Interdisciplinary Materials Research Program Semiannual Progress Report, 1 Mar. - 31 Aug. 1967
Materials science research on inorganic nonmetallic materials, metallic solids, polymers, and solid state physics
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Materials science research on inorganic nonmetallic materials, metallic solids, polymers, and solid state physics
Interdisciplinary materials research in inorganic nonmetallic materials, metallic solids, polymers, and solid state physics
Plane strain fracture toughness determined for crack notched bend specimens using standard test procedure for specific metallic material property
Specimen size and mechanical factors in plane strain fracture toughness testing of metallic materials
Development of structural framework with zero or negligible thermal expansion is discussed. Combination of two types of metallic materials in binary trellis to compensate for thermal expansion is explained. Construction details are presented and illustration is included.
Method fabricates stabilized composite conductor, for use in construction of magnets, using equal amounts of superconducting and metal materials, thus reducing weight, cost and size.
The sputtering process is described in terms of its features: versatility, momentum transfer, configuration of target, precise controls and the relatively slow deposition rate. Sputtered films are evaluated in terms of adherence, coherence, and internal stresses. The strong adherence is attributed to the high kinetic energies of the sputtered material, sputter etched (cleaned) surface, and the submicroscopic particle size. An illustration is a sputtered solid film lubricant such as MoS2. Friction tests were conducted on a thin, 2000 A deg thick MoS2 film. These films are very dense and without observable pinholes, and the particle to particle cohesion is strong. Tolerances (film thickness) can be controlled to a millionth of a centimeter. Very adherent films of sputtered Teflon can be deposited in a single operation on any type of material (metal, glass, paper) and on any geometrical configuration with a dense adherent film.
Container design is used to convert partially densified powder metallurgy compacts into fully densified slabs in one processing step. Technique improves product yield, lowers costs and yields great flexibility in process scale-up. Technique is applicable to all types of fabricable metallic materials that are produced from powder metallurgy process.
Quality control of wheels and rails can be improved by using ultrasonic technique developed for measuring stresses in metallic materials. In addition, parts already in use can be tested and replaced if they are found to be unsafe. Test equipment includes two transducers.
The development of metal structures reinforced with filamentary composites as a weight saving feature of the space shuttle components is discussed. A frame was selected for study that was representative of the type of construction used in the bulk frames of the orbiter vehicle. Theoretical and experimental investigations were conducted. Component tests were performed to evaluate the critical details used in the designs and to provide credibility to the weight saving results. A model frame was constructed of the reinforced metal material to provide a final evaluation of the construction under realistic load conditions.
An improved method of boundary collocation was applied to the two-dimensional stress analysis of the compact specimen. The effects of the pin-loaded holes on stress-intensity factors and crack-opening displacements were investigated for various crack-length-to-specimen-width ratios, hole locations, and internal loadings. The stress-intensity factors for the 'standard' compact specimen under plane-stress or plane-strain conditions were found to be within 1 percent of the stress-intensity factors reported in the ASTM Test for Plane-Strain Fracture Toughness of Metallic Materials (E 399-72) over a range of crack-length-to-specimen-width ratios of 0.4 to 0.7. However, for crack-length-to-specimen-width ratios less than 0.4, the pin-load holes (which were not previously accounted for) had a significant effect on stress intensity and crack-opening displacements.
The basic relationship of ultrasonic signal velocity to directional subsurface stress is reviewed. Inappropriateness of dependency on a single correlative value of constant for a three dimensional stress field in metallic materials is discussed. Implementation of conventional ultrasonic nondestructive testing capabilities integrated to provide a composite technique for the measurement of orthogonal stress components is described, and the procedures for performing the preparatory calibration and subsequent stress field measurements are presented. In conclusion, the prime effect of stress on ultrasonic signal velocity occurs only in the direction of material excitation or particle motion.
This experimental program was undertaken to investigate the crack growth behavior of deep surface flaws in 2219 aluminum. The program included tests of uniaxially loaded surface flaw and center crack panels at temperatures ranging from 20K (-423 F) to ambient. The tests were conducted on both the base metal and as-welded weld metal material. The program was designed to provide data on the mechanisms of failure by ligament penetration, and the residual cyclic life, after proof-testing, of a vessel which has been subjected to incipient penetration by the proof test. The results were compared and analyzed with previously developed data to develop guidelines for the proof testing of thin walled 2219 pressure vessels.
This communication describes the results of an experimental investigation of the fatigue characteristics of a boron-epoxy laminate containing an unloaded circular hole. The study focuses upon characterization of the fatigue damage incurred and its influence upon axial tensile residual strength. Two apparent anomalies in the fatigue behavior for this laminate were observed. First, the fatigue damage was observed to propagate tangentially to the edge of the notch (parallel to the direction of the load), in contrast to propagation in contemporary metallic materials which is perpendicular to the load direction. Second, the residual strength characteristics for the laminate have revealed a significant increase in residual strength subsequent to a fatigue loading of 500,000 cycles at R = 0.1 and S = 0.8 and 0.67 (S = maximum stress/static ultimate). Failure analyses of the fatigue damage are conducted utilizing ultrasonic 'C' scan techniques.
A description is presented of an automated space fabrication technique for basic structural elements, taking into account as representative the design loads and requirements of the solar power satellite structure. Roll forming for continuous cap and brace members is applicable for all proposed metallic materials. Spot-welding, electron beam welding, ultrasonic welding, laser welding, cold welding, and various mechanical fastening techniques are applicable for the automated fabrication process. Termination of the formed cap and brace members can be accomplished by sawing, shearing, punching, and laser cutting. The most cost effective materials were found to be the aluminum alloys. Selected for further study were AL20224T3 and AL2219-T62. In the area of fiber composites, thermoplastic matrix materials with graphite fibers were selected for future studies.
Solid-state low-temperature elastic properties have been experimentally studied at the NBS Cryogenic Division for four years. Most studies were between room temperature and liquid-helium temperature; some were only to liquid-nitrogen temperature. Two dynamic (high-frequency) experimental methods were used, pulse-echo and resonance, resulting in adiabatic elastic constants. The present paper reviews these studies for 47 technological materials - metals, alloys, and composites. The elastic constants primarily discussed are Young's modulus, the shear modulus, the bulk modulus (reciprocal compressibility), and Poisson's ratio. A summary table is presented to show which base metals tend to exhibit regular, irregular, or anomalous behavior in their elastic constant/temperature curves.
A computerized tool for the analysis of time independent cyclic plasticity structural response, life to crack initiation prediction, and crack growth rate prediction for metallic materials is described. Three analytical items are combined: the finite element method with its associated numerical techniques for idealization of the structural component, cyclic plasticity models for idealization of the material behavior, and damage accumulation criteria for the fatigue failure.
Since a large number of the procedures used for inspecting the external tank are concerned with determining flaws in welds, there is a need to develop an inspection technique, which can be automated, to determine flaws in welds and structures with complex geometries. Techniques whereby an eddy current is generated in a metallic material and the changes in the circuit parameters due to material differences are observed, were chosen as one possible approach. Pulsed eddy current and its relationship to multifrequency techniques is discussed as well as some preliminary results obtained from observing pulsed waveforms with apparatus and algorithms currently in use for ultrasonic testing of welds. It can be shown the pulsed eddy current techniques can provide similar results, can eliminate some of the noncritical parameters affecting the eddy current signals, and can facilitate in the detection of critical parameter such as flaws, subsurface voids, and corrosion.