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At least 271 records · Page 15

All sources NASA NTRS DOE OSTI

DOE OSTI2021

ATOMIC Simulations and Experimental Data for CaCO3 Mixtures

This data consists of simulations and experimental measurements of laser-induced breakdown spectroscopy (LIBS). The simulations are produced by ATOMIC, a general purpose plasma modeling and kinetics code that has been designed to compute emission (or absorption) spectra from plasmas [1] and are used to develop a statistical characterization of matrix effects. Our overall suite of simulations includes contains several sets of simulations: training and validation sets of simulations for three and four element mixtures of calcium, carbon, oxygen, and nitrogen (included to account for atmosphere) along with simulations of the individual elements. The 4-element simulations include the mixture of all four elements mentioned and for each of the four individual elements. The 3-element simulations include output for the mixture of calcium, carbon, oxygen and for these three individual elements. The training data were produced using a 600-run design, shown in Figure 1, that varies input parameters temperature (T), electron density (Ne), and proportion of the elements calcium, carbon, oxygen, and nitrogen (Ca; C; O; N) for the 4 element output. The 3-element output includes all parameters except for the proportion of nitrogen. The element proportions (all the variables but T and Ne) sum to one and are unused in the single-element simulations. The validation data was produced with a 80-run design shown in Figure 2. The training and validation simulation outputs for the 4-element simulations for the mixture and for the single element calcium are shown as sample simulations in Figures 3 and 4 respectively. The simulations produce spectra over a range of 190nm - 950nm that roughly mimics the range collected by the SciAps Z-300 LIBS instrument that was used for the experimental data. The measured spectra for a CaCO3 (which may include contribution from Earth's atmosphere) in the experiment is shown in in Figure 5. All files are kept in directories whose names indicate the elemental composition (CaCO3, Ca, C, O, or N), number of elements (3 or 4), and purpose (training, which is not labeled in the file name, or validation) with file names numbered to indicate the line in the design files used to produce the simulation. The designs are provided as text files with names indicating their purpose. The experimental data is provided as a CSV file. [1] J Colgan, EJ Judge, DP Kilcrease, and JE Barefield II. Ab-initio modeling of an iron laser-induced plasma: Comparison between theoretical and experimental atomic emission spectra. Spectrochimica Acta Part B: Atomic Spectroscopy, 97:65{73}, 2014.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

DOE OSTI2023

SPRUCE Peat Mercury, Methylmercury and Sulfur Concentrations from Experimental Plot Cores, 2012

This data set reports the results of analyses of peat core samples for total mercury and methylmercury, as well as carbon, nitrogen and sulfur. Samples were collected as part of a larger sampling campaign from the SPRUCE experimental study plots located in the S1-Bog. From 2012-08-13 to 2012-10-15, a team of SPRUCE investigators and collaborators collected core samples of peat in the SPRUCE experimental plots. The goal was to characterize the biological, physical, and chemical characteristics of peat, and how those characteristics changed throughout the depth profile of the bog, prior to the initialization of the SPRUCE experimental warming and CO2 treatments. Cores were collected from 16 experimental plots; peat cores were collected from the hummock and hollow surfaces to depths of 300 cm in 10 cm, 25, and 50 cm increments (Pierce et al, 2022). Three replicate cores were collected from both hummock and hollow locations in each plot. The coring locations within each plot were mapped. This dataset contains one file in comma separated (*.csv) format. User Note: The coring descriptions and some reported data are the same as in the related data set, Iverson et al. (2014). Samples for mercury and carbon, nitrogen and sulfur analyses by the University of Minnesota were collected as part of this sampling campaign.

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2021

Experimental Study of the Behavior of Phase Change Materials during Interrupted Phase Change Processes

This research article explores the behavior of a phase change material (PCM) when it undergoes interrupted melting and freezing, through experimental investigations using a heat flow meter apparatus. A fatty acid-based organic PCM, encapsulated within polyethylene and thin aluminum foil layers, was experimentally tested in this study. Experiments were designed to represent multiple interrupted phase change scenarios that could occur within PCMs applied in buildings. The experimental results were analyzed and compared with previously reported assumptions in numerical models dealing with PCM hysteresis and interrupted phase change processes. These comparisons indicated that the assumptions used in the different numerical models considered can capture the interrupted phase change phenomena with varying degrees of accuracy. The findings also highlighted the need for additional experimental research on different phase change processes that can occur in building applications of PCMs.

36 MATERIALS SCIENCE↗

DOE OSTI2023

A Novel Experimental Approach to Understand the Transport of Nanodrugs

Nanoparticle-based drugs offer attractive advantages like targeted delivery to the diseased site and size and shape-controlled properties. Therefore, understanding the particulate flow of the nanodrugs is important for effective delivery, accurate prediction of required dosage, and developing efficient drug delivery platforms for nanodrugs. In this study, the transport of nanodrugs including flow velocity and deposition is investigated using three model metal oxide nanodrugs of different sizes including iron oxide, zinc oxide, and combined Cu-Zn-Fe oxide synthesized via a modified polyol approach. The hydrodynamic size, size, morphology, chemical composition, crystal phase, and surface functional groups of the water-soluble nanodrugs were characterized via dynamic light scattering, transmission electron microscopy, scanning electron microscopy-energy dispersive X-ray, X-ray diffraction, and fourier transform infrared spectroscopy, respectively. Two different biomimetic flow channels with customized surfaces are developed via 3D printing to experimentally monitor the velocity and deposition of the different nanodrugs. A diffusion dominated mechanism of flow is seen in size ranges 92 nm to 110 nm of the nanodrugs, from the experimental velocity and mass loss profiles. The flow velocity analysis also shows that the transport of nanodrugs is controlled by sedimentation processes in the larger size ranges of 110–302 nm. However, the combined overview from experimental mass loss and velocity trends indicates presence of both diffusive and sedimentation forces in the 110–302 nm size ranges. It is also discovered that the nanodrugs with higher positive surface charges are transported faster through the two test channels, which also leads to lower deposition of these nanodrugs on the walls of the flow channels. The results from this study will be valuable in realizing reliable and cost-effective in vitro experimental approaches that can support in vivo methods to predict the flow of new nanodrugs.

36 MATERIALS SCIENCE↗

DOE OSTI2023

Experimental Guesswork with Quantum Side Information Using Twisted Light

Guesswork is an information–theoretic quantity which can be seen as an alternate security criterion to entropy. Recent work has established the theoretical framework for guesswork in the presence of quantum side information, which we extend both theoretically and experimentally. We consider guesswork when the side information consists of the BB84 states and their higher-dimensional generalizations. With this side information, we compute the guesswork for two different scenarios for each dimension. We then performed a proof-of-principle experiment using Laguerre–Gauss modes to experimentally compute the guesswork for higher-dimensional generalizations of the BB84 states. We find that our experimental results agree closely with our theoretical predictions. This work shows that guesswork can be a viable security criterion in cryptographic tasks and is experimentally accessible in a number of optical setups.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗

DOE OSTI2024

Experimental Study of Alfvén Wave Reflection from an Alfvén-speed Gradient Relevant to the Solar Coronal Holes

Abstract We report the first experimental detection of a reflected Alfvén wave from an Alfvén-speed gradient under conditions similar to those in coronal holes. The experiments were conducted in the Large Plasma Device at the University of California, Los Angeles. We present the experimentally measured dependence of the coefficient of reflection versus the wave inhomogeneity parameter, i.e., the ratio of the wavelength of the incident wave to the length scale of the gradient. Two-fluid simulations using the Gkeyll code qualitatively agree with and support the experimental findings. Our experimental results support models of wave heating that rely on wave reflection at low heights from a smooth Alfvén-speed gradient to drive turbulence.

79 ASTRONOMY AND ASTROPHYSICS↗

DOE OSTI2021

Evaluation of Experimental and Predicted Vapor-Liquid Equilibrium Data for Systems Relevant to Biomass Fast Pyrolysis and Catalytic Upgrading

The experimental vapor-liquid equilibrium (VLE) data for the binaries relevant to the catalytic fast pyrolysis of biomass have been collected and analyzed using the NIST-COSMO-SAC and NIST-modified UNIFAC models. The existing inconsistencies in the experimental data and the predicted values are discussed. For VLE with furan derivatives, PTxy data are normally reported, and the predicted values are in good agreement with them. For phenolic compounds, the gas phase compositions are available for only 36 % of the points, most results originate from a few laboratories, and each system has been typically studied in a single laboratory. The binaries are identified where more experimental VLE data are required to evaluate quality of the existing experimental and predicted results.

09 BIOMASS FUELS↗

NASA NTRS1972

Criteria for the optimal design of experimental tests

Some of the basic concepts are unified that were developed for the problem of finding optimal approximating functions which relate a set of controlled variables to a measurable response. The techniques have the potential for reducing the amount of testing required in experimental investigations. Specifically, two low-order polynomial models are considered as approximations to unknown functionships. For each model, optimal means of designing experimental tests are presented which, for a modest number of measurements, yield prediction equations that minimize the error of an estimated response anywhere inside a selected region of experimentation. Moreover, examples are provided for both models to illustrate their use. Finally, an analysis of a second-order prediction equation is given to illustrate ways of determining maximum or minimum responses inside the experimentation region.

Canavos, G. C.↗

NASA NTRS1972

An experimental and theoretical investigation of the liquefaction dynamics of a phase change material in a normal gravity environment

Experimental and theoretical investigations were undertaken to determine the role of gravity-induced free convection upon the liquefaction dynamics of a cylindrical paraffin slab under normal gravity conditions. The experimental equipment consisted of a test cell, a fluid-loop heating system, and a multipoint recorder. The test chamber was annular in shape with an effective radius of 1.585 cm and a length of 5.08 cm. The heating chamber was a 1.906 cm diameter tube going through the center of the test chamber, and connected to the fluid loop heating system. All experimental runs were made with the longitudinal axis of the test cell in the vertical direction to insure that convection was not a function of the angular axis of the cell. Ten melting runs were made at various hot wall temperatures. Also, two pure conduction solidification runs were made to determine an experimental latent heat of fusion.

Bain, R. L.↗

NASA NTRS1973

Some effects of experimental error in fracture testing

Effects of experimental imprecision on the stress intensity factors calculated for various practical specimen types are shown. A general form equation for the stress intensity factor is presented and a general error equation is derived. The expected error in the stress intensity factor is given in terms of the precision levels of the basic experimental measurements and derivatives of the stress intensity calibration factor. Nine common fracture specimen types are considered, and the sensitivity of the various types to experimental error is illustrated. Some implications for fracture toughness testing and crack growth rate testing are discussed and methods of analysis are proposed to compensate for the effects of experimental error.

Orange, T. W.↗

NASA NTRS1973

Experimental study of the dynamics of a spherical flame

Preliminary results of an experimental study conducted to investigate the dynamic behavior of flames in explosive gases are presented. The medium was an equimolar acetylene-oxygen mixture maintained initially at a pressure of 110 torr. and room temperature in an experimental vessel 9 cm in internal diameter. Ignition was performed by means of a neodymium laser beam focused on a 0.3 mm diameter steel wire. Experimental observations were performed by the use of a stroboscopic laser-schlieren system yielding a set of photographic records of wave phenomena at a frequency of 200,000 per second. The records reveal the existence of a number of shocks which by a thorough analysis of the blast wave generated by the ignition process, are shown to be due entirely to the flame generated flow field. The capability of a flame to form blast waves in an expanding spherical geometry is thus established, providing an experimental demonstration of the significance the dynamic effects of combustion can achieve.

Oppenheim, A. K.↗

NASA NTRS1973

Some effects of experimental error in fracture testing.

The purpose of this paper is to show the effects of experimental imprecision on the stress intensity factors calculated for various practical specimen types. A general form equation for the stress intensity factor is presented, and a general error equation is derived. The expected error in the stress intensity factor is given in terms of the precision levels of the basic experimental measurements and derivatives of the stress intensity calibration factor. Nine common fracture specimen types are considered, and the sensitivity of the various types to experimental error is illustrated. Some implications for fracture toughness testing and crack growth rate testing are discussed, and methods of analysis are proposed to compensate for the effects of experimental error.

Orange, T. W.↗

NASA NTRS1973

Experimental research on aerostatic suspensions

Suspensions for carrying out experimental investigations, for the purpose of studying a number of problems in dynamics and stability of a suspended cylindrical body at various dynamic loads were investigated in the work. The results of the experimental investigations served as a basis for building a stand with a variable resonator. The experimental stand for suspension of cylindrical object, with a comparatively high natural free vibration frequency in the vertical direction, coinciding with the axis of the suspended object, is distinguished by the possibility of regulating the size of the clearance and is intended for carrying out preliminary experimental studies, for the purpose of selection of optimum aerostatic suspension parameters.

Bushma, L. A.↗

NASA NTRS1975

Comparison of experimental and theoretical boundary-layer separation for inlets at incidence angle at low-speed conditions

Comparisons between experimental and theoretical Mach number distributions and separation locations are presented for the internal surfaces of four different subsonic inlet geometries with exit diameters of 13.97 centimeters. The free stream Mach number was held constant at 0.127, the one-dimensional throat Mach number ranged from 0.49 to 0.71, and the incidence angle ranged from 0 deg to 50 deg. Generally good agreement was found between the theoretical and experimental surface Mach number distributions as long as no flow separation existed. At high incidence angles, where separation was obvious in the experimental data, the theory predicted separation on the lip. At lower incidence angles, the theoretical results indicated diffuser separation which was not obvious from the experimental surface Mach number distributions. As incidence angle was varied from 0 deg to 50 deg, the predicted separation location shifted from the diffuser region to the inlet highlight. Relatively small total pressure losses were obtained when the predicted separation location was greater than 0.6 of the distance between the highlight and the diffuser exit.

Felderman, E. J.↗

NASA NTRS1974

Combustion modeling for experimentation in a space environment

The merits of combustion experimentation in a space environment are assessed, and the impact of such experimentation on current theoretical models is considered. It is noted that combustion theory and experimentation for less than normal gravitational conditions are incomplete, inadequate, or nonexistent. Extensive and systematic experimentation in a space environment is viewed as essential for more adequate and complete theoretical models of such processes as premixed flame propagation and extinction limits, premixed flame propagation in droplet and particle clouds, ignition and autoignition in premixed combustible media, and gas jet combustion of unpremixed reactants. Current theories and models in these areas are described, and some combustion studies that can be undertaken in the Space Shuttle Program are proposed, including crossed molecular beam, turbulence, and upper pressure limit (of gases) studies.

Berlad, A. L.↗

NASA NTRS1975

Experimental and Theoretical Studies of Pulsating Turbulent Flow

The objective of this investigation was to study the effects of small amplitude sinusoidal pulsations on fully developed turbulent flow in a tube from both experimental and theoretical viewpoints. Theoretical models for the macroscopic behavior of pulsating turbulent tube flow were developed for the two cases of very low and very high pulsation frequencies. The models are based on assumptions of quasi-steady and frozen eddy viscosity flow behavior, respectively. The models successfully predict unsteady velocity profiles, thereby supporting the currently proposed definitions of frequency regimes in pulsating turbulent flow. Experimental measurements were made of the time-dependent pressure drop and velocity profiles over the range of frequency-to-Reynolds number ratios from 0.0095 to 0.24. The two macroscopic models developed in this study predict unsteady velocity profiles which are in moderately good agreement with the experiments in their respective frequency regimes, and a previously developed quasi-steady model is found to predict experimental velocity profiles well in both the quasisteady and the frozen eddy viscosity frequency regimes. The effect of flow pulsations on the dissipation of turbulence energy in the vicinity of the wall was measured in the lower transition frequency regime. The long-time averaged dissipation was observed to be unchanged from the steady flow dissipation, within the accuracy of the experiment. A theoretical model of the periodic viscous sublayer was also developed and applied to pulsating flow in a tube, in order to investigate the effects of flow pulsations on the rate of production of turbulence in the region of the wall. The periodic viscous sublayer model predicts sublayer growth periods in steady flow which agree with the published experimental data. When the model is applied to pulsating flow, the response of the sublayer growth period falls into three frequency regimes, the parameters of which are in approximate agreement with the frequency regimes which are defined on the basis of macroscopic flow behavior. The sublayer renewal cycle exhibits quasi-steady flow behavior when the sublayer growth period is much less than the pulsation period, transition behavior when these two periods are approximately equal, and frozen eddy viscosity behavior when the sublayer period is much longer than the pulsation period. The effect of the sublayer growth and renewal cycle on the level of turbulence was investigated by two methods. The velocity fluctuations seen by a point velocity probe located close to the wall were predicted from the model in one method and the rate of turbulence production was estimated from the frequency of sublayer renewal events in the other.

Kingston, G. C.↗

NASA NTRS1975

STOL aircraft transient ground effects. Part 2: Experimental techniques feasibility study

Procedures for simulating transient effects associated with STOL aircraft landings and takeoffs were examined and a basis was developed for selection of an experimental approach based on consideration of simulation requirements, experimental techniques, facilities, and costs. The results are generally applicable to STOL aircraft employing any of the following powered lift systems: externally blown flap, upper surface blown flap, augmentor wing, or internally ducted jet flap. Scaling relationships were developed to apply the simulation requirements to model test situations. Procedures for the derivation of aerodynamic forces from the measured data were discussed. Various means of expressing the aerodynamic data in forms convenient for use in performance or stability and control applications were described. Five different experimental techniques were presented that depend on two different types of experimental facilities, wind tunnels and test tracks, and involving different types of model motion, and factors pertinent to selection were summarized.

Crowder, J. P.↗

NASA NTRS1976

Assessment of analytical and experimental techniques utilized in conducting plume technology tests 575 and 593

Since exhaust plumes affect vehicle base environment (pressure and heat loads) and the orbiter vehicle aerodynamic control surface effectiveness, an intensive program involving detailed analytical and experimental investigations of the exhaust plume/vehicle interaction was undertaken as a pertinent part of the overall space shuttle development program. The program, called the Plume Technology program, has as its objective the determination of the criteria for simulating rocket engine (in particular, space shuttle propulsion system) plume-induced aerodynamic effects in a wind tunnel environment. The comprehensive experimental program was conducted using test facilities at NASA's Marshall Space Flight Center and Ames Research Center. A post-test examination of some of the experimental results obtained from NASA-MSFC's 14 x 14-inch trisonic wind tunnel is presented. A description is given of the test facility, simulant gas supply system, nozzle hardware, test procedure and test matrix. Analysis of exhaust plume flow fields and comparison of analytical and experimental exhaust plume data are presented.

Baker, L. R.↗