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At least 289 records · Page 16

Design, fabrication and test of graphite/polyimide composite joints and attachments for advanced aerospace vehicles

Results of an experimental program to develop several types of graphite/polyimide (GR/PI) bonded and bolted joints for lightly loaded flight components for advanced space transportation systems and high speed aircraft are presented. Tasks accomplished include: a literature survey; design of static discriminator specimens; design allowables testing; fabrication of test panels and specimens; small specimen testing; and standard joint testing. Detail designs of static discriminator specimens for each of the four major attachment types are presented. Test results are given for the following: (1) transverse tension of Celion 3000/PMR-15 laminate; (2) net tension of a laminate for both a loaded and unloaded bolt hole; (3) comparative testing of bonded and co-cured doublers along with pull-off tests of single and double bonded angles; (4) single lap shear tests, transverse tension and coefficient of thermal expansion tests of A7F (LARC-13 amide-imide modified) adhesive; and (5) tension tests of standard single lap, double lap, and symmetric step lap bonded joints. Also, included are results of a finite element analysis of a single lap bonded composite joint.

Barclay, D. L.↗

Tensile and fatigue characterization of multifunctional composites

This research is part of a larger effort to develop advanced self-sensing multifunctional polymer composites that are both lightweight and high-strength, while also enabling structural damage detection, fatigue cycle monitoring, and service life prediction. These multifunctional composites are particularly sought after in the automotive industry for their potential to significantly reduce vehicle weight and simultaneously provide additional functionality like condition monitoring to enhance safety. This study examines the tensile and fatigue properties of a composite material composed of acrylonitrile butadiene styrene (ABS) polymer embedded with piezoelectric barium titanate (BaTiO3) nanoparticles. The integration of BaTiO3 nanoparticles not only supplies the material with self-sensing capabilities but also influences its mechanical properties. While a high content of BaTiO3 nanoparticles is desired to enhance sensing capacity, the brittle nature of such materials causes concerns of decreased strength characteristics. To explore this, various composite samples were fabricated with nanoparticle contents ranging from 0 wt% to 20 wt%. These samples underwent tensile testing to measure their ultimate tensile strengths and Young’s moduli. Following this, fatigue tests were conducted to generate S-N curves, which are essential for understanding the material's durability under cyclic loading. The findings from these tests assess the impact of nanoparticle content on the composite’s tensile strength and fatigue life, providing essential insights that can guide the optimization and design of future self-sensing multifunctional composites. The results suggest that 5 wt% BaTiO3 provides an optimal balance between mechanical properties and nanoparticle concentration, making it a promising composition for semi-structural applications.

Bowland, Christopher [ORNL] (ORCID:000000021229431↗

Imparting Barely Visible Impact Damage to a Stitched Composite Large-Scale Pressure Box

The Pultruded Rod Stitched Efficient Unitized Structure (PRSEUS) is a concept that was developed by The Boeing Company to address the complex structural design aspects associated with a pressurized hybrid wing body (HWB) aircraft configuration, which has been a focus of the NASA Environmentally Responsible Aviation Project. The NASA-Boeing structural development for the HWB aircraft culminated in testing of the multi-bay box, which is an 80%-scale representation of the pressurized center-body section. This structure was tested in the NASA Langley Research Center Combined Loads Test System facility. As part of this testing, barely visible impact damage was imparted to the interior and exterior of the test article to demonstrate compliance with a condition representative of the requirements for Category 1 damaged composite structure as defined by the Federal Aviation Regulations. Interior impacts were imparted using an existing spring-loaded impactor, while the exterior impacts were imparted using a newly designed, gravity-driven impactor. This paper describes the impacts to the test article, and the design of the gravitydriven guided-weight impactor. The guided-weight impactor proved to be a very reliable method to impart barely visible impact damage in locations which are not easily accessible for a traditional drop-weight impactor, while at the same time having the capability to be highly configurable for use on other aircraft structures.

Lovejoy, Andrew E.↗

Room Temperature Creep Of SiC/SiC Composites

During a recent experimental study, time dependent deformation was observed for a damaged Hi-Nicalon reinforced, BN interphase, chemically vapor infiltrated SiC matrix composites subjected to static loading at room temperature. The static load curves resembled primary creep curves. In addition, acoustic emission was monitored during the test and significant AE activity was recorded while maintaining a constant load, which suggested matrix cracking or interfacial sliding. For similar composites with carbon interphases, little or no time dependent deformation was observed. Evidently, exposure of the BN interphase to the ambient environment resulted in a reduction in the interfacial mechanical properties, i.e. interfacial shear strength and/or debond energy. These results were in qualitative agreement with observations made by Eldridge of a reduction in interfacial shear stress with time at room temperature as measured by fiber push-in experiments.

Morscher, Gregory N.↗

The Shape Effect: Influence of 1D and 2D Boron Nitride Nanostructures on the Radiation Shielding, Thermal, and Damping Properties of High-Temperature Epoxy Composites

In space exploration, lightweight multifunctional materials capable of shielding neutron radiation, dissipating heat, and providing damping are essential. Polymer composites reinforced with boron nitride (BN) nanomaterials—specifically one-dimensional boron nitride nanotubes (BNNTs) and two-dimensional boron nitride nanoplatelets (BNNPs)—offer promising solutions. This study investigates how BN nanomaterial morphology influences the performance of high-temperature (HT) epoxy composites. We developed ultralightweight, three-dimensional BN foams comprising 1D BNNTs, 2D BNNPs, and hybrid 1D BNNT/2D BNNP structures via freeze-drying, then infiltrated them with HT epoxy to form dense composites. The BNNT foam exhibited the highest neutron radiation shielding, with a mass absorption coefficient of 26.64 cm2 g −1 , outperforming the hybrid foam (18.18 cm 2 g −1 ) and the BNNP foam (11.12 cm 2 g −1 ). A similar trend was observed in the HT epoxy composites; incorporating these foams at least doubled the mass absorption coefficient compared to the neat polymer. In terms of thermal conductivity, the BNNT/BNNP foam-epoxy composite achieved the highest value of 0.34 W m −1 K −1 , a 2.13-fold increase over neat HT epoxy. The BNNT/BNNP foam-epoxy composites also improved by 1.88 and 1.75 times, respectively. Mechanical testing revealed that BNNP foams withstood the highest loads during nanoindentation (3.53 kN), followed by BNNT/BNNP foams (1.93 kN) and BNNT foams (1.56 kN). All BN foam-epoxy composites exhibited enhanced damping properties, with tan δ increasing by at least 30 % compared to neat HT epoxy. These findings elucidate the impact of BN nanomaterial morphology on the multifunctional performance of HT epoxy composites, offering insights for developing high-performance, tailorable materials for demanding environments.

Kazue Orikasa↗

Test and Analysis of a Buckling-Critical Large-Scale Sandwich Composite Cylinder

Structural stability is an important design consideration for launch-vehicle shell structures and it is well known that the buckling response of such shell structures can be very sensitive to small geometric imperfections. As part of an effort to develop new buckling design guidelines for sandwich composite cylindrical shells, an 8-ft-diameter honeycomb-core sandwich composite cylinder was tested under pure axial compression to failure. The results from this test are compared with finite-element-analysis predictions and overall agreement was very good. In particular, the predicted buckling load was within 1% of the test and the character of the response matched well. However, it was found that the agreement could be improved by including composite material nonlinearity in the analysis, and that the predicted buckling initiation site was sensitive to the addition of small bending loads to the primary axial load in analyses.

Schultz, Marc R.↗

Detection of Delamination in Composite Beams Using Broadband Acoustic Emission Signatures

Delamination in composite structure may be caused by imperfections introduced during the manufacturing process or by impact loads by foreign objects during the operational life. There are some nondestructive evaluation methods to detect delamination in composite structures such as x-radiography, ultrasonic testing, and thermal/infrared inspection. These methods are expensive and hard to use for on line detection. Acoustic emission testing can monitor the material under test even under the presence of noise generated under load. It has been used extensively in proof-testing of fiberglass pressure vessels and beams. In the present work, experimental studies are conducted to investigate the use of broadband acoustic emission signatures to detect delaminations in composite beams. Glass/epoxy beam specimens with full width, prescribed delamination sizes of 2 inches and 4 inches are investigated. The prescribed delamination is produced by inserting Teflon film between laminae during the fabrication of composite laminate. The objectives of this research is to develop a method for predicting delamination size and location in laminated composite beams by combining smart materials concept and broadband AE analysis techniques. More specifically, a piezoceramic (PZT) patch is bonded on the surface of composite beams and used as a pulser. The piezoceramic patch simulates the AE wave source as a 3 cycles, 50KHz, burst sine wave. One broadband AE sensor is fixed near the PZT patch to measure the AE wave near the AE source. A second broadband AE sensor, which is used as a receiver, is scanned along the composite beams at 0.25 inch step to measure propagation of AE wave along the composite beams. The acquired AE waveform is digitized and processed. Signal strength, signal energy, cross-correlation of AE waveforms, and tracking of specific cycle of AE waveforms are used to detect delamination size and location.

Okafor, A. C.↗

Test and Analysis of the 8-foot Diameter Cylindrical Sandwich Composite Test Article CTA8.2B: As part of the NASA Engineering and Safety Center Shell Buckling Knockdown Factor Project

The buckling response of thin-walled cylindrical structures have long been shown to be sensitive to various imperfections. That is, imperfections related to load introduction, boundary conditions, material property variation, and geometric deviations can all contribute to experimentally obtained buckling loads being lower than the buckling loads predicted for perfect representations of the same thin-walled cylindrical structure. To account for the influence of geometry-based imperfections of a thin-walled cylindrical structure on buckling response, a design factor (also known as a buckling knockdown factor) is used during the design phase. Guidelines for buckling knockdown factors are readily available in NASA SP-8007, Buckling of Thin Walled Circular Cylinders, which was updated in 2020. Prior to this recent update, NASA SP-8007 had not been updated since 1969, and since that time, computational analysis, experimental testing, and manufacturing methods have significantly improved. The NASA Engineering and Safety Center (NESC) Shell Buckling Knockdown Factor Project (SBKF, NESC Assessment 07-010-E) had the goal of developing buckling design recommendations for select classes of metallic and composite launch-vehicle structures [3]. Specifically, the test and analysis results from the fourth SBKF composite test article SBKF-P3-CYL-CTA8.2B, which is referred to as CTA8.2B, are described in this paper. This test was the fourth in a series of four tests on sandwich composite cylinders that will be used to experimentally validate analysis methods, which in turn can be used to develop new analysis-based shell buckling design guidelines for typical sandwich composite launch vehicle cylindrical structures. Publications describing previous test validation with analysis are available in Refs. CTA8.2B was designed to occupy one corner of the design space with approximately equal bending stiffnesses in the axial and transverse directions and have a larger ratio of radius to effective shell thickness. Each test article had a unique design and was designed to occupy a specific region of the design space. CTA8.2B was an 8-foot diameter honeycomb-core sandwich cylinder that was fabricated and tested at the NASA Marshall Space Flight Center (MSFC). The primary objectives of this test were to interrogate the structural capability of a composite test article, and to verify the test article design and analysis approach for cylinders subjected to axial compression and combined axial and bending loads. First, descriptions of the test article design and test are given in Section 2.0, and modeling and analysis methods used in support of the test article design and testing activities are described briefly in Section 3.0. Then, select test results are presented and compared to predicted results in Section 4.0, and concluding remarks are presented in Section 5.0. Finally, drawings of CTA8.2B and references used to support the test and analysis are provided in the Appendix.

Nonlinear analysis↗

Ground test experience with large composite structures for commercial transports

The initial ground test of each component resulted in structural failure at less than ultimate design loads. While such failures represent major program delays, the investigation and analysis of each failure revealed significant lessons for effective utilization of composites in primary structure. Foremost among these are secondary loads that produce through-the-thickness forces which may lead to serious weaknesses in an otherwise sound structural design. The sources, magnitude, and effects of secondary loads need to be thoroughly understood and accounted for by the designers of composite primary aircraft structures.

Bohon, H. L.↗

Ground test experience with large composite structures for commercial transports

The initial ground test of each component resulted in structural failure at less than ultimate design loads. While such failures represent major program delays, the investigation and analysis of each failure revealed significant lessons for effective utilization of composites in primary structure. Foremost among these are secondary loads that produce through-the-thickness forces which may lead to serious weaknesses in an otherwise sound structural design. The sources, magnitude, and effects of secondary loads need to be thoroughly understood and accounted for by the designers of composite primary aircraft structures.

Bohon, H. L.↗

Testing of Composite Laminate Specimens with Mid-Length Lateral Notches

Eight fiber-reinforced, carbon-epoxy composite laminate specimens without external stiffeners (unstiffened) were loaded to failure to determine their failure load and mode under the Advanced Composites Project (ACP) Rapid Design Tools activity. Each specimen contained a lateral notch located at the mid-length location. A description of the specimens, instrumentation, test fixtures and procedures is presented, followed by the presentation of the experimental results.

Dawn C Jegley↗

Composite Materials Characterization and Development at AFWAL

The development of test methodology for characterizing matrix dominated failure modes is discussed emphasizing issues of matrix cracking, delamination under static loading, and the relationship of composite properties to matrix properties. Both strength characterization and classical techniques of linear elastic fracture mechanics were examined. Materials development studies are also discussed. Major areas of interest include acetylene-terminated and bismaleimide resins for 350 to 450 deg use, thermoplastics development, and failure resistant composite concepts.

Browning, C. E.↗

Loading rate effect on interlaminar fracture toughness of a thermoplastic composite

A study was undertaken to investigate the loading rate effect on delamination fracture initiation toughness of a thermoplastic composite. For this purpose, double cantilever beam specimens of graphite/PEEK were tested in a displacement controlled mode using an Instron tensile test machine. Specimens were loaded at various crosshead speeds ranging from 0.05 cm/min to 100 cm/min. The interlaminar fracture toughness was found to decrease with increasing loading rate, and this decrease was more than one hundred percent over the five decades of loading rate employed.

Mall, S.↗

Advances in cryogenic foam insulations.

Description of a discretely oriented thread-reinforced polyurethane foam thermal insulation system for liquid hydrogen fuel tanks. The 3-D foam and glass liner composite is designed to be adhesively bonded to the inside surface of the tank wall and to be in direct contact with liquid hydrogen. All elements of this insulation composite are capable of sustaining the loads and environmental conditions imposed by testing under simulated Space Shuttle vehicle requirements at temperatures between -423 and +350 F.

Lemons, C. R.↗

Research on graphite reinforced glass matrix composites

High levels of mechanical performance in tension, flexure, fatigue, and creep loading situations of graphite fiber reinforced glass matrix composites are discussed. At test temperatures of up to 813 K it was found that the major limiting factor was the oxidative instability of the reinforcing graphite fibers. Particular points to note include the following: (1) a wide variety of graphite fibers were found to be comparable with the glass matrix composite fabrication process; (2) choice of fiber, to a large extent, controlled resultant composite performance; (3) composite fatigue performance was found to be excellent at both 300 K and 703 K; (4) composite creep and stress rupture at temperatures of up to 813 K was limited by the oxidative stability of the fiber; (5) exceptionally low values of composite thermal expansion coefficient were attributable to the dimensional stability of both matrix and fiber; and (6) component fabricability was demonstrated through the hot pressing of hot sections and brazing using glass and metal joining phases.

Prewo, K. M.↗

A ceramic nozzle for the NASA-Langley 2.4-m /8.0-ft/ high temperature structures tunnel

Two materials, a refractory castable ceramic and a SiO2-SiO2 composite, were fabricated as nozzle inserts for the Langley Research Center's 2.4-m (8.0-ft) high temperature structures tunnel. The high pressure and intense heat of the CH4-air products of the combustion-gas stream limits the materials that can be used in this tunnel. The castable-ceramic material showed good resistance to erosion and the thermal loads imposed on it by the gas stream but failed in tension when subjected to high hoop stresses. The SiO2-SiO2-composite nozzle insert withstood the thermomechanical loads but eroded unacceptably with increasing test temperature and pressure.

Buckley, J. D.↗

Testing Machine for Biaxial Loading

Standard tensile-testing machine applies bending and tension simultaneously. Biaxial-loading test machine created by adding two test fixtures to commercial tensile-testing machine. Bending moment applied by substrate-deformation fixture comprising yoke and anvil block. Pneumatic tension-load fixture pulls up on bracket attached to top surface of specimen. Tension and deflection measured with transducers. Modified test apparatus originally developed to load-test Space Shuttle surface-insulation tiles and particuarly important for composite structures.

Demonet, R. J.↗

Compression failure mechanisms of uni-ply composite plates with a circular cutout

The effect of circular-hole size on the failure mode of uniply graphite-epoxy composite plates is investigated experimentally and analytically for uniaxial compressive loading. The test specimens are sandwiched between polyetherimide plastic for nondestructive evaluations of the uniply failure mechanisms associated with a range of hole sizes. Finite-element modeling based on classical lamination theory is conducted for the corresponding materials and geometries to reproduce the experimental results analytically. The type of compressive failure is found to be a function of hole size, with fiber buckling/kinking at the hole being the dominant failure mechanism for hole diam/plate width ratios exceeding 0.062. The results of the finite-element analysis supported the experimental data for these failure mechanisms and for those corresponding to smaller hole sizes.

Khamseh, A. R.↗