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All sourcesNASA NTRSDOE OSTI
NASA NTRS2000

Structures and Materials Experimental Facilities and Capabilities Catalog

The NASA Center of Excellent for Structures and Materials at Langley Research Center is responsible for conducting research and developing useable technology in the areas of advanced materials and processing technologies, durability, damage tolerance, structural concepts, advanced sensors, intelligent systems, aircraft ground operations, reliability, prediction tools, performance validation, aeroelastic response, and structural dynamics behavior for aerospace vehicles. Supporting the research activities is a complementary set of facilities and capabilities documented in this report. Because of the volume of information, the information collected was restricted in most cases to one page. Specific questions from potential customers or partners should be directed to the points of contacts provided with the various capabilities. Grouping of the equipment is by location as opposed to function. Geographical information of the various buildings housing the equipment is also provided. Since this is the first time that such an inventory is ever collected at Langley it is by no means complete. It is estimated that over 90 percent of the equipment capabilities at hand are included but equipment is continuously being updated and will be reported in the future.

Horta, Lucas G.↗
DOE OSTI2012

Nanostructured Materials for High Efficiency Low Cost Solution-Processed Photovoltaics

The goal of the project was to develop a suite of materials coupled with processing technologies aimed at the fabrication of entirely solution-processed photovoltaic devices. Most of the emphasis in terms of innovation was placed on the transparent electrodes, widely considered a critical component of the solar cell in terms of cost and performance. The active layer technologies proposed hinged on the fabrication and deposition of semiconducting nanoparticles. The electrode development hit all the milestones proposed: by the end of the grant we were able to fabricate transparent and flexible electrodes with transmission over the solar spectrum higher than 85% and sheet resistance lower than 10 Ω/square. To the best of our knowledge, this is the highest-performance transparent electrode reported. Furthermore these electrodes were deposited by spray-coating, a large-area, low-cost deposition techniques. Hence the first main goal of the proposal, which was to find an alternative to ITO was successfully achieved. Organic photovoltaic devices were made with these electrodes having a performance indistinguishable from that of devices made on ITO (the industry standard), e.g. ~5% for P3HT:PCBM cells. We also innovated in the active-area part of the device where semiconducting inks were designed rather than nanoparticle suspensions. The process we selected, called air-stable ink rolling (AIR) allowed to deposit well-controlled films of ternary and quaternary II-VI semiconductors. Developing a new technology from scratch proved to be more challenging than anticipated and therefore we were not able to demonstrate a fully integrated device using our nanostructured high-performance transparent electrodes as well as AIR active layers. As a result, we did not achieve the second main goal of the proposal, which was to fabricate an entire cell using nanostructured materials. We were able to develop the components separately but did not integrate them in a device.

14 SOLAR ENERGY↗
NASA NTRS2001

Proceedings of the 4th Conference on Aerospace Materials, Processes, and Environmental Technology

The next millennium challenges us to produce innovative materials, processes, manufacturing, and environmental technologies that meet low-cost aerospace transportation needs while maintaining US leadership. The pursuit of advanced aerospace materials, manufacturing processes, and environmental technologies supports the development of safer, operational, next-generation, reusable, and expendable aeronautical and space vehicle systems. The Aerospace Materials, Processes, and Environmental Technology Conference (AMPET) provided a forum for manufacturing, environmental, materials, and processes engineers, scientists, and managers to describe, review, and critically assess advances in these key technology areas.

Griffin, D. E.↗
DOE OSTI2018

Fundamental catalytic challenges to design improved biomass conversion technologies

During the past ten years, there has been significant interest and investment in the study of catalytic conversion of biomass-derived feedstocks into renewable fuels and chemicals. In the United States, an estimated $25 billion has been spent by venture capitalists, industry, and government agencies during this period of time to commercialize “renewable technologies” including solar energy, wind power, batteries, and biofuels (e.g., cellulosic ethanol). Four societal factors are driving these investments including: (1) the increased price of crude oil; (2) concerns about global warming; (3) the desire to improve rural economies where biomass is produced, and; (4) national goals to become energy self-sufficient. Furthermore, underlying these efforts is the realization that lignocellulosic biomass is the only realistic, near-term and non-food-competitive source of renewable organic carbon. To this end, legislative efforts, such as the US Renewable Fuel Standards, have been implemented to create subsidies, tax credits, mandates, and loan guarantees to help bring renewable fuel technologies to market. However, the representative body of industrial efforts to this end has faced significant challenges, with several startup companies having commercialized biomass conversion technologies but having struggled to reach commercial scale; in fact, many of these companies have filed for bankruptcy. This situation is likely due to the challenges associated with scaling up unproven pioneer processes, as well as neophyte investors not understanding the decade-long time frames and the sheer amount of funding that is often required to bring chemical process technologies to market. Nevertheless, several emerging catalytic technologies have either entered the market place, or are currently demonstrating their technologies in fully integrated pilot plants. Commercial and near commercial technologies for second generation biomass conversion technologies to-date include, among others: biomass-derived jet and diesel fuel from both waste vegetable oils and ethanol; small scale production of renewable jet and diesel from landfill gases via Fischer-Tropsch synthesis; catalytic conversion of carbohydrates into gasoline and aromatics; hydropyrolysis of biomass into gasoline and diesel, and; catalytic conversion of wood into aromatics. To be successful, biomass conversion technologies must ultimately be able to compete economically with petroleum technologies, which are already operating at large commercial scales and have been practiced for decades. To this end, various factors must be considered when evaluating the potential for new processes to compete with incumbent technologies; factors such as regional variations in feedstock quality and availability, government policy, subsidies and tax rates, and the proprietary positions of the ancillary technologies that might support the process. By any measure, however, a critical metric of the economic potential of a process is its efficiency with respect to the yield of products from raw materials, and this metric of performance is directly related to atom efficiency of the underlying chemical reactions. Therefore, while promising biomass conversion technologies continue to demonstrate progress towards commercialization, there remains an important need for the catalysis community to aid in this effort by: (1) designing more active, selective and stable catalysts, and (2) elucidating a more detailed understanding of the catalytic chemistries underlying these processes. Indeed, the study of catalytic biomass conversion has grown tremendously during the past decade; and new or emerging technologies that are in the laboratory stage have allowed for biomass to be converted into a wider variety of commodity chemicals and the full range of liquid fuels that are produced from petroleum. The objective of this perspective is to highlight some of the ongoing, fundamental challenges with respect to the catalytic conversion of biomass into renewable products, and to provide insight as to how the catalysis community can overcome several of these challenges. It is our belief that, as an international academic community of catalysis researchers, we can (and must) work together to address these challenges, and to drive progress toward the production of next-generation renewable chemicals and fuels from biomass.

09 BIOMASS FUELS↗
DOE OSTI2017

U.S. Industrial Sector Energy Productivity Improvement Pathways

Economy-wide energy systems forecasting models often propose deep emission reduction pathways as a course of action to achieve environmental goals such as de-carbonization. These pathways typically assume that industries adopt all possible energy efficiency measures and replace their remaining energy demand with low e missions resources, e.g. , renewable or nuclear energy. However, given the significant diversity of energy sources and energy-consuming processes, this over-simplifies the real-world technology, process, and co st constraints common to the industrial sector and is a weakness in existing pathways. Moreover, these pathways do not adequately consider the importance of manufacturing to economic prosperity and for producing the technologies that achieve economy-wide environmental goals. This paper reviews historical industrial energy productivity and introduces an analytic framework for developing industrial sector energy productivity pathways that are driven by the goal to transform both the business as usual trends within the industrial sector, as well as the downstream impacts attributable to manufactured products. The framework includes (1) metrics for quantifying energy productivity growth in term s of physical units, value-added, and service; and (2) concurrent approaches for decoupling energy use an d emissions from manufacturing value-added. The framework presented here highlights that emission reduction pathways need to consider the industrial sector not in the aggregate, but as comprised of diverse manufacturing and non-manufacturing industries that affect the energy productivity of other economic sectors: electric power, transportation, and commercial sectors. Such pathways are better equipped to focus on improving the energy productivity of the US economy.

32 ENERGY CONSERVATION, CONSUMPTION, AND UTILIZATI↗
DOE OSTI2016

Plasma Processing of Superconducting Radio Frequency Cavities

The development of plasma processing technology of superconducting radio frequency (SRF) cavities not only provides a chemical free and less expensive processing method, but also opens up the possibility for controlled modification of the inner surfaces of the cavity for better superconducting properties. The research was focused on the transition of plasma etching from two dimensional flat surfaces to inner surfaces of three dimensional (3D) structures. The results could be applicable to a variety of inner surfaces of 3D structures other than SRF cavities. Understanding the A r/C L plasma etching mechanism is crucial for achieving the desired modification of Nb SRF cavities. In the process of developing plasma etching technology, an apparatus was built and a method was developed to plasma etch a single cell Pill Box cavity. The plasma characterization was done with the help of optical emission spectroscopy. The Nb etch rate at various points of this cavity was measured before processing the SRF cavity. Cylindrical ring-type samples of Nb placed on the inner surface of the outer wall were used to measure the dependence of the process parameters on plasma etching. The measured etch rate dependence on the pressure, rf power, dc bias, temperature, CI2 concentration and diameter of the inner electrode was determined. The etch rate mechanism was studied by varying the temperature of the outer wall, the dc bias on the inner electrode and gas conditions. In a coaxial plasma reactor, uniform plasma etching along the cylindrical structure is a challenging task due to depletion of the active radicals along the gas flow direction. The dependence of etch rate uniformity along the cylindrical axis was determined as a function of process parameters. The formation of dc self-biases due to surface area asymmetry in this type of plasma and its variation on the pressure, rf power and gas composition was measured. Enhancing the surface area of the inner electrode to reduce the asymmetry was studied by changing the contour of the inner electrode. The optimized contour of the electrode based on these measurements was chosen for SRF cavity processing.

Upadhyay, Janardan↗
DOE OSTI2016

Examination of Hybrid Metal Coatings for Mitigation of Fission Product Release and Corrosion Protection of LWR SiC/SiC

There is a need to increase the safety margins of current and future light water reactors (LWRs) due to the unfortunate events at Fukushima Daiichi Nuclear Plant. Safety is crucial to restore public confidence in nuclear energy, acknowledged as an economical, high-­density energy solution to climate change. The development of accident-­tolerant fuel (ATF) concepts is crucial to this endeavor. The objective of ATF is to delay the consequences of accident progression, being inset in high temperature steam and maintaining high thermomechanical strength for radionuclide retention. The use of advanced SiCf-­SiC composite as a substitute for zircaloy-­based cladding is being considered. However, at normal operations, SiC is vulnerable to the reactor coolant and may corrode at an unacceptable rate. As a ceramic-­matrix composite material, it is likely to undergo microcracking operation, which may compromise the ability to contain gaseous fission products. A proposed solution to both issues is the application of mitigation coatings for use in normal operations. At Oak Ridge National Laboratory (ORNL), three coating technologies have been investigated with industry collaborators and vendors. These are electrochemical deposition, cathodic arc physical vapor deposition (PVD hereafter) and vacuum plasma spray (VPS). The objective of this document is to summarize these processing technologies, the resultant as-­processed microstructures and properties of the coatings. In all processes, substrate constraint resulted in substantial tensile stresses within the coating layer. Each technology must mitigate this tensile stress. Electrochemical coatings use chromium as the coolant facing material, and are deposited on a nickel or carbon “bond coat”. This is economical but suffers microcracking in the chromium layer. PVD-­based coatings use chromium and titanium in both metallic form and nitrides, and can be deposited defense-­in-­depth as multilayers. This vapor method eliminated tensile stress during processing and coatings were up to ~30 μm thick without microcracking. VPS produced coatings based on Zircaloy-2, which has a proven reactor-­compatibility. The tensile stresses appearred to be partially mitigated by annealing. Analysis showed that VPS coatings required further optimizations to prevent adverse reactions with the substrate and need a minimum thickness of ~50 μm. In addition, development of coatings are constrained by neutronic depletion analysis, which clearly indicated enrichment as an issue if the coating is too thick. Based on the present work, the cathodic arc PVD technology was considered ready for the extensive testing and evaluation on cladding materials due to their ability to mitigate the excessive tensile stresses and the reasonable coating quality achieved. The VPS Zircaloy-­2 coating technology required additional development toward mitigation of issues related to the substrate reaction and porosity. In the future, PVD and VPS will have be scaled upon successful development and demonstration. Electrochemical coatings, which are proven scalability, currently require development to mitigate issues related to the tensile stress after deposition.

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗
NASA NTRS1977

Speech systems research at Texas Instruments

An assessment of automatic speech processing technology is presented. Fundamental problems in the development and the deployment of automatic speech processing systems are defined and a technology forecast for speech systems is presented.

Doddington, George R.↗
DOE OSTI2014

Structure and constitution of glass and steel compound in glass-metal composite

The research using methods of optical and scanning electronic microscopy was conducted and it discovered common factors on structures and diffusing zone forming after welding glass C49-1 and steel Ct3sp in technological process of creating new glass-metal composite. Different technological modes of steel surface preliminary oxidation welded with and without glass were investigated. The time of welding was varied from minimum encountering time to the time of stabilizing width of diffusion zone.

36 MATERIALS SCIENCE↗
NASA NTRS1999

A New Approach to Measure Contact Angle and Evaporation Rate with Flow Visualization in a Sessile Drop

The contact angle and the spreading process of sessile droplet are very crucial in many technological processes, such as painting and coating, material processing, film-cooling applications, lubrication, and boiling. Additionally, as it is well known that the surface free energy of polymers cannot be directly, measured for their elastic and viscous restraints. The measurements of liquid contact angle on the polymer surfaces become extremely important to evaluate the surface free energy of polymers through indirect methods linked with the contact angle data. Due to the occurrence of liquid evaporation is inevitable, the effects of evaporation on the contact angle and the spreading become very important for more complete understanding of these processes. It is of interest to note that evaporation can induce Marangoni-Benard convection in sessile drops. However, the impacts of the inside convection on the wetting and spreading processes are not clear. The experimental methods used by previous investigators cannot simultaneously measure the spreading process and visualize the convection inside. Based on the laser shadowgraphic system used by the present author, a very simple optical procedure has been developed to measure the contact angle, the spreading speed, the evaporation rate, and to visualize inside convection of a sessile drop simultaneously. Two CCD cameras were used to synchronously record the real-time diameter of the sessile drop, which is essential for determination of both spreading speed and evaporation rate, and the shadowgraphic image magnified by the sessile drop acting as a thin plano-convex lens. From the shadowgraph, the inside convection of the drop can be observed if any and the image outer diameter, which linked to the drop profile, can be measured. Simple equations have been derived to calculate the drop profile, including the instantaneous contact angle, height, and volume of the sessile drop, as well as the evaporation rate. The influence of the inside convection on the wetting and spreading processes can be figured out through comparison of the drop profiles with and without inside convection when the sessile drop is placed at different evaporation conditions.

Zhang, Nengli↗
DOE OSTI2013

New Developments in the Technology Readiness Assessment Process in US DOE-EM - 13247

A Technology Readiness Assessment (TRA) is a systematic, metric-based process and accompanying report that evaluates the maturity of the technologies used in systems; it is designed to measure technology maturity using the Technology Readiness Level (TRL) scale pioneered by the National Aeronautics and Space Administration (NASA) in the 1980's. More recently, DoD has adopted and provided systematic guidance for performing TRAs and determining TRLs. In 2007 the GAO recommended that the DOE adopt the NASA/DoD methodology for evaluating technology maturity. Earlier, in 2006-2007, DOE-EM had conducted pilot TRAs on a number of projects at Hanford and Savannah River. In March 2008, DOE-EM issued a process guide, which established TRAs as an integral part of DOE-EM's Project Management Critical Decision Process. Since the development of its detailed TRA guidance in 2008, DOE-EM has continued to accumulate experience in the conduct of TRAs and the process for evaluating technology maturity. DOE has developed guidance on TRAs applicable department-wide. DOE-EM's experience with the TRA process, the evaluations that led to recently developed proposed revisions to the DOE-EM TRA/TMP Guide; the content of the proposed changes that incorporate the above lessons learned and insights are described. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
DOE OSTI2023

Laboratory-Scale Coal-Derived Graphene Process (Final Report)

The Energy & Environmental Research Center (EERC) conducted a laboratory-scale coal-derived graphene (CDG) project focused on developing a technological process for making graphene from four U.S. domestic coal or coal wastes, including lignite from North Dakota, subbituminous coal from Wyoming, bituminous coal from Utah, and anthracite from Pennsylvania. The project was divided into two performance or budget periods (BPs), with BP1 comprising the up-front laboratory experiments to make graphene materials from coal beginning on May 1, 2020, to April 30, 2022. BP2 was conducted from May 1, 2022, to April 30, 2023, and was focused on analyzing the CDG process economic feasibility and the technical gaps for technological scale-up and commercialization. During this project, a few different coal-derived high-value products have been demonstrated, including graphite, graphene oxide (GO), reduced graphene oxide (rGO), and graphene quantum dots (GQDs). A new graphite microstructure was discovered and named “croissant graphite” because of the exterior morphological and textural resemblance to croissant food items sold in commercial groceries stores. The new graphite structure and the associated preparation from coal or coal waste feedstocks has been the subject of a U.S. patent application. The systematic experimental processes involving coal cleaning, upgrading, and conversion to high-value carbon products culminated into a developed upgraded coal-to-products (UCP) technology that is being pursued for potential fast-track commercialization, if funding is available. It is envisioned that commercialization of the UCP technology would increase consumption of U.S. domestic coals or coal wastes to make environmentally sustainable high-value products for the electronics industry, high-energy-storage applications, and clean energy technologies such as electric vehicle (EV) lithium-ion batteries (LIBs), for which graphite has become a critical mineral commodity. Croissant graphite microstructures, when observed by field emission scanning electron microscopy (FESEM), display wavy surface morphology and often grow from a base that is made of graphitized particles with honeycomb-like layers, which are believed to be graphene layers. While more studies are needed to fully ascertain the mechanisms of the croissant graphite microstructure formation, it is postulated that their growth may begin from curling of the graphene sheets into ribbon-like structures, and continuous growth and densification of the ribbon-like structures forms croissant microstructures. Additional studies are ongoing to evaluate the electrochemical performance of croissant graphite for LIB applications and to determine the experimental conditions necessary to tune on/off croissant formation so that it can be either optimized or suppressed depending on performance evaluation results. In addition to the discovery of croissant graphite, the graphitization process from the four coal ranks in general was successful. X-ray diffraction (XRD) analysis showed that the degree of graphitization (DoG) ranged from 12% to 80% in an early sample set, and further optimization on lignite coal produces a DoG of about 92%, which was spectacular to see as lignite is the lowest-rank coal. Thus, it is expected that the graphitization performance for higher-rank coals will be similar or better when optimized as well. The coal-derived graphite was used to make GO and rGO. Analytical characterization, e.g., by methods such as Raman spectroscopy, XRD, Fourier transform infrared (FTIR) spectroscopy and FESEM, showed that the sequence of converting the coal to graphite, exfoliating it to GO, and then chemically reducing the GO to rGO was successful. Although coal naturally contains aromatic compounds and some relatively small-sized condensed aromatic units, it does not contain graphene sheets. In the UCP process, the aromatic domains in the coals, particularly low-rank coals, are concentrated and condensed further into graphene sheets, which are ordered into a 3D stack during graphitization. The synthesized graphite is then unpacked by methods such as exfoliation to various graphene products. GQDs were synthesized from all four coal types, and their optical properties were demonstrated to be tunable by the coal precursor preprocessing treatments. In all four coal types, enhanced optical properties were observed for the produced GDQs with incremental improvements made to the coal precursors. GQDs produced from raw coal samples displayed lower ultraviolet–visible (UV–Vis) spectroscopy absorbance intensity compared to those obtained from cleaned and upgraded coal residues. The photoluminescence (PL) intensities also varied with pretreatment conditions and with the concentration of GQDs in aqueous solutions. GQDs obtained from anthracite show longer emission wavelengths and can be excited by visible light as opposed to GQDs derived from the other coal ranks. UV fluorescence 3D maps and spectra revealed that the emission wavelength at which the GQDs solutions display the highest intensity was slightly redshifted based on the coal precursor pretreatments. In low-rank coal (lignite and subbituminous) samples, two clusters were observed in the maps for GQDs, which may suggest that there are potentially two types of fluorophores in solution or two main size populations. The ability to tune the properties of GQDs based on processing methods can be exploited to make GQDs for various optical display or optoelectronics applications. The results also highlight the importance of removing coal-borne impurities to improve the quality of the coal precursor for preparation of graphene products. Coal and/or coal wastes preprocessing methods were developed and applied to clean and upgrade the coal precursors prior to graphitization and subsequent conversion to graphene products. The preprocessing methods involve high specific-gravity separations, mineral acid cleaning (no hydrofluoric acid), and subsequent upgrading by reducing the coal-borne heteroatom (nitrogen, sulfur, and oxygen) content using proprietary chemical agents. Analytical characterization revealed that the preprocessing steps were successful, with ash reductions that range from 38% to 80% and residual ash content that was below the 5 wt% initial target. Based on proximate and ultimate analysis, the heteroatom reduction reactions produced upgraded coal residues with the oxygen content reduced by 8% to 24%, with additional reductions in the nitrogen and sulfur contents. An initial assessment of the waste streams from the UCP process shows very small to negligible environmental impact due to CO 2 , NO x , and SO x because most process steps are performed under inert atmosphere with argon. Consequently, reactive oxygen environments that tend to create these species are avoided. The inorganic and potentially hazardous species are released into aqueous waste streams that are easy to handle for proper disposal. The liquid waste streams were found to contain low-level concentrations of rare-earth elements (REEs), which could be concentrated and recovered as value-added by-products. Additionally, the volatile and gaseous fractions from carbonization and heat treatment contain useful organic compounds that can also be recovered as potential valuable by-products. Thus, the UCP technology is considered an environmentally sustainable and promising emerging technology for making high-value products from coal and coal wastes, with potential additional value-added by-products. Analysis of potential markets for the coal-derived carbon products shows a strong demand in both niche market sectors and across a wide variety of other industrial sectors. Graphite is currently considered a critical mineral commodity that has a large and growing demand in the LIB industry for EV applications. Based on data from Fortune Business Insights (2022) and Marketwatch (2023) reports, the average global graphite market is projected to reach about 33 billion by 2028, growing at a compound annual growth rate (CAGR) of about 7%, with much of this growth expected to be in the LIB industry. GO and rGO have strong market potentials in various application areas, such as coatings for anticorrosion, anti-icing, and antimicrobial protection, thermal barriers, wear resistance, sensors, additive manufacturing such as 3D inks, and others. GQDs are the emerging key player in the bioimaging, photovoltaics, and light-emitting diodes (LEDs) applications, with the potential to replace traditional semiconductor quantum dots (SQDs), which are based on metallic systems that are more toxic and more expensive. Biomedical applications of GQDs are becoming more attractive because of low to no toxicity and extremely low cost compared to SQDs. The major challenges for scale-up and commercialization of coal-derived carbon products such as graphene vary from the inherent attributes of graphene itself to reluctance to accept graphene in new manufacturing processes because of the uncertainty of the unknown. The 2D nature of graphene materials with a thickness of one atom presents significant challenges to proper handling/processing, and process scale-up becomes difficult because it requires high-end, expensive equipment, even for routine handling and analysis for quality assurance and control. Pristine graphene can also be extremely difficult to work into other matrices, thus hindering downstream processibility, especially at large scale. Currently, the cost of graphene and graphene products is still high and presents an economic risk that tends to slow down investment in scaling up emerging technologies. The lack of a standard for graphene materials for quality assurance and quality control poses a great challenge not only for the markets but also for commercialization efforts. A first-look economic feasibility analysis of the UCP technology provided valuable information that suggests the UCP process would be feasible, especially when it is scaled to a pilot scale and could be more competitive at the full scale. Graphitization was found to be the most energy-consuming and most capital-intensive step in the overall process. In small laboratory- and bench-scale experiments, labor is a significant contributor to the total process costs. Although these energy, capital, and labor constraints contribute to a higher selling price for the product, a preliminary economic model suggests that the process would be feasible at large scale when the process is fully integrated, optimized, and automated.

01 COAL, LIGNITE, AND PEAT↗
NASA NTRS2014

TPSAS-NF1676L-18913-DND

Composite materials and structures are enabling technology for modern aerospace vehicles. Numerical-control manufacturing, including automated fiber placement (AFP), is widely used to fabricate these components. However, weight and performance requirements for the next generation of aerospace vehicles will push the state-of-art even further, and require development of more advanced materials, manufacturing, and structures technologies that are both affordable and efficient. The Integrated Structural Assembly of Advanced Composites (ISAAC) system is intended to address much of NASA?s critical research needs in advanced composites. The baseline ISAAC system, combining a commercial robot with multiple redundant degrees of freedom, a tool changer interface, and a special-purpose AFP end effector, enables precise and accurate additive manufacturing of composite structures, as well as development of advanced tow-steered structures with tailored load paths. The highly capable baseline system can quickly change end effectors, thus enabling further research for composites manufacturing. This extended system is similar to a high-speed machining center, where interchangeable cutters are used for different operations during metal structures fabrication. This capability enables future development, integration and assessment of new advanced manufacturing technologies, such as in-situ curing and NDE, and through-thickness reinforcements to reduce delaminations. End effectors with these advanced capabilities may be purchased, developed internally or with industry or academia, and then integrated onto the existing robotic platform to perform advanced manufacturing operations and develop new techniques and processes. Technologies, techniques and processes developed using this research-oriented system could then be transitioned to the broader composites industry.

Rob Martin↗
NASA NTRS2005

Control of Effluent Gases from Solid Waste Processing using Impregnated Carbon Nanotubes

One of the major problems associated with solid waste processing technologies is effluent contaminants that are released in gaseous forms from the processes. This is a concern in both biological as well as physicochemical solid waste processing. Carbon dioxide (CO2), the major gas released, does not present a serious problem and there are currently in place a number of flight-qualified technologies for CO2 removal. However, a number of other gases, in particular NOx, SO2, NH3, and various hydrocarbons (e.g. CH4) do present health hazards to the crew members in space habitats. In the present configuration of solid waste processing in the International Space Station (ISS), some of these gases are removed by the Trace Contaminant Control System (TCCS), demands a major resupply. Reduction of the resupply can be effective by using catalyst impregnated carbon nanotubes. For example, NO decomposition to N2 and O2 is thermodynamically favored. Data showing decomposition of NO on metal impregnated carbon nanotubes is presented. Comparisons are made of the existing TCCS systems with the carbon nanotube based technology for removing NOx based on mass/energy penalties.

Li, Jing↗
DOE OSTI2020

Fabrication of field-effect transistors with transfer-free nanostructured carbon as semiconducting channel material

Carbon nanostructures as active channel material in field effect transistors (FETs) are appealing in microelectronics for their improved performance such as high speed and low energy dissipation. However, these devices require the incorporation of nanostructure transfer steps in the fabrication process flow, which makes difficult its application in large scale integration circuits. Here we present a novel method for the fabrication of FETs with nanostructured carbon in the channel with p-type semiconducting properties and intermediate drain-source current (IDS) on/off ratio. The method is based on the use of Ni nanoparticles in the source-drain gap region as seed material for the formation of carbon nanostructures in the FET channel. FETs without Ni nanoparticles in the channel showed no modulation of IDS as a function of gate voltage. The device fabrication process does not require any carbon nanostructure transfer steps since it directly forms carbon nanostructures electrically connected to the device's source and drain electrodes via electron-beam evaporation of carbon and conventional lithographic processes. Since all device fabrication steps are compatible with Si technology processes, they are capable of being further optimized following process development protocols practiced by the semiconductor industry.

77 NANOSCIENCE AND NANOTECHNOLOGY↗
DOE OSTI2017

A Multi-scale, Multi-Model, Machine-Learning Solar Forecasting Technology

The goal of the project was the development and demonstration of a significantly improved solar forecasting technology (short: Watt-sun), which leverages new big data processing technologies and machine-learnt blending between different models and forecast systems. The technology aimed demonstrating major advances in accuracy as measured by existing and new metrics which themselves were developed as part of this project. Finally, the team worked with Independent System Operators (ISOs) and utilities to integrate the forecasts into their operations.

97 MATHEMATICS AND COMPUTING↗
NASA NTRS1967

Study of random process theory aids digital data processing

Study of techniques for all random process technology, including stationary, nonstationary, and Gaussian bivariate, aids digital data processing. It presents material on digital filtering, correlation function, optimal spectral smoothing, deterministic data processing, and nonstationary spectrum and correlation analyses.

Bordner, G. W.↗