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At least 289 records · Page 16

Brighter-fatter Effect in Near-infrared Detectors—III. Fourier-domain Treatment of Flat Field Correlations and Application to WFIRST

Weak gravitational lensing has emerged as a leading probe of the growth of cosmic structure. However, the shear signal is very small and accurate measurement depends critically on our ability to understand how non-ideal instrumental effects affect astronomical images. The Wide-Field Infrared Survey Telescope (WFIRST) will fly a focal plane containing 18 Teledyne H4RG-10 near-infrared detector arrays, which present different instrument calibration challenges from previous weak lensing observations. Previous work [Paper I: Hirata & Choi, PASP, 132, 014501 (2020); and Paper II: Choi & Hirata, PASP, 132, 014502 (2020)] has shown that correlation functions of flat field images, including cross-correlations between different time slices that are enabled by the non-destructive read capability of the infrared detectors, are effective tools for disentangling linear and nonlinear inter-pixel capacitance (IPC) and the brighter-fatter effect (BFE). Here we present a Fourier-domain treatment of the flat field correlations, which allows us to expand the previous formalism to all orders in IPC, BFE, and classical nonlinearity. We show that biases in simulated flat field analyses in Paper I are greatly reduced through the use of this formalism. We then apply this updated formalism to flat field data from three WFIRST flight candidate detectors, and explore the robustness to variations in the analysis. We find that the BFE is present in all three detectors, and that its contribution to the flat field correlations dominates over the nonlinear IPC, in accordance with the results from Paper II on a development detector. The magnitude of the BFE is such that the effective area of a pixel is increased by (3.54 ± 0.03) × 10 -7 for every electron deposited in a neighboring pixel (sensor chip assembly [SCA] 20829, statistical error, not IPC-deconvolved). We compare IPC maps from flat field autocorrelation measurements to those obtained from the single pixel reset method and find a median difference of 0.113% for SCA 20829. After further diagnosis of this difference, we ascribe it largely to an additional source of cross-talk, the vertical trailing pixel effect, and recommend further work to develop a model for this effect. These results represent a significant step toward calibration of the non-ideal effects in WFIRST detectors.

79 ASTRONOMY AND ASTROPHYSICS↗

ExoReL{sup R}: A Bayesian Inverse Retrieval Framework for Exoplanetary Reflected Light Spectra

The high-contrast imaging technique is meant to provide insight into those planets orbiting several astronomical units from their host star. Space missions such as Wide-Field InfraRed Survey Telescope, Habitable Exoplanet Imaging Mission, and Large Ultra-Violet/Optical/InfraRed Surveyor will measure reflected light spectra of cold gaseous and rocky planets. To interpret these observations, we introduce ExoReL{sup R} (Exoplanetary Reflected Light Retrieval), a novel Bayesian retrieval framework to retrieve cloud properties and atmospheric structures from exoplanetary reflected light spectra. As a unique feature, it assumes a vertically nonuniform volume mixing ratio (VMR) profile of water and ammonia, and uses it to construct cloud densities. In this way, clouds and molecular mixture ratios are consistent. We apply ExoReL{sup R} on three test cases: two exoplanets (υ And e and 47 Uma b) and Jupiter. We show that we are able to retrieve the concentration of methane in the atmosphere, and estimate the position of clouds when the signal-to-noise ratio of the spectrum is higher than 15, in line with previous works. Moreover, we described the ability of our model to give a chemical identity to clouds, and we discussed whether or not we can observe this difference in the planetary reflection spectrum. Finally, we demonstrate how it could be possible to retrieve molecular concentrations (water and ammonia in this work) below the clouds by linking the nonuniform VMR profile to the cloud presence. This will help to constrain the concentration of water and ammonia unseen in direct measurements.

79 ASTRONOMY AND ASTROPHYSICS↗

Heat Flux Analysis From IR Imaging on Proto-MPEX

The Prototype Material Plasma Exposure eXperiment (Proto-MPEX) is a linear device used to develop the source and heating concept for MPEX, an experiment to study plasma–material interactions for future fusion reactors. This paper highlights recent analysis and results on Proto-MPEX using an infrared (IR) camera, a key tool for imaging heat fluxes measured at the material target. The target heat fluxes are crucial to understanding the source and heating concepts. The recent analysis includes the application of homography and 3-D finite-element methods to provide between-shot measurements of the 2-D target heat flux profile. The IR camera inferred heat flux is shown to correlate with Langmuir probe inferred heat fluxes for a range of parameters in helicon only and helicon + electron cyclotron heated discharges. Results show both desirable central and undesirable edge heat flux for helicon source and electron heating on the target. These heat flux measurements are shown to be important for better understanding of the source and heating physics.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

End–to–End Metasurface Design for Temperature Imaging via Broadband Planck‐Radiation Regression

A theoretical framework is presented for temperature imaging from long-wavelength infrared (LWIR) thermal radiation (e.g., 8–12 µm) through the end-to-end design of a metasurface-optics frontend and a computational-reconstruction backend. A new nonlinear reconstruction algorithm, “Planck regression”, is introduced to reconstruct the temperature map from a gray scale sensor image, even in the presence of severe chromatic aberration, by exploiting black body and optical physics particular to thermal imaging. This algorithm is combined with an end-to-end approach that optimizes manufacturable, single-layer metasurfaces to yield the most accurate reconstruction. The designs demonstrate high-quality, noise-robust reconstructions of arbitrary temperature maps (including completely random images) in simulations of an ultra-compact thermal-imaging device. Here, it is also shown that Planck regression is much more generalizable to arbitrary images than a straightforward neural-network reconstruction, which requires a large training set of domain-specific images.

36 MATERIALS SCIENCE↗

SCExAO/CHARIS Near-infrared Integral Field Spectroscopy of the HD 15115 Debris Disk

We present new, near-infrared (1.1–2.4 μm) high-contrast imaging of the debris disk around HD 15115 with the Subaru Coronagraphic Extreme Adaptive Optics (SCExAO) system coupled with the Coronagraphic High Angular Resolution Imaging Spectrograph (CHARIS). The SCExAO/CHARIS resolves the disk down to ρ ∼ 0.″2 (r {sub proj} ∼ 10 au), a factor of ∼3–5 smaller than previous recent studies. We derive a disk position angle of PA ∼ 279.°4–280.°5 and an inclination of i ∼ 85.°3–86.2.°. While recent SPHERE/IRDIS imagery of the system could suggest a significantly misaligned two-ring disk geometry, CHARIS imagery does not reveal conclusive evidence for this hypothesis. Moreover, optimizing models of both one- and two-ring geometries using differential evolution, we find that a single ring having a Hong-like scattering phase function matches the data equally well within the CHARIS field of view (ρ ≲ 1″). The disk’s asymmetry, well evidenced at larger separations, is also recovered; the west side of the disk appears, on average, around 0.4 mag brighter across the CHARIS bandpass between 0.″25 and 1″. Comparing Space Telescope Imaging Spectrograph (STIS) 50CCD optical photometry (2000–10500 Å) with CHARIS near-infrared photometry, we find a red (STIS/50CCD−CHARIS broadband) color for both sides of the disk throughout the 0.″4–1″ region of overlap, in contrast to the blue color reported at similar wavelengths for regions exterior to ∼2″. Further, this color may suggest a smaller minimum grain size than previously estimated at larger separations. Finally, we provide constraints on planetary companions and discuss possible mechanisms for the observed inner disk flux asymmetry and color.

79 ASTRONOMY AND ASTROPHYSICS↗

Automated bubble analysis of high-speed subcooled flow boiling images using U-net transfer learning and global optical flow

Capturing and analyzing the bubble dynamics is crucial to improving the understanding of boiling heat transfer mechanisms and predicting boiling heat transfer coefficient and boiling crisis. High speed video (HSV) imaging has been used for decades towards this end. Still, there is no universal approach to quantitatively analyze bubble dynamics from HSV images. In this study, we propose a data-driven post-processing approach to segment, track, and identify wall-attached vapor bubbles from HSV images of the boiling process in subcooled flow conditions. Firstly, we employ a transfer learning framework with a U-Net-based convolution neural network (CNN) architecture to detect and segment bubbles in HSV images of diverse contrast and surface texture using very little data (e.g., 10 images) for training. Then, we evaluate the trained CNN model with 100 ground-truth images, and the validation results show that the model accuracy and precision in detecting the optical footprint of bubbles are higher than 90%. Finally, we suggest a criterion to identify a condensing bubble based on the divergence of the bubble displacement, which is calculated from sequential segmented bubble images using a global optical flow code. Using this combination of machine learning and optical flow, we can identify nucleation sites and track the growth of bubbles nucleating at each site to quantify nucleation site density, nucleation frequency, and other fundamental boiling parameters. The proposed system is validated using results obtained on a special heater, which enables both infrared (IR) thermometry and HSV imaging on a metallic surface. We compare the fundamental boiling parameters obtained by the two different diagnostics. The results show good agreement. In conclusion, the difference between the measurements of nucleation site density, averaged nucleation frequency, and averaged growth time performed with the two techniques is always within ± 20% and mostly ± 10% of the values measured with IR thermometry.

42 ENGINEERING↗

Depth Thermography: Noninvasive 3D Temperature Profiling Using Infrared Thermal Emission

Here, we introduce a technique based on infrared thermal emission, termed depth thermography, that can remotely measure the temperature distribution beneath the surface of certain objects. Depth thermography utilizes the thermal-emission spectrum in the semitransparent spectral region of the target object to extract its temperature as a function of depth, in contrast with conventional thermography, which uses the spectrally integrated thermally emitted power to measure the surface temperature. Coupled with two-dimensional imaging, for example using an infrared hyperspectral camera or scanning a single-pixel spectrometer, this technique can yield volumetric temperature distributions. Furthermore, we carried out a proof-of-concept experiment on an asymmetrically heated fused-silica window, extracting the temperature distribution throughout the sample. Depth thermography may enable noncontact volumetric temperature measurements of microscopic objects such as multilayer electronic devices or macroscopic volumes of liquids and gases, as well as simultaneous all-optical measurements of optical and thermal properties of materials.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

202508 HAIIC IR Images with Attitude Data at BNF

This campaign aims to collect infrared imagery using a custom data acquisition system to improve and validate a previously developed attitude estimation algorithm, with a focus on ensuring reliable performance at higher altitudes. The system integrates a Boson+320 infrared camera, a VN-200 IMU for recording attitude data synchronized with image acquisition, and a Raspberry Pi 4B+ for onboard processing and storage. Image orientation was controlled using a Gremsy T7 gimbal. The primary dataset spans roll angles from −40° to 40° and pitch angles from −20° to 40°, sampled at 1° increments. Additional, smaller datasets were also collected at 2.5° angular intervals.

Boson+320↗

Laboratory Heat Flux Estimates of Seawater Foam for Low Wind Speeds

Laboratory experiments were conducted to measure the heat flux from seafoam continuously generated in natural seawater. Using a control volume technique, heat flux was calculated from foam and foam-free surfaces as a function of ambient humidity (ranged from 40% to 78%), air–water temperature difference (ranged from -9 °C to 0 °C), and wind speed (variable up to 3 m s-1). Water-surface skin temperature was imaged with a calibrated thermal infrared camera, and near-surface temperature profiles in the air, water, and foam were recorded. Net heat flux from foam surfaces increased with increasing wind speed and was shown to be up to four times greater than a foam-free surface. The fraction of the total heat flux due to the latent heat flux was observed for foam to be 0.75, with this value being relatively constant with wind speed. In contrast, for a foam-free surface the fraction of the total heat flux due to the latent heat flux decreased at higher wind speeds. Temperature profiles through foam are linear and have larger gradients, which increased with wind speed, while foam free surfaces show the expected logarithmic profile and show no variation with temperature. The radiometric surface temperatures show that foam is cooler and more variable than a foam-free surface, and bubble-resolving thermal images show that radiometrically transparent bubble caps and burst bubbles reveal warm foam below the cool surface layer, contributing to the enhanced variability.

54 ENVIRONMENTAL SCIENCES↗

Photoionization and Photofragmentation Dynamics of I 2 in Intense Laser Fields: A Velocity-Map Imaging Study

The photoionization and photofragmentation dynamics of I 2 in intense femtosecond near-infrared laser fields were studied using velocity-map imaging of cations, electrons, and anions. A series of photofragmentation pathways originating from different cationic electronic states were observed following single ionization, leading to I + fragments with distinct kinetic energies, which could not be resolved in previous studies. Photoelectron spectra indicate that these high-lying dissociative states are primarily produced through nonresonant ionization from several molecular orbitals (MO) of the neutral. The photoelectron spectra also show clear signatures of resonant ionization pathways (Freeman resonances) to low-lying bound ionic states via Rydberg states of the neutral moiety. To investigate the role of these Rydberg states further, we imaged anionic products (I – ) formed through ion-pair dissociations of neutral molecules excited to these Rydberg states by the intense femtosecond laser pulse. Collectively, these results shed significant new light on the complex dynamics of I 2 molecules in intense laser fields and on the important role of neutral Rydberg states in a full description of strong-field phenomena in molecules.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

Probing nanoparticle substrate interactions with synchrotron infrared nanospectroscopy: Coupling gold nanorod Fabry-Pérot resonances with SiO 2 and $h$-BN phonons

Spectroscopic interrogation of materials in the midinfrared with nanometer spatial resolution is inherently difficult due to the long wavelengths involved, reduced detector efficiencies, and limited availability of spectrally bright, coherent light sources. Technological advances are driving techniques that overcome these challenges, enabling material characterization in this relatively unexplored spectral regime. Synchrotron infrared nanospectroscopy (SINS) is an imaging technique that provides local sample information of nanoscale target specimens in an experimental energy window between 330 and 5000 cm -1 . Here, using SINS, we analyzed a series of individual gold nanorods patterned on a SiO 2 substrate and on a flake of hexagonal boron nitride. The SINS spectra reveal interactions between the nanorod photonic Fabry-Pérot resonances and the surface phonon polaritons of each substrate, which are characterized as avoided crossings. A coupled oscillator model of the hybrid system provides a deeper understanding of the coupling and provides a theoretical framework for future exploration.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

Capillary-Enhanced Two-Phase Micro-Cooler Using Copper-Inverse-Opal Wick with Silicon Microchannel Manifold for High-Heat-Flux Cooling Application

In this work, we demonstrate a two-phase capillary-fed boiling micro-cooler that consists of a ~ 25-..mu..m-thick copper inverse opal (CIO) porous wicking structure for high-heat-flux boiling and a silicon 3D-manifold for distributed liquid delivery and vapor extraction across a 0.5 cm x 0.5 cm heated area. At low inlet water mass flow rates of 1.5 to 1.9 g(min)-1, the micro-cooler displays nearly two-phase boiling with exit vapor quality ~ 1 and a high critical heat flux (CHF) of 253 to 320 W cm-2 with low superheat of ~ 10 degrees C resulting in a thermal resistance of boiling ~ 0.025 cm2 degrees C W-1 or heat transfer coefficient of 0.4 MW m-2 degrees C-1. For higher flow rates of 5, 10, and 15 g(min)-1, the micro-cooler exhibits a hybrid single-phase and two-phase cooling regime where the contribution of the sensible heat (single-phase) cooling is linearly added to that of the two-phase cooling. For the highest flow rate of 15 g(min)-1, the CHF is increased to ~ 500 W cm-2 resulting in an overall thermal resistance of ~ 0.18 cm2 degrees C W-1. However, the two-phase heat transfer effectiveness, which estimates the utilization level of the inlet mass flow rate for two-phase boiling, is reduced to ~ 0.11. To achieve the best cooling system performances, the micro-cooler must operate entirely within the two-phase boiling regime (exit vapor quality or two-phase heat transfer effectiveness ~ 1). Ideally, the "coolant" should be delivered near its saturation temperature (~ 100 degrees C for water), which provides significant advantages for the energy-efficient operation of data centers and power electronics. We present detailed analysis with Infrared and high speed camera images at various inlet flow rates and heat fluxes to understand complex heat transfer in the micro-cooler. Furthermore, a conjugate thermofluidic simulation model, which incorporates the physics of capillary-fed boiling in a porous copper layer, agrees well with the experimental data.

capillary-enhanced boiling↗

A Co-Registered In-Situ and Ex-Situ Dataset from an Electron Beam Powder Bed Fusion Additive Manufacturing Process (Peregrine v2023-09)

This release contains a co-registered in-situ and ex-situ Peregrine dataset from a single Arcam Q10 Electron Beam Powder Bed Fusion (EB-PBF) Inconel 738 build. These data were collected at the Manufacturing Demonstration Facility (MDF) located at Oak Ridge National Laboratory (ORNL). The dataset includes layer-wise Near Infrared (NIR) in-situ imaging data, in-situ temporal sensor data, ex-situ X-Ray Computed Tomography (X-CT) scans, and the target part geometries. Additionally, anomaly detections produced by a trained Dynamic Segmentation Convolutional Neural Network (DSCNN) are provided.

36 MATERIALS SCIENCE↗

Spinning metasurface stack for spectro-polarimetric thermal imaging

Spectro-polarimetric imaging in the long-wave infrared (LWIR) region plays a crucial role in applications from night vision and machine perception to trace gas sensing and thermography. However, the current generation of spectro-polarimetric LWIR imagers suffers from limitations in size, spectral resolution, and field of view (FOV). While meta-optics-based strategies for spectro-polarimetric imaging have been explored in the visible spectrum, their potential for thermal imaging remains largely unexplored. In this work, we introduce an approach for spectro-polarimetric decomposition by combining large-area stacked meta-optical devices with advanced computational imaging algorithms. The co-design of a stack of spinning dispersive metasurfaces along with compressive sensing and dictionary learning algorithms allows simultaneous spectral and polarimetric resolution without the need for bulky filter wheels or interferometers. Our spinning-metasurface-based spectro-polarimetric stack is compact (<10×10×10cm) and robust, and it offers a wide field of view (20.5°). We show that the spectral resolving power of our system substantially enhances performance in machine learning tasks such as material classification, a challenge for conventional panchromatic thermal cameras. Our approach represents a significant advance in the field of thermal imaging for a wide range of applications including heat-assisted detection and ranging (HADAR).

Optics↗

Deriving the Infrared Complex Refractive Indices of Organic Powders for Optical Modeling: Comparison of Methods

Identification of solids via infrared reflection spectroscopy requires a spectral library of all solids likely to be encountered. A confounding factor in populating such a spectral library is that the reflectance spectra of solids vary with their form, including particle size, film thickness, and substrate. To reduce the efforts of experimentally constructing such a library, an alternate strategy is to use the wavelength-dependent optical constants, n and k, of a solid to calculate a series of reflectance spectra corresponding to each scenario or morphology. Because most n/k measurements are best performed on mm-sized crystals, however, the challenge of determining the optical constants increases when a solid is only readily available as a powder, as is often the case. Some organic solids, such as caffeine, are both unavailable in large crystals and difficult to press into pellets. In this study, the infrared optical constants, or complex refractive indices, of caffeine were determined using three different methods: single-angle reflectance, infrared spectroscopic ellipsometry, and quantitative absorbance measurements of KBr pellets. The n and k values derived through each method were used to model the hyperspectral imaging reflectance spectrum of a caffeine film on a steel planchet. Over 1,110 – 870 cm-1, the single-angle reflectance-derived n and k had the best correlation with the experimental spectrum. These results suggest different organic solids may require different methods to determine the most accurate infrared complex refractive indices for synthetic spectral libraries.

FTIR, hyperspectral imaging, infrared, infrared (I↗

Thermal Image Processing for Feature Extraction from Encapsulated Phase Change Materials

Encapsulated inorganic particles with high melting points (>300 °C) are desired as high-temperature Phase Change Materials (PCMs) for next-generation Latent Heat Thermal Energy Storage (LHTES) systems. One of the many challenges during the development of PCMs is to achieve a high throughput that in turn depends on accurately modeling the relation between process parameters and geometric & thermal properties of the PCMs particle. During the production of the PCMs, a high-speed infrared camera is used to acquire images of the encapsulated material under controlled illumination conditions. This research article focuses on the development of image processing techniques for both geometric and thermal feature extraction during the development of the PCMs. A user-friendly GUI has been designed in MATLAB and preliminary experimental results have demonstrated that the method is fast, accurate and reliable for a high throughput production. The extracted features will be used to develop Machine Learning (ML) models to predict the geometric and thermal properties of the PCM based on the process parameter settings. The ML model will accelerate the search for the optimized process settings to boost the throughput of the production.

25 ENERGY STORAGE↗

Airborne hyperspectral imaging of nitrogen deficiency on crop traits and yield of maize by machine learning and radiative transfer modeling

Nitrogen is an essential nutrient that directly affects plant photosynthesis, crop yield, and biomass production for bioenergy crops, but excessive application of nitrogen fertilizers can cause environmental degradation. To achieve sustainable nitrogen fertilizer management for precision agriculture, there is an urgent need for nondestructive and high spatial resolution monitoring of crop nitrogen and its allocation to photosynthetic proteins as that changes over time. Here, we used visible to shortwave infrared (400–2400 nm) airborne hyperspectral imaging with high spatial (0.5 m) and spectral (3–5 nm) resolutions to accurately estimate critical crop traits, i.e., nitrogen, chlorophyll, and photosynthetic capacity (CO 2 -saturated photosynthesis rate, V max,27 ), at leaf and canopy scales, and to assess nitrogen deficiency on crop yield. We conducted three airborne campaigns over a maize (Zea mays L.) field during the growing season of 2019. Physically based soil-canopy Radiative Transfer Modeling (RTM) and data-driven approaches i.e. Partial-Least Squares Regression (PLSR) were used to retrieve crop traits from hyperspectral reflectance, with ground truth of leaf nitrogen, chlorophyll, V max,27 , Leaf Area Index (LAI), and harvested grain yield. To improve computational efficiency of RTMs, Random Forest (RF) was used to mimic RTM simulations to generate machine learning surrogate models RTM-RF. The results show that prior knowledge of soil background and leaf angle distribution can significantly reduce the ill-posed RTM retrieval. RTM-RF achieved a high accuracy to predict leaf chlorophyll content (R 2 = 0.73) and LAI (R 2 = 0.75). Meanwhile, PLSR exhibited better accuracy to predict leaf chlorophyll content (R 2 = 0.79), nitrogen concentration (R 2 = 0.83), nitrogen content (R 2 = 0.77), and V max,27 (R 2 = 0.69) but required measured traits for model training. We also found that canopy structure signals can enhance the use of spectral data to predict nitrogen related photosynthetic traits, as combining RTM-RF LAI and PLSR leaf traits well predicted canopy-level traits (leaf traits × LAI) including canopy chlorophyll (R 2 = 0.80), nitrogen (R 2 = 0.85) and V max,27 (R 2 = 0.82). Compared to leaf traits, we further found that canopy-level photosynthetic traits, particularly canopy V max,27 , have higher correlation with maize grain yield. This study highlights the potential for synergistic use of process-based and data-driven approaches of hyperspectral imaging to quantify crop traits that facilitate precision agricultural management to secure food and bioenergy production.

54 ENVIRONMENTAL SCIENCES↗

Cancer cell membrane-coated rare earth doped nanoparticles for tumor surgery navigation in NIR-II imaging window

With the attractive characteristics of low toxicity, narrow emission spectra, long fluorescence lifetime, and no photobleaching, rare-earth doped nanoparticles (RENPs) have become promising imaging nanoplatforms in the second near-infrared window (NIR-II, 1000–1700 nm). Many studies have been devoted to different surface modification strategies of RENPs to achieve good NIR-II tumor imaging property. However, the tumor imaging efficiency of these approaches remains disappointing. Herein, two methods were pursued to modify RENPs with either polyethylene glycol (PEG) or cancer-cell-membrane to generate PEGylated-RENPs and cancer-cell-membrane camouflaged RENPs (CC-RENPs), respectively. Furthermore, this study demonstrated that cancer-cell-membrane coating of RENPs greatly improved tumor imaging performance in NIR-II window than PEG coating. Besides, CC-RENPs uptakes in liver and spleen significantly decreased. Importantly, CC-RENPs was found to be capable to aid us to pursue precise resection of the tumor. In conclusion, CC-RENPs are capable of targeting tumors and show high tumor NIR-II imaging quality. They are highly promising nanomaterials for future medical applications.

62 RADIOLOGY AND NUCLEAR MEDICINE↗