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At least 271 records · Page 15
All sourcesNASA NTRSDOE OSTI
NASA NTRSDate not supplied

Gaseous By-Product of Thermal Vacuum Processing of Lunar Highland Simulant

Scientists at Kennedy Space Center are advancing technologies to achieve oxygen extraction on the Lunar surface. One such technology is Molten Regolith Electrolysis (MRE) in which regolith simulant is melted under high temperatures to perform oxygen extraction through electrolysis of the melt pool. A study was conducted to understand the molten formation and proper-ties of Lunar Highlands Simulants (LHS-1) under high vacuum environments ranging between 10-6 Torr. These studies include investigating the regolith melt behavior and by-product gas analysis systems to prepare for pilot plant development and operations. The off-gassing rates and pressure build-up, gaseous compounds, and material compatibility may be a risk to MRE systems. The KSC findings are reported here for inclusion into future mis-sion architecture and operational planning. The four stages of the experiment were vacuum, resistive heating, regolith melt and gas detection. The regolith mass of 70 g was melted in a 40 cm tall x 50 cm diameter vacuum chamber at temperature increase rate 47 ℃ /min and ramp rate of 1 ampere/3 min up to an 18-amp maximum. The test is conducted for about 60 minutes and the constituent gases produced during heating of regolith is monitored with a re-sidual gas analyzer. During the molten formation, primary off-gassing volatiles included water vapor (18 amu), a peak at 44 amu (FeO2 – expected), and atomic oxygen (16 amu), among a series of other compounds that could create compatibility issues such as magnesium, chlorine, and silicon oxide. These results add to the knowledge required for successful oxygen extraction on the moon.

Molten Regolith Electrolysis↗
NASA NTRSDate not supplied

Carbothermal Reduction Demonstration: Laser Driven Reaction in a Thermal-Vacuum Environment and Project Status

Introduction: Lunar regolith is approximately 45% oxygen by mass. The majority of the oxygen is bound in silicate minerals. The carbothermal reduction process has been proven to be effective at removing oxygen from lunar regolith simulants [1]. The Carbothermal Reduction Demonstration (CaRD) project aims to increase the Technology Readiness Level (TRL) of a combined solar concentrator and carbothermal reduction systemin order to demonstrate this technology on the lunar surface. The CaRD project is divided into two design cycles, a brass board and prototype. The status of both design cycles will be discussed, as well as concepts for how this technology can be applied to the Artemis program in the future. Brassboard Vacuum Test: For the brassboard demonstration, a 2 kW Nd-YAG laser was used to heat lunar regolith simulant within a carbothermal reactor developed by Sierra Space. The reactor was placed inside of a 15 ft thermal vacuum chamber at the Johnson Space Center. The resulting reaction products were analyzed using both a gas chromotograph and mass spectrometer provided by Kennedy Space Center. Thermal data was also collected. Prototype Design: For the prototype, the CaRD team will perform another thermal vacuum test at JSC using the same interfaces and assets developed for the brassboard but will test a new carbothermal reactor design that Sierra Space is developing through the Carbothermal Oxygen Production Reactor (COPR) Tipping Point project that will include a means to autonomously move regolith in and out of the reactor. In addition, a deployable solar concentrator is being developed by Glenn Research Center using mirrors produced by Carbon Mirror Applications. The solar concentrator will be used to deliver solar energy into a carbothermal reactor to melt regolith and extract oxygen. Avionics and software for the concentrator are being developed by Kennedy Space Center. Future Concepts: An ongoing task within the CaRD project is to update models that can be used to determine the mass, power, and size of In-Situ Resource Utilization concepts at various scales. These models can now be used to analyze alternatives for future applications based on the latest available data.

A J Paz↗
NASA NTRSDate not supplied

Thermal Vacuum and Vibration Testing of the Differential Thermal Expansion Thermal Switch

The Extended Stroke, Reverse Operation, Differential Expansion Thermal Switch for Extreme Variable Environments uses materials with both positive and negative coefficients of thermal expansion (CTE) arranged in concentric cylinders so that the thermal switch (TS) operates passively, opening a gap between interfaces to create a low thermal contact when cold, and closing the gap between interfaces to create a high thermal contact when hot. This paper details the testing of the TS at Marshall Space Flight Center including the pre-vibe thermal vacuum cycle test, vibration test, post-vibe thermal vacuum cycle test, and long duration thermal vacuum cycle test. The pre- and post-vibe thermal cycle and the long duration cycle test tested to hot and cold plateau initial temperatures of 40 °C, and -173 °C, respectively. The pre- and post-vibe tests required plateau holds of at least 2 hours, whereas the long duration cycle test required plateau holds of at least 20 hours. The tests each used a rate of temperature change of < 2 °C/min when transitioning between plateaus. The data collected from each thermal test is compared to show the operation of the TS both before and after the vibration test to GEVS levels, and throughout the long duration cycle test. From the data collected, the total conductance through the TS interfaces is calculated for both on (TS closed – during hot plateau) and off (TS open – during cold plateau) configurations, and the turndown ratio is also calculated. Challenges and lessons learned from the testing are also discussed.

thermal control technology↗
NASA NTRSDate not supplied

On Predicting Transient Pressure in Vacuum Systems Featuring Getter Materials

Getter materials have been used to reduce pressure or partial pressures in a variety of vacuum applications ranging from vacuum tubes to space flight science instruments. Testing of getter materials has tended to emphasize the capacity of candidate materials to collect specific gas species in sufficient quantities to size them in these applications. When determining a getter material’s capacity, it is typically subjected to enough excess target gas to ensure it sorbs as quickly as possible. However, when both the gas source strength and the getter’s sorption rate exhibit transient decay behavior, such data is not sufficient to predict the targeted species’ partial pressure within a vacuum system as a function of time.

M. S. Woronowicz↗
NASA NTRSDate not supplied

Trace Contaminant Control Test Bed for Evaluation of TCC Prototypes with Vacuum Regenerable and Non-Regenerable Sorbents

A new Space Suit Exploration Portable Life Support System (xPLSS) is being designed, built, integrated, and tested into the Extra-Vehicular Mobility Unit (xEMU). The Trace Contaminant Control (TCC) system is a component in the oxygen ventilation loop of xPLSS that removes contaminants generated by the crewmembers’ metabolic processes. The primary trace contaminants that must be removed include ammonia (NH3), carbon monoxide (CO), formaldehyde (CH2O), and methyl mercaptan (CH3SH). The current state-of-the-art TCC sorbent is non-regenerable activated carbon. As a non-regenerable sorbent, its use negatively impacts the logistics for future missions. Thus, an ideal solution can be a vacuum-regenerable sorbent integrated with the xPLSS CO2/H2O removal system. To test new designs and sorbents, XploSafe has constructed a recirculating test bed that mimics the environment within the xPLSS by providing concentrations of the trace contaminant analytes generated at the operating temperature, humidity, pressure, and flow rates of the xPLSS. This system can perform regeneration or desorption by exposing the sorbent to a pressure swing from 4.3 psia to <1 torr over approximately 2 minutes. Using this test system, XploSafe evaluated various TCC prototypes constructed using rapid prototyping techniques and identified a process that allows vacuum regenerative TCC designs to be quickly examined for flow, pressure drop, and performance. By using toluene as a segregate for volatile organics, this test system was evaluated using both vacuum regenerable and non-regenerable sorbents to demonstrate the operational effectiveness of these sorbents in maintaining the concentrations of the trace contaminant analytes below the 7-day Spacecraft Maximum Allowable Concentrations.

Nicholas Materer↗
NASA NTRSDate not supplied

On Predicting Transient Pressure in Vacuum Systems Featuring Getter Materials

Getter materials have been used to reduce pressure or partial pressures in a variety of vacuum applications ranging from vacuum tubes to space flight science instruments. Testing of getter materials has tended to emphasize the capacity of candidate materials to collect specific gas species in sufficient quantities to size them in these applications. When determining a getter material’s capacity, it is typically subjected to enough excess target gas to ensure it sorbs as quickly as possible. However, when both the gas source strength and the getter’s sorption rate exhibit transient decay behavior, such data is not sufficient to predict the targeted species’ partial pressure within a vacuum system as a function of time.

M. S. Woronowicz↗
NASA NTRSDate not supplied

On Predicting Transient Pressure in Vacuum Systems Featuring Getter Materials

Getter materials have been used to reduce pressure or partial pressures in a variety of vacuum applications ranging from vacuum tubes to space flight science instruments. Testing of getter materials has tended to emphasize the capacity of candidate materials to collect specific gas species in sufficient quantities to size them in these applications. When determining a getter material’s capacity, it is typically subjected to enough excess target gas to ensure it sorbs as quickly as possible. However, when both the gas source strength and the getter’s sorption rate exhibit transient decay behavior, such data is not sufficient to predict the targeted species’ partial pressure within a vacuum system as a function of time.

Michael Woronowicz↗
NASA NTRSDate not supplied

Thermal Vacuum Testing Strategy and Thermal Desktop Model Correlation for the Moon to Mars Planetary Autonomous Construction Technologies (MMPACT) Robotic Terrestrial Arm

This paper discusses the initial thermal vacuum testing of the MMPACT robotic terrestrial arm. The robotic arm is part of a construction system designed for the lunar south pole surface. The first thermal vacuum test was a risk mitigation test to ensure the arm could operate in vacuum, with all other data collection as secondary priorities. 44 thermocouples (TCs) were attached to the arm. Installation was done with additional care to account for both the extra wiring harness weight on the arm with the TC wires and increased focus on stabilizing the TC attachments to the moving components. Thermal steady state of <= 0.01°C/hour was reached for the hot set of testing conditions. This data was used to correlate the Thermal Desktop (TD) model to the test results within +/- 5°C.

Thermal analysis↗
NASA NTRSDate not supplied

Thermal Vacuum Testing Strategy and Thermal Desktop Model Correlation for the Moon to Mars Planetary Autonomous Construction Technologies (MMPACT) Robotic Terrestrial Arm

This paper discusses the initial thermal vacuum testing of the MMPACT robotic terrestrial arm. The robotic arm is part of a construction system designed for the lunar south pole surface. The first thermal vacuum test was a risk mitigation test to ensure the arm could operate in vacuum, with all other data collection as secondary priorities. 44 thermocouples (TCs) were attached to the arm. Installation was done with additional care to account for both the extra wiring harness weight on the arm with the TC wires and increased focus on stabilizing the TC attachments to the moving components. Thermal steady state of <= 0.01°C/hour was reached for the hot set of testing conditions. This data was used to correlate the Thermal Desktop (TD) model to the test results within +/- 5°C.

Thermal analysis↗
NASA NTRSDate not supplied

Thermal Design and Thermal Vacuum Testing of the StarBurst Instrument

The StarBurst Multimessenger Pioneer is a small satellite mission serving as a wide-field gamma-ray observatory designed to capture the initial emissions of short gamma-ray bursts, electromagnetic signatures of neutron star mergers. This paper presents the final thermal design and analysis of the StarBurst Instrument, comprising the bus-to-instrument interface plate, control electronics, and twelve crystal detector units, which form the core of the mission’s science capability. The passive thermal control system design requires consideration of restrictive keep-out zones, unknown orbital parameters, and narrow temperature limits of the detectors. Also summarized is the instrument level thermal vacuum cycle test, correlated model refinements, and updated model results. Following successful completion of the instrument test campaign, the hardware was integrated with the spacecraft bus for spacecraft level testing, including additional thermal vacuum testing. The results from the spacecraft level thermal vacuum test will further inform the instrument thermal model, ensuring accurate flight temperature predictions. StarBurst launches as a secondary payload in 2027 and has a mission duration of at least one year.

StarBurst↗
NASA NTRS2008

Carbon Nanotube Vacuum Gauges Utilizing Long, Dissipative Tubes

CNT Vacuum Gauges: a) have a broad range of pressure response from 760 - 10(exp -6) Torr. b) have current changes approx. 100's nA in high vacuum regime (10(exp -6) Torr) and sensitivity increases with power and substrate removal. c) have a negative dR/dT (TCR negative) where a thermal hopping energy E(sub a) was determined to be approx. 40 meV. d) have compatible fabrication requirements for their integration with micromachined structures. e) can be operated at low power (nW - micro-W). f) have an active device region footprint of < 10 sq microns. g) are non-intrusive due to small size and passive operation.

nanotube sensors↗
NASA NTRS1963

Feasibility of liquid-metal vacuum seals

A basic component of any ultrahigh-vacuum system is a seal capable of isolating a test chamber from its higher pressure surroundings. Two of the most common vacuum seals now in use are the elastomer O-ring seal and the metallic shear seal. The former has the problem of outgassing and gas permeation; the latter requires a large force per unit seal-length to maintain the sealing action. The search for a seal which would provide minimal virtual and real leak rates in a chamber, without requiring a large force to consummate the seal, led to investigation of a liquid-metal seal.

SEALANT↗
NASA NTRS1965

Space vacuum investigations

Inaccessible-Non Repairable- Costly: The meaning of these words is absolute in the event of a complete failure of an orbiting spacecraft. Adequate design, or rather, minimizing chance of failure, challenges all scientists and engineers. Where experience has not been developed, the risk involved in a new application must be weighed against the consequence of a design failure. In space work, the spectrum of consequence is extremely wide. It ranges from loss of scientific data on one hand, to loss of life on the other.. There is little question that knowledge of the space environment and its effects must be determined to produce reliable spacecraft. Tests to prove the design must be performed with equipment capable of simulating the effects of the environment in which the design is to operate. This does not necessarily mean that the natural environment must be duplicated. The degree of environmental simulation that should be achieved depends primarily upon the significance of the physical effects it causes. The purpose of space vacuum simulation in an environmental test program should be accurately conceived and the testing phased to obtain maximum information from the limited samples available for test. This discussion is confined to some of the factors involved in simulating the effects of space vacuum environment. This survey is by no means complete, but will touch on some of the highlights in this field: 1. A description of the environment 2. The level of simulation necessary to evaluate its effects 3. Test equipment capability 4. Experience in test 5. Experience in orbit 6. Observations & future emphasis

VACUUM EFFECT↗
NASA NTRS2007

Prospects for Ultra-Stable Timekeeping with Sealed Vacuum Operation in Multi-Pole Linear Ion Trap Standards

A recent long-term comparison between the compensated multi-pole Linear Ion Trap Standard (LITS) and the laser-cooled primary standards via GPS carrier phase time transfer showed a deviation of less than 2.7x10(exp -17)/day. A subsequent evaluation of potential drift contributors in the LITS showed that the leading candidates are fluctuations in background gases and the neon buffer gas. The current vacuum system employs a "flow-through" turbomolecular pump and a diaphragm fore pump. Here we consider the viability of a "sealed" vacuum system pumped by a non-evaporable getter for long-term ultra-stable clock operation. Initial tests suggests that both further stability improvement and longer mean-time-between-maintenance can be achieved using this approach

timekeeping stability↗
NASA NTRS2014

James Webb Space Telescope (JWST) Integrated Science Instruments Module (ISIM) Cryo-Vacuum (CV) Test at GSFC

JWST ISIM has entered into its system-level testing program at NASA Goddard Space Flight Center (GSFC). In December 2013, ISIM successfully completed the first in a series of three cryo-vacuum tests, which included two flight science instruments. Since then, there have been full-fledged efforts towards the CV2 test scheduled to finish at the end of 2014. The complexity of the mission has generated challenging requirements that demand highly reliable system performance and capabilities from the Space Environment Simulator (SES) vacuum chamber. In order to satisfy the program requirements, GSFC had to develop unique structural and thermal hardware to test ISIM. Most noteworthy is a helium shroud structure and cooling system built in order to achieve operational temperatures below 20K (-253C). This paper: (1) provides an overview of the integrated mechanical and thermal facility systems required to achieve the objectives of JWST ISIM testing, (2) communicates the performance and challenges of the SES during the first ISIM test, and (3) summarizes the action plan to improve the system prior to the next test.

Thermal Vacuum Cryo Testing Chamber↗
NASA NTRS2015

Impact of Drilling Operations on Lunar Volatiles Capture: Thermal Vacuum Tests

In Situ Resource Utilization (ISRU) enables future planetary exploration by using local resources to supply mission consumables. This idea of 'living off the land' has the potential to reduce mission cost and risk. On the moon, water has been identified as a potential resource (for life support or propellant) at the lunar poles, where it exists as ice in the subsurface. However, the depth and content of this resource has yet to be confirmed on the ground; only remote detection data exists. The upcoming Resource Prospector mission (RP) will 'ground-truth' the water using a rover, drill, and the RESOLVE science package. As the 2020 planned mission date nears, component level hardware is being tested in relevant lunar conditions (thermal vacuum). In August 2014 a series of drilling tests were performed using the Honeybee Robotics Lunar Prospecting Drill inside a 'dirty' thermal vacuum chamber at the NASA Glenn Research Center. The drill used a unique auger design to capture and retain the lunar regolith simulant. The goal of these tests was to investigate volatiles (water) loss during drilling and sample transfer to a sample crucible in order to validate this regolith sampling method. Twelve soil samples were captured over the course of two tests at pressures of 10(exp-5) Torr and ambient temperatures between -80C to -20C. Each sample was obtained from a depth of 40 cm to 50 cm within a cryogenically frozen bed of NU-LHT-3M lunar regolith simulant doped with 5 wt% water. Upon acquisition, each sample was transferred and hermetically sealed inside a crucible. The samples were later baked out to determine water wt% and in turn volatile loss by following ASTM standard practices. Of the twelve tests, four sealed properly and lost an average of 30% of their available water during drilling and transfer. The variability in the results correlated well with ambient temperature (lower the temperature lower volatiles loss) and the trend agreed with the sublimation rates for the same temperature. Moisture retention also correlated with quantity of sample: a larger amount of material resulted in less water loss. The drilling process took an average of 10 minutes to capture and transfer each sample. The drilling power was approximately 20 Watt with a Weight on Bit of approximately 30 N. The bit temperature indicated little heat input into formation during the drilling process.

drilling↗