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At least 271 records · Page 15

Direct VLBI detection of the magnetosphere surrounding the young star S1 in Rho Ophiuchi

VLBI 6-mm data are presently used to investigate the circularly polarized radio core previously identified around the young B3 star S1 in Rho Ophiuchi. The measured angular diameter and brightness temperature are found to be consistent with gyrosynchrotrom radiation emission from mildly relativistic electrons. A simple model based on a pole-on dipolar magnetic field of about 2 kG at the stellar surface suggests itself as consistent with the main observed features of the S1 magnetosphere; an important feature of the model is its taking the influence of the X-ray-emitting plasma into account. S1 may represent a new type of young stellar object, characterized by very extended magnetic fields.

Andre, Philippe↗

Energy resolution of the LZ detector for high-energy electronic recoils

The LUX-ZEPLIN (LZ) detector is a dual-phase liquid xenon time projection chamber (TPC) installed at the Sanford Underground Research Facility (Lead, South Dakota) at a depth of 1478 meters. Although the main objective of LZ is the direct detection of dark matter, its low background environment allows for the search of other rare processes, such as the neutrinoless double beta decay of xenon isotopes 134 Xe and 136 Xe with the respective Q-values of 826 keV and 2458 keV. The sensitivity of the detector to these decays is directly determined by the energy resolution, which, in turn, is degraded by non-uniformities in detector response. In this work, we present a novel method to correct, in the data, the non-uniformity of the light collected by an array of photosensors in a scintillation detector. This method is based on the knowledge of the light response functions of individual photosensors. With these techniques, we report, at a very early phase of the detector operations, a state-of-the-art energy resolution (σ/μ) of (0.67 ± 0.01)% at 2614 keV for the fiducial volume of 5.6 tonnes of liquid xenon.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

X-Ray Microanalysis and Electron Energy Loss Spectrometry in the Analytical Electron Microscope: Review and Future Directions

This paper reviews and discusses future directions in analytical electron microscopy for microchemical analysis using X-ray and Electron Energy Loss Spectroscopy (EELS). The technique of X-ray microanalysis, using the ratio method and k(sub AB) factors, is outlined. The X-ray absorption correction is the major barrier to the objective of obtaining I% accuracy and precision in analysis. Spatial resolution and Minimum Detectability Limits (MDL) are considered with present limitations of spatial resolution in the 2 to 3 microns range and of MDL in the 0.1 to 0.2 wt. % range when a Field Emission Gun (FEG) system is used. Future directions of X-ray analysis include improvement in X-ray spatial resolution to the I to 2 microns range and MDL as low as 0.01 wt. %. With these improvements the detection of single atoms in the analysis volume will be possible. Other future improvements include the use of clean room techniques for thin specimen preparation, quantification available at the I% accuracy and precision level with light element analysis quantification available at better than the 10% accuracy and precision level, the incorporation of a compact wavelength dispersive spectrometer to improve X-ray spectral resolution, light element analysis and MDL, and instrument improvements including source stability, on-line probe current measurements, stage stability, and computerized stage control. The paper reviews the EELS technique, recognizing that it has been slow to develop and still remains firmly in research laboratories rather than in applications laboratories. Consideration of microanalysis with core-loss edges is given along with a discussion of the limitations such as specimen thickness. Spatial resolution and MDL are considered, recognizing that single atom detection is already possible. Plasmon loss analysis is discussed as well as fine structure analysis. New techniques for energy-loss imaging are also summarized. Future directions in the EELS technique will be the development of new spectrometers and improvements in thin specimen preparation. The microanalysis technique needs to be simplified and software developed so that the EELS technique approaches the relative simplicity of the X-ray technique. Finally, one can expect major improvements in EELS imaging as data storage and processing improvements occur.

Goldstein, J. I.↗

Fixed-target serial femtosecond crystallography using in cellulo grown microcrystals

The crystallization of recombinant proteins in living cells is an exciting new approach in structural biology. Recent success has highlighted the need for fast and efficient diffraction data collection, optimally directly exposing intact crystal-containing cells to the X-ray beam, thus protecting the in cellulo crystals from environmental challenges. Serial femtosecond crystallography (SFX) at free-electron lasers (XFELs) allows the collection of detectable diffraction even from tiny protein crystals, but requires very fast sample exchange to utilize each XFEL pulse. Here, an efficient approach is presented for high-resolution structure elucidation using serial femtosecond in cellulo diffraction of micometre-sized crystals of the protein HEX-1 from the fungus Neurospora crassa on a fixed target. Employing the fast and highly accurate Roadrunner II translation-stage system allowed efficient raster scanning of the pores of micro-patterned, single-crystalline silicon chips loaded with living, crystal-containing insect cells. Compared with liquid-jet and LCP injection systems, the increased hit rates of up to 30% and reduced background scattering enabled elucidation of the HEX-1 structure. Using diffraction data from only a single chip collected within 12 min at the Linac Coherent Light Source, a 1.8 Å resolution structure was obtained with significantly reduced sample consumption compared with previous SFX experiments using liquid-jet injection. This HEX-1 structure is almost superimposable with that previously determined using synchrotron radiation from single HEX-1 crystals grown by sitting-drop vapour diffusion, validating the approach. This study demonstrates that fixed-target SFX using micro-patterned silicon chips is ideally suited for efficient in cellulo diffraction data collection using living, crystal-containing cells, and offers huge potential for the straightforward structure elucidation of proteins that form intracellular crystals at both XFELs and synchrotron sources.

Lahey-Rudolph, J. Mia (ORCID:0000000152797267)↗

Gamma ray polarimetry

Spectroscopic instruments currently being proposed may possess polarimetric capabilities which sould be nurtured and enhanced to permit characterization of basic emission mechanisms which are impossible using other techniques. Compton scattering and pair production detected the polarization of high energy (E is greater than 50 keV) protons in laboratory experiments. The polarization properties of a detection system consisting of 19 germanium crystals in a closed packed array are examined and the advantages of such a detector over Thompson scattering are discussed. The possiblity of using pair production to detect polarization of high energy gamma rays, and the associated modulation factors are discussed. The central difficulty involved in using pair production polarimeters in astrophysical applications is that the typical opening of the electron or positron direction with respect to the incident photon aircitron is small, of order E/sq mc. Multiple scattering in the material used to convert the photons to an electron positron pair causes deviations in the direction of the electron and positron.

Long, K. S.↗

Fiber optic links for microwave/millimeter-wave systems

Recent advances in device technology for microwave/mm-wave (M/MMW) analog fiber-optic communication systems are surveyed, with discussion of system parameters, design optimization methods, and hardware selection and manufacturing considerations. Particular attention is given to 1-km-link systems operating at 21, 30, and 12 GHz for satellite-communication, electronic-warfare, and radar applications. The design and fabrication simplicity of direct modulation is weighed against the wide bandwidth, low distortion, and mm-wave and frequency operation advantages of external modulation. Homodyne or heterodyne coherent detection is shown to improve system S/N by 10-20 dB over conventional detection methods. Diagrams, drawings, photographs, and graphs of typical performance data are included.

Pan, J. J.↗

The EGRET high energy gamma ray telescope

The Energetic Gamma Ray Experiment Telescope (EGRET) on the Compton Gamma Ray Observatory (GRO) is sensitive in the energy range from about 20 MeV to about 30,000 MeV. Electron-positron pair production by incident gamma photons is utilized as the detection mechanism. The pair production occurs in tantalum foils interleaved with the layers of a digital spark chamber system; the spark chamber records the tracks of the electron and positron, allowing the reconstruction of the arrival direction of the gamma ray. If there is no signal from the charged particle anticoincidence detector which surrounds the upper part of the detector, the spark chamber array is triggered by two hodoscopes of plastic scintillators. A time of flight requirement is included to reject events moving backward through the telescope. The energy of the gamma ray is primarily determined by absorption of the energies of the electron and positron in a 20 cm deep NaI(Tl) scintillator.

Hartman, R. C.↗

Forecasting the arrival of fast coronal mass ejecta at Earth by the detection of 2-20 keV neutral atoms

Studies have shown that Earth passages of fast coronal mass ejections (CMEs) trigger geomagnetic storms. Early identification of fast earth-directed CME can help provide storm warnings, but detection of such by coronagraphs is extremely difficult. We suggest that energetic hydrogen atoms (EHA) between 2 and 10 keV produced during the transit phase of an Earth-directed CME by recombination between protons and electrons in the CME can travel ahead of the CME and act as harbingers of a magnetic storm. This forecasting scheme should work if enough EHA are produced, because while CMEs decelerate continuously after their ejection, the EHA fluxes produced in the initial phase of fast CMEs propagate at their initial high speeds. Model simulations support this proposed mechanism.

Hsieh, K. C.↗

Auroral ionospheric signatures of the plasma sheet boundary layer in the evening sector

We report on particles and fields observed during Defense Meteorological Satellite Program (DMSP) F9 and DE 2 crossings of the polar cap/auroral oval boundary in the evening magnetic local time (MLT) sector. Season-dependent, latitudinally narrow regions of rapid, eastward plasma flows were encountered by DMSP near the poleward boundary of auroral electron precipitation. Ten DE 2 orbits exhibiting electric field spikes that drive these plasma flows were chosen for detailed analysis. The boundary region is characterized by pairs of oppositely-directed, field-aligned current sheets. The more poleward of the two current sheets is directed into the ionosphere. Within this downward current sheet, precipitating electrons either had average energies of a few hundred eV or were below polar rain flux levels. Near the transition to upward currents, DE 2 generally detected intense fluxes of accelerated electrons and weak fluxes of ions, both with average energies between 5 and 12 keV. In two instances, precipitating ions with energies greater than 5 keV spanned both current sheets. Comparisons with satellite measurements at higher altitudes suggest that the particles and fields originated in the magnetotail inside the distant reconnection region and propagated to Earth through the plasma sheet boundary layer. Auroral electrons are accelerated by parallel electric fields produced by the different pitch angle distributions of protons and electrons in this layer interacting with the near-Earth magnetic mirror. Electric field spikes driving rapid plasma flows along the poleward boundaries of intense, keV electron precipitation represent ionospheric responses to the field-aligned currents and conductivity gradients. The generation of field-aligned currents in the boundary layer may be understood qualitatively as resulting from the different rates of earthward drift for electrons and protons in the magnetotail's current sheet.

Burke, W. J.↗

Obtaining Real Production Data Through On-Component Printed SIR Patterns

Cleanliness validation of printed circuit assemblies has become increasingly important as electronic assemblies become smaller, denser, and more challenging to clean, prompting an increase in reliance in custom solutions. With increasingly fast paced development cycles, long lead times and costs of quality custom surrogate test boards become prohibitive in obtaining cleanliness data that is a true representative of the final product. In this study, aerosol jet printing, an additive manufacturing technology for electronics, was used to manufacture surface insulation resistance (SIR) test structures that were evaluated on their ability to detect cleanliness defects and remain stable when clean, as well as their survivability to standard electronics wash processes. Additionally, in an effort to further increase the agility of true product testing, SIR test structures were printed directly onto ball-grid-arrays (BGAs) and tested the survivability of conformally printed leads for data acquisition. SIR test structures displayed good wash survivability on standard FR4 and BGAs, including wraparounds for on-component prints, and high sensitivity to cleanliness defects. The presented results demonstrate the feasibility of printed SIR structures as a quick-turn, highly customizable solution for wash validation with potential for increased fidelity cleanliness testing.

SIR, Additive Manufacturing, Printed Electronics, ↗

Evaluation of Pulse Counting for the Mars Organic Mass Analyzer (MOMA) Ion Trap Detection Scheme

The Mars Organic Mass Analyzer is being developed at Goddard Space Flight Center to identify organics and possible biological compounds on Mars. In the process of characterizing mass spectrometer size, weight, and power consumption, the use of pulse counting was considered for ion detection. Pulse counting has advantages over analog-mode amplification of the electron multiplier signal. Some advantages are reduced size of electronic components, low power consumption, ability to remotely characterize detector performance, and avoidance of analog circuit noise. The use of pulse counting as a detection method with ion trap instruments is relatively rare. However, with the recent development of high performance electrical components, this detection method is quite suitable and can demonstrate significant advantages over analog methods. Methods A prototype quadrupole ion trap mass spectrometer with an internal electron ionization source was used as a test setup to develop and evaluate the pulse-counting method. The anode signal from the electron multiplier was preamplified. The an1plified signal was fed into a fast comparator for pulse-level discrimination. The output of the comparator was fed directly into a Xilinx FPGA development board. Verilog HDL software was written to bin the counts at user-selectable intervals. This system was able to count pulses at rates in the GHz range. The stored ion count nun1ber per bin was transferred to custom ion trap control software. Pulse-counting mass spectra were compared with mass spectra obtained using the standard analog-mode ion detection. Prelin1inary Data Preliminary mass spectra have been obtained for both analog mode and pulse-counting mode under several sets of instrument operating conditions. Comparison of the spectra revealed better peak shapes for pulse-counting mode. Noise levels are as good as, or better than, analog-mode detection noise levels. To artificially force ion pile-up conditions, the ion trap was overfilled and ions were ejected at very high scan rates. Pile-up of ions was not significant for the ion trap under investigation even though the ions are ejected in so-called 'ion-micro packets'. It was found that pulse counting mode had higher dynamic range than analog mode, and that the first amplification stage in analog mode can distort mass peaks. The inherent speed of the pulse counting method also proved to be beneficial to ion trap operation and ion ejection characterization. Very high scan rates were possible with pulse counting since the digital circuitry response time is so much smaller than with the analog method. Careful investigation of the pulse-counting data also allowed observation of the applied resonant ejection frequency during mass analysis. Ejection of ion micro packets could be clearly observed in the binned data. A second oscillation frequency, much lower than the secular frequency, was also observed. Such an effect was earlier attributed to the oscillation of the total plasma cloud in the ion trap. While the components used to implement pulse counting are quite advanced, due to their prevalence in consumer electronics, the cost of this detection system is no more than that of an analog mode system. Total pulse-counting detection system electronics cost is under $250

Van Amerom, Friso H.↗

Single electron in a storage ring: a probe into the fundamental properties of synchrotron radiation and a powerful diagnostic tool

An experimental study of undulator radiation generated by a single electron was carried out at the Integrable Optics Test Accelerator (IOTA) storage ring at Fermilab. Photons were detected with a single-photon avalanche diode (SPAD) at an average rate of 20 kHz, corresponding to one detection every few hundred revolutions. Events were continuously recorded by a picosecond event timer for as long as 5 minutes at a time. The collected data were used to directly test the predictions of classical Poisson photostatistics. The study was motivated in part by a previous observation of sub-Poissonian statistics in a similar experiment with synchrotron radiation. In addition, we show that the time series of recorded events can be used to study the synchrotron motion of a single electron, yielding dynamical parameters such as the phase jitter of the radiofrequency cavity and the dependence of the synchrotron period on amplitude. Research plans for further experiments are also discussed.

47 OTHER INSTRUMENTATION↗

Measurement of plasma temperature and density using radiation absorption

A light beam of predetermined wavelength, preferably monochromatic, is directed through a plasma to be measured. The absorption of the light by the plasma is detected for deriving an absorption coefficient of the plasma. Knowing the absorption coefficient of the plasma and independently measuring either the electron density or temperature of the plasma allows solution of an equation to derive the other unknown quantity, i.e. either electron density or temperature. In a preferred method, the absorption coefficient of the plasma is derived simultaneously for two probing light beams of substantially different predetermined wave-lengths. Knowing these two coefficients allows solution of two simultaneous equations to derive the electron density and temperature of the plasma.

Kenneth W Billman↗

Integrated Optoelectronic Interface

Proposed optoelectronic integrated-circuit device serves as "universal" or standard interface for transmission and reception of digital and analog signals in communication, data-processing, and control systems. Eliminates need for custom design of interface circuitry in sense that it embodies "master-chip" design easily adaptable to use with specific equipment. Includes directly modulated semiconductor laser to generate light signals for transmission along optical fiber; positive/intrinsic/negative, avalanche, or other photodiode to detect light signals received along another optical fiber;and driving, synchronizing, preamplifying, and signal-regenerating circuitry. Muliplexes electronic signals before transmission and/or demultiplexes electronic signals after reception.

Katz, Joseph↗

A New GaAs Laser Radar for Atmospheric Measurements

A special GaAs lidar using fiber coupled diode lasers was constructed for the purpose of measuring the extinction coefficient distribution within a large atmospheric volume at a rate compatible with atmospheric kinematics. The technique is based on taking backscatter signature ratios over spatial increments after the returns are normalized by pulse integration. Essential aspects of the lidar design are beam pulse power, repetition rate, detection system dynamic range and decay linearity. It was necessary to preclude the possibility of eye hazard under any operating conditions, including directly viewing the emitting aperture at close distance with a night-adapted eye. The electronic signal processing and control circuits were built to allow versatile operations. Extinction coefficient measurements were made in fog and clouds using a low-power laboratory version of the lidar, demonstrating feasibility. Data are presented showing range squared corrected backscatter profiles converted to extinction coefficient profiles, temporal signal fluctuations, and solar induced background noise. These results aided in the design of the lidar which is described. Functional tests of this lidar and the implications relevant to the design of a prototype model are discussed. This work was jointly sponsored by Sperry Rand Corporation under its Independent Research and Development program; the Air Force Avionics Laboratory, Wright Field, Dayton, Ohio; and the Naval Ammunition Depot, Crane, Indiana.

Brown, R. T.↗

Ultrasensitive Label-free Electronic Chip for DNA Analysis Using Carbon Nanotube Nanoelectrode Arrays

There is a strong need for faster, cheaper, and simpler methods for nucleic acid analysis in today s clinical tests. Nanotechnologies can potentially provide solutions to these requirements by integrating nanomaterials with biofunctionalities. Dramatic improvement in the sensitivity and multiplexing can be achieved through the high-degree miniaturization. Here, we present our study in the development of an ultrasensitive label-free electronic chip for DNA/RNA analysis based on carbon nanotube nanoelectrode arrays. A reliable nanoelectrode array based on vertically aligned multi-walled carbon nanotubes (MWNTs) embedded in a SiO2 matrix is fabricated using a bottom-up approach. Characteristic nanoelectrode behavior is observed with a low-density MWNT nanoelectrode array in measuring both the bulk and surface immobilized redox species. The open-end of MWNTs are found to present similar properties as graphite edge-plane electrodes, with a wide potential window, flexible chemical functionalities, and good biocompatibility. A BRCA1 related oligonucleotide probe with 18 bases is covalently functionalized at the open ends of the MWNTs and specifically hybridized with an oligonucleotide target as well as a PCR amplicon. The guanine bases in the target molecules are employed as the signal moieties for the electrochemical measurements. Ru(bpy)3(2+) mediator is used to further amplify the guanine oxidation signal. This technique has been employed for direct electrochemical detection of label-free PCR amplicon through specific hybridization with the BRCAl probe. The detection limit is estimated to be less than approximately 1000 DNA molecules, approaching the limit of the sensitivity by laser-based fluorescence techniques in DNA microarray. This system provides a general electronic platform for rapid molecular diagnostics in applications requiring ultrahigh sensitivity, high-degree of miniaturization, simple sample preparation, and low- cost operation.

Li, Jun↗

Billion-pixel x-ray camera (BiPC-X)

The continuing improvement in quantum efficiency (above 90% for single visible photons), reduction in noise (below 1 electron per pixel), and shrink in pixel pitch (less than 1 μm) enable billion-pixel x-ray cameras (BiPC-X) based on commercial complementary metal–oxide–semiconductor (CMOS) imaging sensors. We describe BiPC-X designs and prototype construction based on flexible tiling of commercial CMOS imaging sensors with millions of pixels. Device models are given for direct detection of low energy x rays (<10 keV) and indirect detection of higher energies using scintillators. Modified Birks’s law is proposed for light yield non-proportionality in scintillators as a function of x-ray energy. Single x-ray sensitivity and spatial resolution have been validated experimentally using a laboratory x-ray source and the Argonne Advanced Photon Source. Possible applications include wide field-of-view or large x-ray aperture measurements in high-temperature plasmas, the state-of-the-art synchrotron, x-ray free electron laser, and pulsed power facilities.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Report on Task USA A 0931 (A.252) Implementation of Fast, Front-End Electronics for Improved Low-Dead Time Neutron Counting

The International Atomic Energy Agency's (IAEA) Department of Safeguards is working on the elaboration and implementation of advanced Non-Destructive Assay (NDA) methods, generally known as neutron noise analysis, for the verification of critical and sub-critical cores containing substantial quantities of direct use nuclear material. These verification methods rely on interpreting time properties of the neutron multiplication process, which are to be extracted from measured neutron pulse trains. The interpretations are highly dependent on the quality of the measured data, which is directly related to the capability of an employed neutron detector to resolve very close detection events originating from neutron bursts produced in a highly multiplying medium. Therefore, the application of detectors with minimum dead-time, pile-up, and other distortion effects is required. This report describes the work under Task USA A 0931 (A.252 Implementation of fast, front-end electronics for improved low-dead time neutron counting).

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗