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At least 271 records · Page 15

Engineering the Interface: Advanced Surface Technologies for Lunar Dust Management and Equipment Longevity

Through the Artemis program, NASA intends to develop a sustainable human foothold on the Moon, ultimately paving the way for crewed exploration of Mars. The Moon's hostile environment poses numerous obstacles, including exposure to radiation, temperature extremes, micrometeoroid threats, and particularly the persistent problem of lunar dust. Lunar dust impacts nearly every aspect of surface operations through adhesion and abrasion mechanisms, with contamination from anthropogenic activities (landing, rovers) far outweighing natural phenomena. Multiple adhesion pathways contribute to surface contamination in the lunar environment, including van der Waals forces, electrostatic forces, chemical reaction, and magnetic forces from elemental iron deposits. Sharp asperities from micrometeoroid bombardment and atmospheric absence increase interaction potential and enable mechanical interlocking. Low cohesion between dust particles exacerbates these challenges, as minimal interaction potential between dust and nearby surfaces overcomes particle cohesion, causing contamination. Lunar dust adhesion mitigation technologies can be categorized as either active, requiring external energy, or passive, relying on intrinsic material properties. Ultrasonic and electrodynamic technologies have been developed to the highest technology readiness level for active approaches. Passive strategies primarily focus on surface chemistry and topography modifications. At NASA Langley Research Center, approaches include surface migration agents to reduce surface energy, topographical modification using laser ablation patterning, and tailored surface conductivity to reduce intrinsic adhesion force. Performance has been evaluated using custom-built ultrasonic and centrifuge instruments. Plume-surface interactions from lunar landers can propel micrometer-sized particles at velocities up to 1000 m s-1.8 These particles pose risks to landers, habitats and infrastructure, leading to erosion, degradation, and reduced component lifespan. A panel recovered from Surveyor III was determined to have been severely abraded because of lunar dust displaced from the Apollo 12 lunar module that landed 160 m away. The performance of metallic surfaces has been evaluated via high velocity single particle impact using the laser-induced project impact test (LIPIT) facility at the University of Utah. Peridynamics modeling, a form of continuum mechanics that uses a nonlocal approach enabling greater simulation capabilities of crack initiation and fracture, has also been utilized to gain greater insight into material response during impact events. Lunar dust contamination challenges extend to power generation systems and moving equipment. Cables, rotation stages, and other mechanisms may experience limited range of motion and reduced lifetime due to dust infiltration. NASA Langley Research Center has evaluated traditional aerospace alloys, softgoods, wear resistant ceramics, and several polymer and polymer composite materials. Test methods have included traditional techniques like Taber abrasion testing, as well as designed test configurations developed in the DUSTE (dust, ultraviolet radiation, and space thermal environmental) chamber that reproduce mechanism functions in operational environment. Beyond laboratory experiments, several flight experiments have been conducted. Materials were exposed to the low Earth orbit environment on the Materials International Space Station Experiment (MISSE) and to the lunar surface environment through the Aegis Aerospace Regolith Adherence Characterization (RAC) payload and the Honeybee Robotics PlanetVac payload. Determining lunar dust's impact on surface exploration and habitation requires comprehensive experimental and computational capabilities combined with lessons learned from initial lunar activities. Identifying the greatest environmental challenges and developing mitigation technologies provides the clearest path toward successfully, expeditiously, and efficaciously completing NASA's mission. This presentation will discuss ongoing efforts at NASA Langley Research Center and collaborator contributions to these critical objectives.

Surface Engineering↗

Photothermal Properties of Nanostructured Black Titanium Dioxide for Targeted Cellular and Microbial Elimination

Heterophase black titanium dioxide (hB-TiO 2 ), characterized by broadened near-infrared (NIR) absorption, has emerged as a promising photothermally active nanomaterial. This study focused on the synthesis of nanoscale hB-TiO 2 and its evaluation as a multifunctional agent for photothermal therapy (PTT). The purity and composition of the mixed-phase nanoscale hB-TiO 2 were demonstrated by X-ray diffraction, and the morphology of nanoparticles was imaged by transmission electron microscopy. Extensive additional characterization was conducted to validate the optoelectronic properties. The material was further evaluated in biological systems using NIH 3T3-GFP fibroblasts and the fungus Candida albicans. Nanoscale hB-TiO 2 exhibited good biocompatibility in the absence of laser irradiation and effectively ablated both NIH 3T3-GFP cells and C. albicans following 20 min of laser exposure. This noninvasive treatment strategy leverages NIR-responsive materials to induce localized hyperthermia. The findings provide grounds for the use of selectively induced hyperthermia, which could be employed for the targeted destruction of cells or fungi with minimal impact on surrounding tissue if the material is functionalized with specific targeting groups and delivered to cells or fungal infections.

Irradiation↗

Micromechanics-Based Structural Analysis (FEAMAC) and Multiscale Visualization within Abaqus/CAE Environment

A unified framework is presented that enables coupled multiscale analysis of composite structures and associated graphical pre- and postprocessing within the Abaqus/CAE environment. The recently developed, free, Finite Element Analysis--Micromechanics Analysis Code (FEAMAC) software couples NASA's Micromechanics Analysis Code with Generalized Method of Cells (MAC/GMC) with Abaqus/Standard and Abaqus/Explicit to perform micromechanics based FEA such that the nonlinear composite material response at each integration point is modeled at each increment by MAC/GMC. The Graphical User Interfaces (FEAMAC-Pre and FEAMAC-Post), developed through collaboration between SIMULIA Erie and the NASA Glenn Research Center, enable users to employ a new FEAMAC module within Abaqus/CAE that provides access to the composite microscale. FEA IAC-Pre is used to define and store constituent material properties, set-up and store composite repeating unit cells, and assign composite materials as sections with all data being stored within the CAE database. Likewise FEAMAC-Post enables multiscale field quantity visualization (contour plots, X-Y plots), with point and click access to the microscale i.e., fiber and matrix fields).

Arnold, Steven M.↗

Investigation of a Macromechanical Approach to Analyzing Triaxially-Braided Polymer Composites

A macro level finite element-based model has been developed to simulate the mechanical and impact response of triaxially-braided polymer matrix composites. In the analytical model, the triaxial braid architecture is simulated by using four parallel shell elements, each of which is modeled as a laminated composite. The commercial transient dynamic finite element code LS-DYNA is used to conduct the simulations, and a continuum damage mechanics model internal to LS-DYNA is used as the material constitutive model. The material stiffness and strength values required for the constitutive model are determined based on coupon level tests on the braided composite. Simulations of quasi-static coupon tests of a representative braided composite are conducted. Varying the strength values that are input to the material model is found to have a significant influence on the effective material response predicted by the finite element analysis, sometimes in ways that at first glance appear non-intuitive. A parametric study involving the input strength parameters provides guidance on how the analysis model can be improved.

Goldberg, Robert K.↗

A numerical procedure for predicting creep and delayed failures in laminated composites

A numerical procedure is described for predicting the viscoelastic response of general laminates. A nonlinear compliance model is used to predict the creep response of the individual laminae. A biaxial delayed failure model predicts ply failure. The numerical procedure, based on lamination theory, increases by increments through time to predict creep compliance and delayed failures in laminates. Numerical stability problems and experimental verification are discussed. Although the program has been quite successful in predicting creep of general laminates, the assumptions associated with lamination theory have resulted in erroneous bounds on the predicted material response. Delayed failure predictions have been conservative. Several improvements are suggested to increase the accuracy of the procedure.

Dillard, D. A.↗

Recent Developments to the Porous Microstructure Analysis (PuMA) Software

The Porous Microstructure Analysis (PuMA) software is a suite of tools for the analysis of porous materials and generation of material microstructures. From microstructural data, often obtained through X-ray microtomography, PuMA can determine a number of effective material properties and perform material response simulations. Version 2.2 includes capabilities for computing volume fractions, porosity, specific surface area, effective thermal and electrical conductivities, and continuum and rarefied diffusive tortuosity. PuMA can also simulate competitive diffusion/reaction processes at the micro-scale, such as surface oxidation. In this poster, recent advancements to the PuMA software are detailed, including the full refactoring of PuMA into v3.0, a new module to compute heat conduction in anisotropic materials, a particle method for simulating molecular beam experiments, a new finite-volume Laplace solver, complex fibrous material generation, woven material generation, and a coupling of PuMA with the DAKOTA software for advanced statistics.

PuMA↗

Micro-Structural Response of DP 600 to High Strain Rate Deformation

The object of this study was to investigate the micro-structural response of DP 600 subjected to high strain rate, ballistic impact tests. The ballistic tests were conducted using normal impact of a hardened steel penetrator into a 2 mm thick sheet of DP 600. The average strain rates produced from this test method are on the order of 10(exp 5)/s. Electron microscopy was used to investigate the microstructure before and after high strain rate deformation. A variation in material response was observed between tests conducted at 0.8 x 105 and 25 x 10(exp 5)/s.

Hamburg, Brian↗

Research and development program for the development of advanced time-temperature dependent constitutive relationships. Volume 1: Theoretical discussion

The results of a 10-month research and development program for the development of advanced time-temperature constitutive relationships are presented. The program included (1) the effect of rate of change of temperature, (2) the development of a term to include time independent effects, and (3) improvements in computational efficiency. It was shown that rate of change of temperature could have a substantial effect on the predicted material response. A modification to include time-independent effects, applicable to many viscoplastic constitutive theories, was shown to reduce to classical plasticity. The computation time can be reduced by a factor of two if self-adaptive integration is used when compared to an integration using ordinary forward differences. During the course of the investigation, it was demonstrated that the most important single factor affecting the theoretical accuracy was the choice of material parameters.

Cassenti, B. N.↗

Results from Two Full-Scale Hawker 4000 Fuselage Drop Tests

In the spring of 2022, NASA Langley Research Center (LaRC) conducted two full-scale drop tests on a Hawker 4000 partial fuselage structure for the evaluation of composite material response under dynamic impact loading conditions. The specific objectives of the tests were to induce dynamic composite damage initiation and progression and in primary structure and to understand the nature of the failure modes. The tests were conducted via dividing the fuselage hardware into three smaller sections. Dynamic drop tests were conducted on the forward and aft portions of the fuselage under different dynamic loading conditions, while the middle section was reserved for materials testing. Both tests were conducted by dropping the test articles from a height of 14 feet with significant amounts of pitch, which was added to initiate damage in specific regions of the structure. The test articles were ballasted then instrumented with accelerometers at various locations and speckle-coated on both exterior sides with a black and white stochastic pattern for use with three-dimensional digital image correlation (3D-DIC). In addition, the interior belly portion of the forward section test article was also speckle-coated, which was intended to capture deformations on the belly of the test article from the interior at impact. The interior of the aft section test article was not speckle-coated. Prior to testing, bow-tie markers were applied at various locations for use in marker tracking, to measure impact conditions such as vertical impact velocity and pitch. In this report, a partial summary of the data collected from the tests is presented. The data was primarily in the form of accelerometers to measure impact acceleration and 3D-DIC to measure deformation and failure onset and propagation. Post-test inspections revealed the primary damage mechanism was fiber cracking and delamination primarily in and around the area that contacted the impact surface. Acceleration pulse shapesin the ballast locations were trapezoidal in nature and ranged between 10 g and 40 g, depending on the location and test.

full scale testing↗

Results from Two Full-Scale Hawker 4000 Fuselage Drop Tests

In the spring of 2022, NASA Langley Research Center (LaRC) conducted two full-scale drop tests on a Hawker 4000 partial fuselage structure for the evaluation of composite material response under dynamic impact loading conditions. The specific objectives of the tests were to induce dynamic composite damage initiation and progression and in primary structure and to understand the nature of the failure modes. The tests were conducted via dividing the fuselage hardware into three smaller sections. Dynamic drop tests were conducted on the forward and aft portions of the fuselage under different dynamic loading conditions, while the middle section was reserved for materials testing. Both tests were conducted by dropping the test articles from a height of 14 feet with significant amounts of pitch, which was added to initiate damage in specific regions of the structure. The test articles were ballasted then instrumented with accelerometers at various locations and speckle-coated on both exterior sides with a black and white stochastic pattern for use with three-dimensional digital image correlation (3D-DIC). In addition, the interior belly portion of the forward section test article was also speckle-coated, which was intended to capture deformations on the belly of the test article from the interior at impact. The interior of the aft section test article was not speckle-coated. Prior to testing, bow-tie markers were applied at various locations for use in marker tracking, to measure impact conditions such as vertical impact velocity and pitch. In this report, a partial summary of the data collected from the tests is presented. The data was primarily in the form of accelerometers to measure impact acceleration and 3D-DIC to measure deformation and failure onset and propagation. Post-test inspections revealed the primary damage mechanism was fiber cracking and delamination primarily in and around the area that contacted the impact surface. Acceleration pulse shapesin the ballast locations were trapezoidal in nature and ranged between 10 g and 40 g, depending on the location and test.

full scale testing↗

Lessons Learned from Aerothermal Flight Data on NASA Mars Entry Vehicles

The NASA Mars Science Laboratory (MSL) and Mars 2020 entry vehicles included temperature measurements inside and direct heat flux on the surface of the thermal protection system (TPS) material. The instrumentation was included to begin addressing predictive capabilities for aerodynamic heating and ablative TPS material response. The MSL aeroshell included temperature measurements at seven heatshield locations, from which total aerodynamic heating was reconstructed. The Mars 2020 instrumentation suite included eleven heatshield measurement locations and new backshell measurements at nine locations: six with temperature sensors, two with sensors to directly measure total heat flux, and one to measure radiative heat flux. Both instrumentation suites returned full sets of data, with all temperature sensors nearest to the surface surviving entry, indicating minimal material recession. Heatshield boundary layer transition (BLT) was observed for both vehicles prior to the time of peak heating, with transition starting near the shoulder and progressing towards the stagnation area. MSL’s higher speed on approach to Mars resulted in higher total heating compared to Mars 2020, with the maximum occurring near the heatshield’s leeside shoulder. The Mars 2020 backshell heating data indicate significant contributions from shock layer radiation. Heating from Navier-Stokes flowfield calculations are in family with reconstructed heating. The paper covers the instrumentation, BLT and reconstructed heating on both heatshields, backshell heating for Mars 2020, TPS performance, and predicted versus reconstructed heat fluxes. Opportunities for improved design approaches for future Mars missions are discussed, especially for the upcoming Mars Sample Return mission.

Mars Science Laboratory↗

Lessons Learned from Aerothermal Flight Data on NASA Mars Entry Vehicles

The NASA Mars Science Laboratory (MSL) and Mars 2020 entry vehicles included temperature measurements inside and direct heat flux on the surface of the thermal protection system (TPS) material. The instrumentation was included to begin addressing predictive capabilities for aerodynamic heating and ablative TPS material response. The MSL aeroshell included temperature measurements at seven heatshield locations, from which total aerodynamic heating was reconstructed. The Mars 2020 instrumentation suite included eleven heatshield measurement locations and new backshell measurements at nine locations: six with temperature sensors, two with sensors to directly measure total heat flux, and one to measure radiative heat flux. Both instrumentation suites returned full sets of data, with all temperature sensors nearest to the surface surviving entry, indicating minimal material recession. Heatshield boundary layer transition (BLT) was observed for both vehicles prior to the time of peak heating, with transition starting near the shoulder and progressing towards the stagnation area. MSL’s higher speed on approach to Mars resulted in higher total heating compared to Mars 2020, with the maximum occurring near the heatshield’s leeside shoulder. The Mars 2020 backshell heating data indicate significant contributions from shock layer radiation. Heating from Navier-Stokes flowfield calculations are in family with reconstructed heating. The paper covers the instrumentation, BLT and reconstructed heating on both heatshields, backshell heating for Mars 2020, TPS performance, and predicted versus reconstructed heat fluxes. Opportunities for improved design approaches for future Mars missions are discussed, especially for the upcoming Mars Sample Return mission.

Mars Science Laboratory↗

Icarus Application to Dragonfly Heatshield

Icarus, an in-house material response solver developed at NASA Ames, is applied to perform 2-D bondline-temperature analysis on the heatshield surface of the latest Dragonfly entry system design for a mission to Titan. Two axisymmetric domains are used: the near-shoulder region and the entire heatshield. The heatshield consists of a PICA TPS bonded to a layered system of Aluminum honeycomb wrapped by an M55J carbon-fiber facesheet. The backshell, which is also included for more accurate analysis, consists of similar materials layered. Icarus simulations using both domains indicate that the in-plane thermal conductivity property of the M55J facesheet is observed to play a dominant role in bondline temperature. Similarly, the maximum bondline temperature is found around the PICA-tile-interface region instead of the near-shoulder region or the stagnation point based on the current trajectory using the orthotropic properties of M55J. Therefore, these findings indicate the significance of 2-D or higher-dimensional material modeling analysis in fully understanding how bondline temperature behaves across the heatshield and obtaining a basis for TPS design locations. Verification at different radial locations ahead of the shoulder, where thermal conduction is close to 1-D, between Icarus (2-D), Icarus (1-D), and FIAT is performed and good agreement is observed. With the entire heatshield domain, the total mass loss of the aeroshell materials is approximately 3% of their initial mass potentially due to thermal decomposition of phenolic resins inside PICA under the current high-heating environment.

TPS material modeling↗

TPSAS-NF1676L-13792-DND

Extreme structural requirements of future aerospace vehicles motivate the development of new, ultra-durable materials and game-changing methodologies for material certification and sustainment. Computational simulations spanning many orders of magnitude in length and time scales—from the nanoscale of underlying damage processes to the larger scales of continuum cracks—are being developed to support these requirements. Results of these simulations are used to deduce key aspects of material response to loads and environments, including: - The microstructural mechanics that govern metal fatigue crack initiation and growth - The variety and complexity of the dislocation-precipitate interac- tions that underpin plastic behavior and damage evolution - The energetic principles that govern the interaction of water with crack surfaces within a structural component - The mechanics of grain boundary separation Modeling the physics behind these metal fatigue behaviors is extremely complex, and requires intensive, high-fidelity simulations. The knowledge gained through these simulations, however, is forming the keystone for advanced material design and will enable development of more capable, reliable structures for aerospace vehicles.

Jacob Hochhalter↗

Characterization of ablator dynamics initiated by picket-pulse conditions

Direct-drive laser-fusion targets may include low-cost plastic ablator material. Here, this work describes a tabletop experimental system designed to enable the investigation of the interaction of such ablator material as a function of the laser wavelength and the associated excitation mechanism. This experimental system offers time-resolved imaging of the material response with subpicosecond temporal resolution and ≈1-μm spatial resolution. The system involves synchronized femtosecond and picosecond lasers to initiate and characterize the dynamics of polystyrene planar targets irradiated by conditions similar to a “picket” prepulse from a direct-drive pulse shape. Ultrafast imaging of the initial excitation process followed by the resulting critical plasma formation, shock-wave propagation, and blowoff plasma expansion is used to compare the impact of excitation wavelength, 355 nm or 266 nm, on the ensuing dynamics. This work aims to investigate fundamental laser material interactions to help advance physics models that can inform the development of laser driver and target designs.

42 ENGINEERING↗

Informing ARC divertor design and plasma facing material selection through integrated modeling

This INFUSE 2023 project between UCLA and Commonwealth Fusion Systems used computer modeling to test whether tungsten materials can survive in CFS's ARC fusion reactor divertor. The team simulated plasma conditions and material responses, finding that tungsten-rhenium alloys resist grain growth better than pure tungsten, and that hydrogen buildup depends more on particle flux than temperature. The work helps CFS design durable plasma-facing components for their fusion power plant.

36 MATERIALS SCIENCE↗

2024 roadmap on magnetic microscopy techniques and their applications in materials science

Considering the growing interest in magnetic materials for unconventional computing, data storage, and sensor applications, there is active research not only on material synthesis but also characterisation of their properties. In addition to structural and integral magnetic characterisations, imaging of magnetisation patterns, current distributions and magnetic fields at nano- and microscale is of major importance to understand the material responses and qualify them for specific applications. In this roadmap, we aim to cover a broad portfolio of techniques to perform nano- and microscale magnetic imaging using superconducting quantum interference devices, spin centre and Hall effect magnetometries, scanning probe microscopies, x-ray- and electron-based methods as well as magnetooptics and nanoscale magnetic resonance imaging. The roadmap is aimed as a single access point of information for experts in the field as well as the young generation of students outlining prospects of the development of magnetic imaging technologies for the upcoming decade with a focus on physics, materials science, and chemistry of planar, three-dimensional and geometrically curved objects of different material classes including two-dimensional materials, complex oxides, semi-metals, multiferroics, skyrmions, antiferromagnets, frustrated magnets, magnetic molecules/nanoparticles, ionic conductors, superconductors, spintronic and spinorbitronic materials.

2D materials↗

Recrystallization, cracking, and erosion of dispersoid-strengthened tungsten materials during exposure to divertor plasmas

In this study, we investigated the effects of combined intense particle and heat flux exposure on advanced tungsten plasma-facing materials within the DIII-D fusion facility. Our test matrix included two types of dispersoid-strengthened tungsten (containing either 100 nm diameter TiO 2 or Ni particles), along with high-purity polycrystalline tungsten as a reference. This experiment relied on a sample geometry angled at 15° relative to the divertor surface, thereby allowing the surfaces to intercept steady-state perpendicular heat fluxes (q ⟂ ) ranging from 10.1 to 19.6 MW/m 2 . During each shot, the samples were exposed to 42 Hz edge-localized modes (ELMs), allowing us to test the material response to transient heating. We correlated the exposure conditions with extensive post-test surface composition analysis and microscopy to determine how the plasma modified each surface. The angled specimens closest to the strike point received the highest combined heat and particle flux and melted midway through the experiment. EBSD analysis revealed they were completely recrystallized throughout, with an average grain size >100 µm. On the other hand, the specimens that received a lower steady state heat flux survived with more superficial surface damage. Whereas the high-purity polycrystalline tungsten exhibited a higher surface roughness, the dispersoid-strengthened material exhibited more extensive shallow inter-granular cracking. In addition, the surface was depleted of dispersoids following plasma exposure, possibly because of evaporation and/or sputtering. The results described here provide insights into the performance of these materials in a fusion environment which can guide further optimization for use in long-pulse devices.

Kolasinski, Robert D. [Sandia National Laboratorie↗