated and time-studied to develop and refine tooling and manufacturing methods and to establish a realistic baseline for estimating costs. Six of the panels were bonded to a DC-3 airframe. The work included a detailed estimate of fabrication and installation costs.
White, volume-reflecting dielectric material absorbs essentially none of the incident radiant energy, and continues to reflect even though in severe environment its surface is melted and is being vaporized. Process of overall reflectance in dielectric material, involving internal refractions and reflections, is similar to process of reflection in paints.
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Analysis methods for predicting cyclic creep deflection in stiffened metal panel structures, were applied to full size panels. Results were compared with measured deflections from cyclic tests of thin gage L605, Rene' 41, and TDNiCr full size corrugation stiffened panels. A design criteria was then formulated for metallic thermal protection panels subjected to creep. A computer program was developed to calculate creep deflections.
An Outer Planets Probe which retains the charred heatshield during atmospheric descent must deploy a sampling tube through the heatshield to extract atmospheric samples for analysis. Once the sampling tube is deployed, the atmospheric samples ingested must be free of contaminant gases generated by the heatshield. Outgassing products such as methane and water vapor are present in planetary atmospheres and hence, ingestion of such species would result in gas analyzer measurement uncertainties. This paper evaluates the potential for, and design impact of, the extracted atmospheric samples being contaminated by heatshield outgassing products. Flight trajectory data for Jupiter, Saturn and Uranus entries are analyzed to define the conditions resulting in the greatest potential for outgassing products being ingested into the probe's sampling system. An experimental program is defined and described which simulates the key flow field features for a planetary flight in a ground-based test facility. The primary parameters varied in the test include: sampling tube length, injectant mass flow rate and angle of attack. Measured contaminant levels predict the critical sampling tube length for contamination avoidance. Thus, the study demonstrates the compatibility of a retained heatshield concept and high quality atmospheric trace species measurements.
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Because of the loss of ductility with exposure to oxidizing conditions, long time applications of titanium alloys have been limited to temperatures below 700 K and short time applications have been limited to temperatures below 815 K. Oxygen barrier coatings for shielding Ti-6Al-2Sn-4Zr-2Mo alloy from oxidation during exposure to high temperatures were studied using foil gage specimens. The coatings included micrometer-thick sputtered SiO2 and chemical-vapor-deposited silicate layers both with and without an aluminum basecoat. The oxidation rates and resistance to embrittlement of the coated specimens were significantly better than those of the uncoated specimens.
Optical-properties data for ceramic fabrics woven from silica, aluminoborosilicate, or silicon carbide yarns are presented. The normal hemispheric reflectances and transmittances measured at room temperature and over the spectral range of 250 to 2500 nm show a large dependence on fabric weight and a lesser dependence on fabric weave pattern. Reflectances of silicon carbide fabrics are lower by a factor of about 10 than those of silica and aluminoborosilicate. The reflectance and transmittance of silica and aluminoborosilicate fabrics decrease at wavelengths below 500 nm because of material absorption. A two-flux analytical model is used to derive spectral absorption and scattering coefficients for the silica and aluminoborosilicate fabrics from the measured reflectance and transmittance data, and comparisons are made with available data for other ceramics.