Insulated weld tooling permits uniform, high quality weld
The application of a ceramic material coating to all surfaces contacting parts to be welded permits greater weld strength than the conventional weld tooling method.
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The application of a ceramic material coating to all surfaces contacting parts to be welded permits greater weld strength than the conventional weld tooling method.
Birefringent coating for strain measurements on large surfaces contains constituents that can be premixed and sprayed as a single component with conventional paint spray equipment. Elevated temperatures are not required for spraying or curing of the coating material which has long pot life.
Literature review provides compilation of properties of coating materials used for external application on space vehicles. Attention is given to absorptance-emittance data and experimental spectral reference curves.
Improved organic potting and conformal coating materials protect fragile electronic components and circuitry from mechanical shock and vibration, moisture, and corrosion. These materials meet specifications covering resistance to cycling, radiation, flammability, and sterilizing agents for certain space applications.
Flexible bulb is squeezed to change mean free path of hydrogen atoms, and to change bulb's volume without changing its surface area. Volumes in the different configurations are measured to learn the change in mean free path and calculate wall shift. Various bulb coating materials are described.
Application of commercial coating to exterior of sandwich panel structures for determining presence of voids in brazed plates is discussed. Procedure for applying coating material and method of conducting nondestructive tests are explained. Illustrations are included to show appearance of voids.
A previous investigation indicated that combustion efficiency of low burning-rate propellants could be improved if the aluminum fuel was replaced by aluminum particles coated with a magnesium-aluminum eutectic alloy (ALCAL). The purpose of the present investigation was to evaluate the possibility of improving the combustion efficiency of these propellants by admixing the eutectic with the aluminum rather than coating the aluminum. Tests of three propellants similar in every respect except for the metal fuel were conducted in test motors with 4.54 kg (10 lbm) of propellant. The first propellant used aluminum fuel; the second contained aluminum admixed with magnesium-aluminum eutectic; the third used ALCAL. The test results show the the admixed fuel gave better low burning-rate combustion efficiency than the other two. The test results also showed that the ALCAL was deficient in that much, if not all, of the coating material could be found as the fine particles in a bimodal mix of aluminum and eutectic. The combustion efficiency of low burning-rate aluminized propellants can be significantly improved by mixing a small amount of magnesium-aluminum alloy with the aluminum fuel.
The final report for the large orbiting X-ray telescope (LOXT) high resolution mirror design study is presented. The following tasks were performed: (1) Generation of a reference and alternate preliminary design for the LOXT high resolution mirror assembly, which will meet the LOXT scientific requirements, and are within the present state of the art of materials and fabrication techniques. (2) Measurement, in X-rays, of the scattering properties of a variety of optical flats, embodying materials, coatings, and polishing techniques which might be applicable to the flight configuration LOXT high resolution mirror. (3) Preparation of a procurement specification for a paraboloid test mirror of the size of the innermost paraboloid of the high resolution mirror assembly, including the design requirements for the reference design evolved from this preliminary design study. The results of the engineering and scientific analysis and the conclusions drawn are presented. The procurement specification for the test mirror is included.
A electronic device including lead attachment structure which permits operation of the devices over a wide temperature range is reported. The device comprises a core conductor having a thin coating of metal thereon whereby only a limited amount of coating material is available to form an alloy which bonds the core conductor to the device electrode, the electrode composition thus being affected only in the region adjacent to the lead.
The effect of high humidity (95% RH) at 60 C, 70 C, 85 C and 100 C on the solid-to-liquid reversion of polyurethane elastomers (used for potting electrical connectors and conformal coating printed circuit boards) was investigated. Hardness measurements were conducted on eleven elastomers to track reversion for a 101-day period. The primary purpose of the tests was to provide data to predict service life for the polyurethane elastomers. This was not accomplished as the hardness did not deteriorate rapidly enough at the lower test temperatures. The tests did determine that the potting and coating materials most widely used on the S-1C Program are susceptible to reversion but appear adequate for service in the S-1C environment.
A prototype penetrator instrument was impacted into a dry lake bed. Laboratory studies of the soil surrounding the penetrator revealed that the soil was contaminated by paint and metal from the penetrator's casing. Paint pigment rich in titanium and sulfur was found in the adjacent soil. The highly mobile paint pigment migrated onto viewing ports in the penetrator's exterior. Bulk analysis of the soil adjacent to the impactor showed a significant increase in both elements, as well as the presence of metal chips from the casing and nose cone. It is recommended that great care be taken in the use of coating materials and the metal alloys selected for the penetrator's exterior, or the accuracy of any experiment requiring an uncontaminated in situ sample may be adversely affected.
An analysis of toughness and strength in intermittently bonded brittle filament/brittle matrix composites is presented that shows the importance of the coating material in achieving high toughness properties. Some observations are made on methods of measuring the components of toughness in composites. Both a mathematical model and experimental results are incorporated into the discussion.
The high tensile strengths of strong interfacial bonding may be combined with the large fracture toughness of weak interfacial bonding in brittle fiber/brittle matrix composites by intermittently coating the filaments before layup so as to have random alternate weak and strong regions. Appropriate coating materials enable Cook-Gordon Mode I interfacial debonding to take place, which produces very long pull-out lengths with an associated large contribution to toughness. Unidirectional boron-epoxy composites have been so made which have toughnesses greater than 200 kJ/sq m while retaining rule of mixtures tensile strengths. Similar trends have been observed for crossply layups.
The adherence, friction, and wear properties of thin hard refractory compound coatings applied to 440C bearing steel by radiofrequency sputtering were investigated. Friction and wear tests were done with nonconforming pin on disk specimens. The compounds examined were chromium carbide, molybdenum silicide, and titanium carbide. The adherence, friction, and wear were markedly improved by the application of a bias voltage to the bearing steel substrate during coating deposition. Analysis by X-ray photoelectron spectroscopy indicated that the improvement may be due to a reduction in impurities in bias deposited coatings. A fivefold reduction in oxygen concentration in MoSi2 coating by biasing was noted. Chromium carbide was not effective as an antiwear coating. Molybdenum silicide provided some reduction in both friction and wear. Titanium carbide exhibited excellent friction and antiwear properties at light loads. Plastic flow and transfer of the coating material onto the pin specimen appears to be important in achieving low friction and wear.
The primary objective of this review is to tabulate the basic recommendations of several solar telescope studies. A primary matrix, listing some of the basic optical parameters, was compiled and forms the basis for a table. From this table it is apparent that a strong consensus exists on the configuration of the telescope and on its fundamental dimensionless parameters. Other tables presented in this document address the basic approach of each study to the telescope design as well as to the design of critical subsystems. These subsystem problems include the material, coating, configuration, mounting, launch locks, and thermal control of the primary mirror, the structure of the main telescope and the instrument bay, the mechanisms for radiation rejection, thermal control, and meteoroid shielding, and methods of maintaining image quality by proper alignment and by image motion compensation.
RF-sputtered coatings of CrB2, MoSi2, Mo2C, TiC, and MoS2 were examined by X-ray photoelectron spectroscopy (XPS). Data on stoichiometry, impurity content, and chemical bonding were obtained. The influences of sputtering target history, deposition time, RF power level, and substrate bias were studied. Significant deviations from stoichiometry and high oxide levels were related to target outgassing. The effect of substrate bias depended on the particular coating material studied.
Reflection polarizers and analyzers for the extreme UV spectral region are discussed. The conditions for optimum polarization are presented, and the polarization characteristics of a number of metal coatings, including gold and some of the platinum metals, are given. The performance of three- and four-mirror polarizers, using these metal coatings, is discussed. The properties required of a polarization analyzer are presented, and the performance of single and three- and four-reflection analyzers are discussed in terms of the optical properties of coating materials that might be useful for analyzers.
Instrumentation, results, and future prospects for sky surveys at UV wavelengths inaccessible from the ground are reviewed. Detectors and optical materials, coatings, and systems for UV surveys are discussed, previously performed UV sky surveys are recounted, and some specific results of these surveys are examined. The rationale for UV surveys is explained, and the detectors and instrumentation considered for future UV surveys are described. It is noted that for the wavelength range from 1000 to 2000 A, detectors and instrumentation are already available to provide an all-sky UV survey of moderate resolution (10 to 30 arcsec) and moderate sensitivity (reaching hot stars as faint as 18th visual magnitude in direct imagery and 11th magnitude spectrographically with 2-A resolution).