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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 271 records · Page 15

Study of acoustic emission during mechanical tests of large flight weight tank structure

A polyphenylane oxide insulated, flight weight, subscale, aluminum tank was monitored for acoustic emissions during a proof test and during 100 cycles of environmental test simulating space flights. The use of a combination of frequency filtering and appropriate spatial filtering to reduce background noise was found to be sufficient to detect acoustic emission signals of relatively small intensity expected from subcritical crack growth in the structure. Several emission source locations were identified, including the one where a flaw was detected by post-test X-ray inspections. For most source locations, however, post-test inspections did not detect flaws; this was partially attributed to the higher sensitivity of the acoustic emission technique than any other currently available NDT method for detecting flaws.

Nakamura, Y.↗

Holographic nondestructive testing with impact excitation.

Review of some experimental results of bond flaw detection in composite materials by holographic recording of the surface of samples subjected to mechanical impact. The resulting deformation of the samples recorded in a sequence of double exposure holograms at increasingly longer time intervals after impact renders the presence of flaws observable. A proposed deformation enhancement technique increases detection sensitivity and is helpful in visualizing smaller flaws.

Chu, W. P.↗

Study of acoustic emission during mechanical tests of large flight weight tank structure

A PPO-insulated, flight-weight, subscale, aluminum tank was monitored for acoustic emissions during a proof test and during 100 cycles of environmental test simulating space flights. The use of a combination of frequency filtering and appropriate spatial filtering to reduce background noise was found to be sufficient to detect acoustic emission signals of relatively small intensity expected from subcritical crack growth in the structure. Several emission source locations were identified, including the one where a flaw was detected by post-test x-ray inspections. For most source locations, however, post-test inspections did not detect flaws; this was partially attributed to the higher sensitivity of the acoustic emission technique than any other currently available NDT method for detecting flaws. For these non-verifiable emission sources, a problem still remains in correctly interpreting observed emission signals.

Mccauley, B. O.↗

Electromagnetic radiation screening of microcircuits for long life applications

The utility of X-rays as a stimulus for screening high reliability semiconductor microcircuits was studied. The theory of the interaction of X-rays with semiconductor materials and devices was considered. Experimental measurements of photovoltages, photocurrents, and effects on specified parameters were made on discrete devices and on microcircuits. The test specimens included discrete devices with certain types of identified flaws and symptoms of flaws, and microcircuits exhibiting deviant electrical behavior. With a necessarily limited sample of test specimens, no useful correlation could be found between the X-ray-induced electrical response and the known or suspected presence of flaws.

Brammer, W. G.↗

Reliability after inspection

The investigation is concerned with the derivation of relationships between the probability of having manufacturing defects, the probability of detecting a flaw, and the final reliability. Equations for the simple situation in which only one flaw can be present are used to introduce the relationships in a Bayes' theorem approach to the assessment of the final reliability. Situations which are prevalent in composites manufacturing are considered. Attention is given to a case involving the random occurrence of flaws on a laminate surface.

Davidson, J. R.↗

A study to improve the mechanical properties of silicon carbide ribbon fibers

Preliminary deposition studies of SiC ribbon on a carbon ribbon substrate showed that the dominant strength limiting flaws were at the substrate surface. Procedures for making the carbon ribbon substrate from polyimide film were improved, providing lengths up to 450 meters (1,500 ft.) of flat carbon ribbon substrate 1,900 microns (75 mils) wide by 25 microns (1 mil) thick. The flaws on the carbon ribbon were smaller and less frequent than on carbon ribbon used earlier. SiC ribbon made using the improved substrate, including a layer of pyrolytic graphite to reduce further the severity of substrate surface flaws, showed strength levels up to the 2,068 MPa (300 Ksi) target of the program, with average strength levels over 1,700 MPa (250 Ksi) with coefficient of variation as low as 10% for some runs.

Debolt, H. E.↗

Fracture mechanics correlation of boron/aluminum coupons containing stress risers

The mechanical behavior of boron/aluminum near stress risers has been studied and reported. This effort was directed toward defining the tensile behavior of both unidirectional and (0/ plus or minus 45) boron/aluminum using linear elastic fracture mechanics (LEFM). The material used was 5.6-mil boron in 6061 aluminum, consolidated using conventional diffusion bonding techniques. Mechanical properties are reported for both unidirectional and (0/ plus or minus 45) boron/aluminum, which serve as control data for the fracture mechanics predictions. Three different flawed specimen types were studied. In each case the series of specimens remained geometrically similar to eliminate variations in finite size correction factors. The fracture data from these tests were reduced using two techniques. They both used conventional LEFM methods, but the existence of a characteristic flaw was assumed in one case and not the other. Both the data and the physical behavior of the specimens support the characteristic flaw hypothesis. Cracks were observed growing slowly in the (0/ plus or minus 45) laminates, until a critical crack length was reached at which time catastrophic failure occurred.

Adsit, N. R.↗

Surface finish effects and the strength-grain size relation in SiC

The effect of surface finish on the strength-grain size relation was investigated for dense hot-pressed SiC. Failure initiated predominantly via the propagation of extrinsic machining-induced flaws for the range of grain sizes and machining grit sizes studied. These results are consistent with the region of large-grain-size flaw control as delineated by Prochazka and Charles. The severity of machining-induced flaws, relative to the machining grit size, decreased with increasing machining grit size and decreasing SiC grain size.

Cranmer, D. C.↗

Flight inspection data and crack initiation times

Lockheed C-130 service-flight inspection data is reduced by means of fracture mechanics and statistical analysis into a form from which the probability of time to crack initiation and the distribution of initial flaw sizes for various locations on the aircraft can be determined. Crack sizes are normalized by extrapolating a growing crack backwards from its first recorded size to .03 inches (crack initiation size) yielding the time to crack initiation. In a similar fashion, the crack is grown backwards to a time equal to zero to yield an initial flaw size. In order to perform the discussed computations, crack growth constants were computed for each individual location and were analyzed statistically. Statistical distributions were fitted to times to crack initiation and to initial flaw sizes in order to describe their expected behavior. Weibull and Johnson distributions have been found to fit the data reasonably well but for a better fit convolution integrals of Poisson load distributions and Weibull strength distributions are needed.

Johnson, W. S.↗

Delayed fracture of silicon: Silicon sheet growth development for the large area silicon sheet task of the low cost silicon solar array project

Bar specimens were cut from ingots of single crystal silicon, and acid etched prior to testing. Artificial surface flaws were introduced in specimens by indentation with a Knoop hardness tester. The specimens were loaded in four-point bending to 95 percent of the nominal fracture stress, while keeping the surface area, containing the flaw, wet with test liquids. No evidence of delayed fracture, and, therefore stress corrosion, of single crystal silicon was observed for liquid environments including water, acetone, and aqueous solutions of NaCl, NH4OH, and HNO3, when tested with a flaw parallel to a (110) surface. The fracture toughness was calculated.

Chen, T. J.↗

Preliminary development of a fundamental analysis model for crack growth in a fiber reinforced composite material

A mathematical model for the strength of fiber reinforced composites containing specific flaws is described. The approach is to embed a local heterogeneous region surrounding the crack tip in an anisotropic elastic continuum. By consideration of the individual failure events activated near the flaw tip, a strength prediction can be made from basic properties of the composite constituents. Computations for arbitrary flaw size and orientation have been performed for unidirectional composites with linear elastic-brittle constituent behavior. The mechanical properties were those of graphite epoxy. With the rupture properties arbitrarily varied to test the capability of the model to reflect real fracture modes in fiber composites, it is shown that fiber breakage, matrix crazing, crack bridging, matrix-fiber debonding, and axial splitting all can occur during gradually increasing load prior to catastrophic fracture. Qualitative comparisons with experimental results on edge-notched unidirectional graphite epoxy specimens have also been made.

Kanninen, M. F.↗

Some fundamental aspects of the fatigue and fracture response of composite materials

A simple analytical model, based on the concept that the constraining plies surrounding cracks through the thickness of a given ply or plies control the spacing of those cracks by controlling the surrounding stress state, appears to agree well with experimental data. Such a model can be used to evaluate critically various constraint situations including the prediction of the ability of a given constraint layer to arrest flaw development. The analytical model, which uses an equilibrium element approach in the present case, is sensitive to lamina and laminate elastic properties, flaw size, stacking sequence, and an interlaminar stress transfer distance which is estimated from experimental observations. The analysis is easily extended to study flaw growth and plastic region formation.

Reifsnider, K. L.↗

Influence of quality control variables on failure of graphite/epoxy under extreme moisture conditions

Tension tests on graphite/epoxy composites were performed to determine the influence of various quality control variables on failure strength as a function of moisture and moderate temperatures. The extremely high and low moisture contents investigated were found to have less effect upon properties than did temperature or the quality control variables of specimen flaws and prepreg batch to batch variations. In particular, specimen flaws were found to drastically reduce the predicted strength of the composite, whereas specimens from different batches of prepreg displayed differences in strength as a function of temperature and extreme moisture exposure. The findings illustrate the need for careful specimen preparation, studies of flaw sensitivity, and careful quality control in any study of composite materials.

Clements, L. L.↗

Pulsed eddy current testing

Since a large number of the procedures used for inspecting the external tank are concerned with determining flaws in welds, there is a need to develop an inspection technique, which can be automated, to determine flaws in welds and structures with complex geometries. Techniques whereby an eddy current is generated in a metallic material and the changes in the circuit parameters due to material differences are observed, were chosen as one possible approach. Pulsed eddy current and its relationship to multifrequency techniques is discussed as well as some preliminary results obtained from observing pulsed waveforms with apparatus and algorithms currently in use for ultrasonic testing of welds. It can be shown the pulsed eddy current techniques can provide similar results, can eliminate some of the noncritical parameters affecting the eddy current signals, and can facilitate in the detection of critical parameter such as flaws, subsurface voids, and corrosion.

Workman, G. L.↗

Investigating reliability attributes of silicon photovoltaic cells - An overview

Reliability attributes are being developed on a wide variety of advanced single-crystal silicon solar cells. Two separate investigations: cell-contact integrity (metal-to-silicon adherence), and cracked cells identified with fracture-strength-reducing flaws are discussed. In the cell-contact-integrity investigation, analysis of contact pull-strength data shows that cell types made with different metallization technologies, i.e., vacuum, plated, screen-printed and soldered, have appreciably different reliability attributes. In the second investigation, fracture strength was measured using Czochralski wafers and cells taken at various stages of processing and differences were noted. Fracture strength, which is believed to be governed by flaws introduced during wafer sawing, was observed to improve (increase) after chemical polishing and other process steps that tend to remove surface and edge flaws.

Royal, E. L.↗

Influence of quality control variables on failure of graphite/epoxy under extreme moisture conditions

Tension tests on graphite/epoxy composites were performed to determine the influence of various quality control variables on failure strength as a function of moisture and moderate temperatures. The extremely high and low moisture contents investigated were found to have less effect upon properties than did temperature or the quality control variables of specimen flaws and prepreg batch to batch variations. In particular, specimen flaws were found to drastically reduce the predicted strength of the composite, whereas specimens from different batches of prepreg displayed differences in strength as a function of temperature and extreme moisture exposure. The findings illustrate the need for careful specimen preparation, studies of flaw sensitvity, and careful quality control in any study of composite materials. Previously announced in STAR as N80-33493

Clements, L. L.↗

Assessing the Reliability of NDE

Versatile FORTRAN computer algorithm developed for calculating and plotting reliability of nondestructive evaluation (NDE) technique for inspection of flaws. Developed specifically to determine reliability of radiographic and ultrasonic methods for detection of critical flaws in structural ceramic materials. Reliability displayed in form of plot of probability of detection versus flaw size. NDE methods used in such applications as diagnostic medicine, quality control in industrial production, and prediction of failure in structural components.

Roth, Don J.↗

Nondestructive evaluation by acousto-ultrasonics

Acousto-ultrasonics is an ultrasonic technique that was originally devised to cope with the particular problems associated with nondestructive evaluation (NDE) of fiber/polymer composite structures. The fiber/polymer composites are more attenuating to ultrasound than any other material presently of interest. This limits the applicability of high-frequency ultrasonics. A common use of ultrasound is the imaging of flaws internal to a structure by scattering from the interface with the flaw. However, structural features of composites can scatter ultrasound internally, thus obscuring the flaws. A need relative to composites is to be able to nondestructively measure the strength of laminar boundaries in order to assess the integrity of a structure. Acousto-ultrasonics has exhibited the ability to use the internal scattering to provide information for determining the strength of laminar boundaries. Analysis of acousto-ultrasonic signals by the wave ray paths that compose it leads to waveform partitioning that enhances the sensitivity to mechanical strength parameters.

Kautz, Harold E.↗