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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 289 records · Page 16
All sourcesNASA NTRSDOE OSTI
DOE OSTI2023

Distributed fiber-optic sensor network for sensing the corrosion onset and quantification

Materials, methods of making, and methods of sensing liquid droplets with high spatial resolution as a signature of the on-set of corrosion using a hierarchical sensor network A hierarchical sensor network for sensing liquid droplets with high spatial resolution as a signature of the on-set of corrosion, including an interrogation system; and an intermediate sensor array layer in communication with the interrogation system. The network includes an interrogation system and an intermediate sensor array layer in communication with the interrogation system.

Ohodnicki, Paul R.↗
NASA NTRS2018

A Novel Sensing Tether for Rovers

Luna has extended the length of its fiber optic shape sensing technology out to a continuous, high-fidelity measurement of a 100-meter sensor, creating a novel concept for a self-monitoring tether for robotic exploration. This tether is capable of measuring its own tension, curvature, and full 3-D shape along its entire length as it is deployed by a robotic rover. Using Optical Frequency Domain Reflectometry (OFDR) and the Rayleigh scatter signature to sense the state of a customized multicore optical fiber, the new technology is lightweight, compact, and immune to electromagnetic interference. Results are presented from tests with a 50-meter tether on the Axel Rover at JPL’s Mars Yard testing ground.

Kominsky, Daniel↗
DOE OSTI2025

Novel High Resolution High Temperature In-Line Sensors for Steel Manufacturing

To support efficiency, productivity, yield improvements, and future industry 4.0 and SMART manufacturing objectives for a competitive and prosperous steel industry, this program has embarked on an effort to develop, demonstrate and deploy several novel sensing technologies based on fiber optics for use in production steel facilities. Over the duration of this program, our team has successfully demonstrated three of these technologies: (1) near continuous Rayliegh Scattering optical frequency domain reflectometry (OFDR) sensing with single mode silica fibers for temperature sensing to 700 C, (2) semi-distributed fiber Bragg grating (FBG) sensing with multimode sapphire fibers for temperature sensing to >1600 C, and (3) remote in-situ Raman analysis for slag and flux chemistry analysis at steelmaking temperatures >1550 C. Each of these sensor and interrogation systems was developed, refined, and tested in our labs at Missouri S&T and then successfully deployed at SSAB’s production facilities at two sites, one in Montpelier, IA and one in Mobile, AL.

36 MATERIALS SCIENCE↗
DOE OSTI2021

Passive sensing of a microparticle modified hybrid, fiber-reinforced composite

The widespread commercial adoption of high-performance, fiber-reinforced composites has pushed research interests toward the next generation of composites. These new composites are tasked with integrating additional functionalities into the structures without causing a trade-off in mechanical performance. One such functionality that has received significant interest is sensing. This is especially important for composites using high-performance fibers (e.g., carbon fiber) because their strain-to-failure is relatively low, resulting in brittle fracture. Besides, fiber damage can be hidden within the composite, potentially leading to premature catastrophic failure if not detected. In prior research, we demonstrated continuous feed-through deposition of ceramic nanoparticles on carbon fiber’s surface that simultaneously enhanced both the piezoresistive response and interlaminar shear strength. In this work, a similar continuous feed-through deposition process was used to demonstrate passive sensing and energy harvesting by integrating ferroelectric microparticles on the surface of electrically nonconductive fibers. The sensing and energy harvesting capabilities were characterized by mechanically straining composite beams and measuring the power generated. The improvements in mechanical properties are shown through interlaminar shear strength tests. Therefore, this research aims to demonstrate a high throughput, commercially scalable approach to coat fibers with ferroelectric microparticles that enable passive sensing as well as improved mechanical performance when fabricated into a fiber-reinforced composite.

Bowland, Christopher↗
NASA NTRS2001

Utilization of Infrared Fiber Optic in the Automotive Industry

Fiber optics are finding a place in the automotive industry. Illumination is the primary application today. Soon, however, fiber optics will be used for data communications and sensing applications. Silica fiber optics and plastic fibers are sufficient for illumination and communication applications however, sensing applications involving high temperature measurement and remote gas analysis would benefit from the use of infrared fiber optics. Chalcogonide and heavy metal fluoride glass optical fibers are two good candidates for these applications. Heavy metal fluoride optical fibers are being investigated by NASA for applications requiring transmission in the infrared portion of the electromagnetic spectrum. Zirconium-Barium-Lanthanum-Aluminum-Sodium-Fluoride (ZBLAN) is one such material which has been investigated. This material has a theoretical attenuation coefficient 100 times lower than that of silica and transmits into the mid-IR. However, the measured attenuation coefficient is higher than silica due to impurities and crystallization. Impurities can be taken care of by utilizing cleaner experimental protocol. It has been found that crystallization can be suppressed by processing in reduced gravity. Fibers processed in reduced gravity on the KC135 reduced gravity aircraft were found to be free of crystals while those processed on the ground were found to have crystals. These results will be presented along with plans for producing continuous lengths of ZBLAN optical fiber on board the International Space Station.

Tucker, Dennis S.↗
NASA NTRS2003

Simultaneous Temperature and Strain Sensing for Cryogenic Applications Using Dual-Wavelength Fiber Bragg Gratings

A new technique has been developed for sensing both temperature and strain simultaneously by using dual-wavelength fiber-optic Bragg gratings. Two Bragg gratings with different wavelengths were inscribed at the same location in an optical fiber to form a sensor. By measuring the wavelength shifts that resulted from the fiber being subjected to different temperatures and strains, the wavelength-dependent thermo-optic coefficients and photoelastic coefficients of the fiber were determined. This enables the simultaneous measurement of temperature and strain. In this study, measurements were made over the temperature range from room temperature down to about 10 K, addressing much of the low temperature range of cryogenic tanks. A structure transition of the optical fiber during the temperature change was found. This transition caused splitting of the waveforms characterizing the Bragg gratings, and the determination of wavelength shifts was consequently complicated. The effectiveness and sensitivities of these measurements in different temperature ranges are also discussed.

Wu, Meng-Chou↗
DOE OSTI2021

Fiber laser microphones with graphene diaphragms

An acoustic sensor comprises a sensing head comprising an optical fiber having a tip. A graphene diaphragm is disposed on the tip and is configured to vibrate in response to an acoustic signal. A fiber laser is optically coupled to the sensing head. The fiber laser comprises a first set of fiber Bragg gratings and a second set of fiber Bragg gratings. A gap is present between the first set and the second set of fiber Bragg gratings. The fiber laser is configured to generate a sensing optical signal having a first intensity in response to an excitation optical signal, the sensing optical signal impinging on the graphene diaphragm such that a feedback optical signal is reflected from the graphene diaphragm towards the fiber laser and has and has a second intensity modulated by the vibration of the graphene diaphragm that corresponds to the acoustic signal.

Liao, Shaolin↗
DOE OSTI2024

Embedded Fiber Optic Sensors in Structural Materials for Sensing in Extreme Environments

This slide deck presents the research results in embedding fiber optic sensors in structural materials. Fiber optic sensors were embedded in stainless steel and nickel via electric field assisted sintering. The embedded sensors were evaluated in terms of fiber integrity, fiber-matrix bonding, fiber functionality, mechanical properties, and machinability.

36 - MATERIALS SCIENCE↗
NASA NTRS2006

High-sensitivity cryogenic temperature sensors using pressurized fiber Bragg gratings

Cryogenic temperature sensing was studied using a pressurized fiber Bragg grating (PFBG). The PFBG was obtained by simply applying a small diametric load to a regular fiber Bragg grating (FBG), which was coated with polyimide of a thickness of 11 micrometers. The Bragg wavelength of the PFBG was measured at temperatures from 295 to 4.2 K. A pressure-induced transition occurred at 200 K during the cooling cycle. As a result the temperature sensitivity of the PFBG was found to be nonlinear but reach 24 pm/K below 200 K, more than three times the regular FBG. For the temperature change from 80 K to 10 K, the PFBG has a total Bragg wavelength shift of about 470 pm, 10 times more than the regular FBG. From room temperature to liquid helium temperature the PFBG gives a total wavelength shift of 3.78 nm, compared to the FBG of 1.51 nm. The effect of the coating thickness on the temperature sensitivity of the gratings is also discussed.

Wu, Meng-Chou↗
NASA NTRS2006

High-sensitivity Cryogenic Temperature Sensors using Pressurized Fiber Bragg Gratings

Cryogenic temperature sensing was studied using a pressurized fiber Bragg grating (PFBG). The PFBG was obtained by simply applying a small diametric load to a regular fiber Bragg grating (FBG), which was coated with polyimide of a thickness of 11 micrometers. The Bragg wavelength of the PFBG was measured at temperatures from 295 to 4.2 K. A pressure-induced transition occurred at 200 K during the cooling cycle. As a result the temperature sensitivity of the PFBG was found to be nonlinear but reach 24 pm/K below 200 K, more than three times the regular FBG. For the temperature change from 80 K to 10 K, the PFBG has a total Bragg wavelength shift of about 470 pm, 10 times more than the regular FBG. From room temperature to liquid helium temperature the PFBG gives a total wavelength shift of 3.78 nm, compared to the FBG of 1.51 nm. The effect of the coating thickness on the temperature sensitivity of the gratings is also discussed.

Wu, Meng-Chou↗
DOE OSTI2024

Portable fiber optic sensor for rare earth elements and other critical metals using photoluminescence methods

Rare earth elements and other metals are vital to a range of technologies that are used in the energy and defense sectors. However, monopolistic market conditions have caused significant concern over the stability of the critical metal supply chain, and this has spurred extensive efforts in many nations to produce these metals domestically, both from conventional sources such as mining and well as from unconventional sources such as coal and its utilization byproducts. Slow and expensive characterization methods pose a significant barrier for both metals prospecting and process monitoring. A promising solution to this challenge is the development of highly sensitive luminescent sensors for metals, which can offer low costs, portability, and sensitivity. Anionic zinc adeninate metal-organic frameworks (BioMOFs) are known to distinguishing and detect part-per-billion levels of terbium, europium, samarium, and dysprosium in water by sensitizing the narrow, element-specific emission bands from these lanthanides. Here, a BioMOF material is immobilized onto a large diameter, solarization-resistant fiber optic tip integrated with a portable, low-cost spectrometer for rare earth element sensing. Immobilizing the sensing material on fiber instead of dispersing the sensing material in solution offers several advantages: it facilitates solvent removal, which enhances luminescent signal from the sensitized lanthanides, and it also allows the BioMOF to be recycled for multiple uses. The sensing system was deployed on a simulated process stream and exhibited qualitative agreement with inductively-coupled plasma mass spectrometry for terbium and europium detection, highlighting the potential for the sensing system to be deployed for real-world applications. By using different sensing materials, the same portable sensor may be deployed to detect other energy relevant metals such as cobalt, providing a cost-effective and sensitive platform for critical metal characterization.

Crawford, Scott↗
NASA NTRS2020

Fiber-Optic Strain-Based Deflection and Twist Sensing for a High-Aspect-Ratio Swept Wing

Designs of aircraft structures have been moving toward leaner, lightweight designs for increased fuel efficiency. The Passive Aeroelastic Tailored (PAT) wing developed under the NASA Advanced Air Transport Technology (AATT) project is an example of a swept-wing design with high aspect ratio that incorporates lightweight highly-flexible tailored composite construction. The passive aeroelastic tailored structural design has explored the design space to enable aeroelastically tailored wing structures to increase aspect ratios (from 9 to 14) and ultimately reduce weight by 20 percent to 25 percent without impacting aeroelastic performance. To further study the aeroelastic performance of such a wing, the NASA Armstrong Flight Research Center (AFRC) (Edwards, California) has developed efficient real-time structural algorithms that are used in conjunction with a fiber-optic measurement system for lightweight vehicle applications. The AFRC Fiber Optic Sensing System (FOSS) provides up to 8,000 distributed surface strain measurements at one-half-inch increments and can be used to estimate a variety of structural parameters such as shape and load. This report discusses the implementation of strain-based displacement and twist-sensing techniques applied to the PAT wing test article tested at the NASA AFRC Flight Loads Laboratory. Empirical FOSS strain data are collected under varying loading conditions. Strain data are processed with the displacement and twist-sensing algorithms and independently verified by comparison to conventional ground-based instrumentation.

Pena, Francisco↗
DOE OSTI2022

A portable fiber optic sensor for the luminescent sensing of cobalt ions using carbon dots

Cobalt is critical to energy-relevant technologies, and demand for cobalt will increase significantly with growing global adoption of renewables. However, supply chain stability is threatened by economic and geopolitical factors, incentivizing domestic cobalt production from alternative resources such as coal, coal utilization byproducts (e.g., ash, acid mine drainage) and electronic waste. Rapid, inexpensive, and portable characterization techniques are needed to reduce production costs associated with cobalt prospecting and process monitoring. Here, in this research, we develop a compact, portable fiber optic luminescent probe for cobalt using phosphorus and nitrogen co-doped carbon dots as the sensing material. The carbon dot emission overlaps well with the cobalt absorption band at ~510 nm, leading to a selective decrease in emission as a function of cobalt concentration. The system responds nearly instantly to the presence of cobalt, with detection limits of 0.7 and 3.5 ppm in water and pH 1.68 buffer, respectively, providing comparable performance to a commercial spectrometer at a significantly lower cost. Moreover, the sensor is selective for cobalt in the presence of 13 of the most common metal ions encountered in coal utilization byproducts and is responsive to cobalt when spiked into an acid mine drainage leachate sample, highlighting the sensor's potential for real-world deployment in challenging matrices. In addition, integrating the carbon dots with a filter paper substrate produced ‘test strip’ sensors that exhibited a selective and sensitive visual response to cobalt using a handheld UV lamp. Taken together, the sensing system represents a significant step forward in the development of low-cost practical sensors for high-value metals in complex streams.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2023

Embedding of Fiber Optic Sensors in Stainless Steel for Sensing in Harsh Environments

Structural health monitoring is critical for components working in harsh environments to assess their safety and integrity. This can be realized with advanced sensors, such as fiber optic sensors, embedded in these components. Recent studies have used ultrasonic consolidation (UC) and laser-based additive manufacturing (AM) techniques to embed fiber optic sensors in metals. However, sensor embedding using these techniques has been challenging, with gaps and voids around the embedded fiber. Successful embedding of fiber optic sensors requires good contact between the fiber and the matrix to eliminate potential gas/liquid leaks in critical systems such as in nuclear and aerospace services. Defect-free fiber/matrix bond is also essential for accurate measurement of parameters of interest, such as temperature and strain. This study developed a novel fiber embedding technique based on electric field-assisted sintering (EFAS). Sapphire optical fibers with diameters of 125 µm and 250 µm were embedded in stainless steel (SS) 316L using EFAS. The embedding was completed by sintering SS 316L powders at a pressure of 50MPa, hold time of 5 min, and temperatures of 1000°C, 1100°C, and 1200°C. Joule heating mechanism during EFAS enabled rapid sintering of the SS 316L powder with resulting sample densities over 99%. Microscopy analysis performed on the cross-sections revealed a defect-free bond between the embedded fiber and SS 316L. The good integrity of the embedded fiber was evidenced by optical transmittance measurement. Optical attenuation of the fiber before and after embedment was examined in the near-infrared region. Scanning electron microscopy was employed to investigate the grain morphology of SS 316L near the embedded fiber. Hardness distribution in the sintered part was also investigated to study the effect of the embedded fiber on the mechanical properties of the as-fabricated component. The results indicated that EFAS was able to embed fiber in SS with good fiber functionality and part quality.

36 - MATERIALS SCIENCE↗
NASA NTRS1985

Remote displacement measurement using a passive interferometer with a fiber-optic link

Remote displacement measurement is demonstrated using a Fabry-Perot cavity with a multimode optical fiber link. The sensing cavity modulates, as a function of its length, the spectrum of a light-emitting diode (LED). The light returns via the fiber and is analyzed by a tunable reference cavity. A closed-loop control causes the reference cavity to track the sensing cavity length within 2 x 10 to the -12th m. Displacement range is 2 x 10 to the -6th m. The reference cavity length is measured interferometrically, using a laser, to obtain the sensing cavity length. Advantages of this sensing technique include compatibility with multimode fiber-optic components, high immunity to optical losses, and large dynamic range.

Beheim, G.↗
DOE OSTI2024

Utah FORGE: Well 16B(78)-32 Distributed Temperature Sensing Data from April and May 2024

This dataset includes Neubrex Energy Services fiber optic distributed temperature sensing (DTS) data from well 16B(78)-32 during stimulation and circulation, including interaction with well 16A(78)-32, during April and May 2024. The DTS data are stored in HDF5 file format and are accompanied by a PowerPoint report on the study. All times in this dataset are in UTC. Depths are in MD relative to Kelly Bushing Height, and temperatures are in degrees Fahrenheit. All DTS measurements were made using a Yokogawa 3000DTSX Distributed Temperature Sensing Interrogator Unit, with a spatial sampling interval of 3.28 feet and a temporal sampling rate of 129 seconds. The third-party Pressure-Temperature Gauge data should be used with caution after April 20, 2024, as its performance is not considered reliable beyond this date.

15 GEOTHERMAL ENERGY↗
DOE OSTI2023

Toward local core outlet temperature monitoring in gas-cooled nuclear reactors using distributed fiber-optic temperature sensors

Gas-cooled nuclear reactors operate at temperatures up to 950 °C with significant spatial variations in power generation and coolant flow through hundreds of parallel flow channels, resulting in complex mixing at the core outlet. The high temperatures and complex mixing can damage downstream components, challenge reactor calorimetry for power determination, and result in significant conservatism in calculated peak fuel temperatures, which ultimately limits the total power output. Directly measuring each gas stream individually is unrealistic using single point thermocouples, requiring more robust sensing techniques. Fiber-optic sensors are resilient to high temperatures (up to 1,000 °C) and radiation damage. Moreover, distributed measurements can be made along the length of one fiber, making them potential candidates for monitoring local core outlet temperatures to improve core calorimetry and identify hot channels. Here, to the authors’ knowledge, this manuscript is the first to report spatially distributed fiber optic temperature measurements to quantify mixing at the outlet of a relevant orifice plate under prototypic temperature and flow regimes to assess the feasibility of using fiber-optic sensors for distributed measurements of coolant temperature in gas-cooled reactors. A single optical fiber captured dynamic changes in local temperatures, whereas the mixed outlet temperature exhibited a muted response and could not identify which channels were responsible for the change in the mixed outlet temperature. The discussion focuses on potential challenges for deploying distributed optical fibers in gas-cooled reactors, including the effects of vibrations, radiation-induced signal attenuation and drift, and routing of the fiber while minimizing flow obstructions.

42 ENGINEERING↗