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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 307 records · Page 17
All sourcesNASA NTRSDOE OSTI
NASA NTRS1983

Effects of random member length errors on the accuracy and internal loads of truss antennas

The effects of random member length errors on the surface accuracy, the defocus, and the residual, internal loads of tetrahedral truss antenna reflectors have been studied analytically. The analytical procedure involves performing multiple, deterministic finite element structural analyses for a particular truss. For each analysis, the normally distributed, random member length errors are selected by random number generator. A best fit paraboloid analysis is used to determine a root mean square error and defocus from each analysis. The statistical properties of these quantities as well as the internal loads are calculated from the results of many independent analyses. Results indicate that the number of members in a tetrahedral truss antenna of a given diameter has a significant effect on surface accuracy, defocus and internal loads. It was also found that the member axial stiffnesses and antenna focal length have a very small effect on reflector surface accuracy.

Greene, W. H.↗
DOE OSTI2022

Characterization of an aerosolized nanoparticle beam beyond the diffraction limit through strong field ionization

Abstract The study of nanomaterials is an active area of research for technological applications as well as fundamental science. A common method for studying properties of isolated nanoparticles is by an in-vacuum particle beam produced via an aerodynamic lens. Despite being common practice, characterization of such beams has proven difficult as light scattering detection techniques fail for particles with sizes beyond the diffraction limit. Here we present a new technique for characterizing such nanoparticle beams using strong field ionization. By focusing an ultrafast, mJ-level laser into the particle beam, a nanoparticle within the laser focus is ionized and easily detected by its ejected electrons. This method grants direct access to the nanoparticle density at the location of the focus, and by scanning the focus through the transverse and longitudinal profiles of the particle beam we attain the 3-dimensional particle density distribution for a cylindrically symmetric beam. Further, we show that strong field ionization is effective in detecting spherical nanoparticles as small as 10 nm in diameter. Additionally, this technique is an effective tool in optimizing the particle beam for specific applications. As an example we show that the particle beam density and width can be manipulated by restricting the gas flow into the aerodynamic lens.

77 NANOSCIENCE AND NANOTECHNOLOGY↗
NASA NTRS2019

Characterization of Propellant Flow and Bias Required to Initiate an Arc Discharge in a Heaterless Hollow Cathode

Heaterless hollow cathodes provide an opportunity to reduce complexity and improve reliability in electric propulsion systems. While removal of the heater has little effect on steady-state operation of a hollow cathode, it has a considerable effect on the ignition process. To successfully integrate a heaterless hollow cathode into a spaceflight electric propulsion system, it will be necessary to establish definitive requirements for the propellant feed and electrical subsystems so that ignition of a plasma discharge can be achieved reliably. The aim of this research was to form a better understanding of these requirements by performing an investigation of the propellant flow and voltage conditions required for the ignition of a plasma arc discharge. This aim was achieved by performing discharge initiation experiments using both a specially designed experimental apparatus and a functional heaterless hollow cathode assembly. It was demonstrated that there is a distinct difference in the voltage required to initiate a plasma discharge between two common electric propulsion propellants, xenon and krypton, which suggests that the developmental testing of heaterless hollow cathodes needs to be performed with the appropriate propellant gas species. Heaterless hollow cathode ignition experiments showed that the keeper orifice diameter has a strong effect on the voltage required to ignite a plasma discharge at a given propellant mass flow rate, while the effect of keeper-cathode separation distance was only strong at flow rates below 25 sccm (Xe).

Ham, Ryan K.↗
NASA NTRS1974

Research turbine for high-temperature core engine application. 2: Effect of rotor tip clearance on overall performance

A 25.4-cm (10-in) tip diameter turbine was tested to determine the effect of rotor radial tip clearance on turbine overall performance. The test turbine was a half-scale model of a 50.8-cm-(20-in.-) diameter research turbine designed for high-temperature core engine application. The test turbine was fabricated with solid vanes and blades with no provision for cooling air and tested at much reduced inlet conditions. The tests were run at design speed over a range of pressure ratios for three different rotor clearances ranging from 2.3 to 6.7 percent of the annular blade passage height. The results obtained are compared to the results obtained with three other turbines of varying amounts of reaction.

Szanca, E. M.↗
NASA NTRS1960

Mixing Characteristics Downstream of Core Region of High-Temperature Axisymmetric Jets Exhausting Into Transonic and Supersonic Streams

A series of rocket motors with varying exit to throat area ratios was tested in the 8- by 6-foot wind tunnel to determine the effects of mixing on jet diameter and temperature decay at large distances (x/d > 30) from the nozzle exit. An approximate method to account for effects of the initial expansion was evolved. It was determined that the combustion efficiency has an important effect on jet spreading, since the unburned products can burn downstream of the nozzle. The data showed considerable scatter; however, mixing rates were, in general, lower than those observed for subsonic jets. Data for angles of attack of 5 and 10 deg are also presented, giving the respective centerline shift and temperature decay as a function of axial distance.

Huff, Ronald G.↗
NASA NTRS2013

Long Hole Film Cooling Dataset for CFD Development : Infrared Thermography and Thermocouple Surveys - Part 1

An experiment investigating flow and heat transfer of long (length to diameter ratio of 18) cylindrical film cooling holes has been completed. In this paper, the thermal field in the flow and on the surface of the film cooled flat plate is presented for nominal freestream turbulence intensities of 1.5 and 8 percent. The holes are inclined at 30deg above the downstream direction, injecting chilled air of density ratio 1.0 onto the surface of a flat plate. The diameter of the hole is 0.75 in. (0.01905 m) with center to center spacing (pitch) of 3 hole diameters. Coolant was injected into the mainstream flow at nominal blowing ratios of 0.5, 1.0, 1.5, and 2.0. The Reynolds number of the freestream was approximately 11,000 based on hole diameter. Thermocouple surveys were used to characterize the thermal field. Infrared thermography was used to determine the adiabatic film effectiveness on the plate. Hotwire anemometry was used to provide flowfield physics and turbulence measurements. The results are compared to existing data in the literature. The aim of this work is to produce a benchmark dataset for Computational Fluid Dynamics (CFD) development to eliminate the effects of hole length to diameter ratio and to improve resolution in the near-hole region. In this report, a Time-Filtered Navier Stokes (TFNS), also known as Partially Resolved Navier Stokes (PRNS), method that was implemented in the Glenn-HT code is used to model coolant-mainstream interaction. This method is a high fidelity unsteady method that aims to represent large scale flow features and mixing more accurately.

Shyam, Vikram↗
DOE OSTI2021

Early development of multifilament polyacrylonitrile-derived structural hollow carbon fibers from a segmented arc spinneret

Carbon fiber is a highly desired material for structural applications requiring high strength and stiffness and low weight but has seen only incremental improvements in properties over the last few decades. Further increases in carbon fiber specific properties, including specific strength and specific modulus, would further propel its unique capabilities. One method to produce high specific property carbon fibers for structural applications is the development of hollow carbon fibers. In this work, we report on the early development of polyacrylonitrile-derived structural hollow carbon fibers. Here, multifilament, continuous tow, polyacrylonitrile-based precursor hollow fibers were successfully produced utilizing a segmented arc spinneret approach. When batch oxidized, the hollow precursor fibers demonstrated evidence of oxidation proceeding from both the interior and exterior of the filament. Further results suggested that reducing the precursor hollow fiber wall thickness would allow for complete, homogeneous oxidation, thereby avoiding the skin-core structure often observed in commercial carbon fiber. Here, hollow carbon fibers were as small as 35 µm outer diameter, 22 µm inner diameter (6.5 µm wall thickness). At these diameters, the hollow carbon effective fiber specific strength was 0.54 N/tex and the effective specific modulus was 120 N/tex, approaching the effective specific modulus of T700S at 136 N/tex.

36 MATERIALS SCIENCE↗
DOE OSTI2020

Volatilization Behavior of Supported Au Nanoparticle Arrays under H 2 at High Temperature

In this work, the fabrication and experimental study of model Au nanoparticle arrays (nanodots) was used to allow a direct comparison of reactive evaporation at elevated temperatures and nonambient H 2 -containing gas atmospheres with theoretical models. Strong temperature and H 2 -concentration dependencies were confirmed as expected, and the observed dependence in particle diameter with time was effectively described using a reactive evaporation and gas phase diffusion based quantitative model.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2025

Probing Nanorod Assembly and Dynamics in Polymer Nanocomposites in Equilibrium and Shear

Coarse-grained molecular dynamics simulations are used to examine the structure and dynamics of nanorod assemblies in polymer melts under equilibrium and simple shear. We show that as the concentration of nanorods increases, there is a transition from an isotropic phase to a two-phase region in which the nanorods phase separate into a dilute phase and dense bundles of hexagonally packed nanorods. The onset of the two-phase region is below that predicted by Onsager theory, which we attribute to an effective increase in the diameter of nanorods due to a layer of polymer bound to the rod surfaces. Equilibrium simulations show that increasing polymer chain length N enhances nanorod bundling at fixed nanorod concentration. Simulations of systems undergoing simple shear show that flow enhances nanorod alignment and bundling relative to those of equilibrium systems with similar properties. Finally, simulations reveal that increasing nanorod length enhances nanorod alignment under shear at equivalent shear rates but not at equivalent Péclet numbers. Overall, our simulations highlight that polymer matrix-nanorod attraction (i.e., chemistry), shear rate, and matrix chain length are desirable design variables to control the structure of nanorod-containing soft materials under simple shear.

diffusion↗
DOE OSTI2024

Interconnected Nanoporous Polysulfone by the Self-Assembly of Randomly Linked Copolymer Networks and Linear Multiblocks

Porous materials have attracted considerable attention due to their versatile applications, especially in water purification. Interconnected nanoporous structures are distinguished by their high degree of porosity and resistance to clogging, as well as their insensitivity to nanostructural orientation. Previous works on randomly linked copolymer systems have shown that they can effectively produce disordered cocontinuous nanostructures, which upon removal of one component yield interconnected nanoporous materials. However, the cocontinuous nanomaterials previously developed using polystyrene (PS) and poly(d,l-lactic acid) (PLA) strands, and the resulting interconnected nanoporous PS monoliths, were far too brittle to enable practical use as membranes. Here, we study the self-assembly of randomly linked copolymer networks prepared using blocks of the engineering polymer polysulfone (PSU). A wide cocontinuous regime (spanning 40 wt %) was found for randomly end-linked copolymer networks (RECNs) constructed from PSU and PLA strands, via a combination of mechanical testing, gravimetry, small-angle X-ray scattering, and scanning electron microscopy. The PSU/PLA cocontinuous nanomaterial with symmetric composition showed 2.4 times higher Young’s modulus and ~100 times greater toughness than the corresponding PS/PLA sample. The interconnected nanoporous PSU fabricated after etching of PLA even exhibited 1.6 times greater toughness than PS/PLA prior to PLA removal. To facilitate the production of thin films of cocontinuous nanomaterials, we applied solution-processable randomly linked linear PSU/PLA multiblock polymers onto ultrafiltration membranes. Here, the interconnected nanoporous PSU thin film generated by etching PLA was found to effectively reject 50 nm diameter particles without significantly compromising permeability. This discovery presents a valuable addition to the existing techniques used to fabricate PSU membranes. In contrast to traditional methods, which are sensitive to processing conditions, produce a wide range of pore sizes, and offer limited adjustability of pore size, the current technique is anticipated to enable interconnected PSU membranes with more uniform and tailorable porosity.

36 MATERIALS SCIENCE↗
DOE OSTI2023

Prediction and Validation of Flow Properties in Porous Lattice Structures

High-porosity metal foams have been extensively studied as an attractive candidate for efficient and compact heat exchanger design. With the advancements in additive manufacturing, such foams can be manufactured with controlled topology to yield highly tailorable mechanical and transport properties. In this study, a lattice Boltzmann method (LBM)-based pore-scale model is implemented to simulate the fluid flow in additively manufactured (AM) metal foams with unit cell topologies of Cube, Face Diagonal (FD)-Cube, Tetrakaidecahedron (TKD), and Octet lattices. The pressure gradient versus average velocity profiles predicted by the LBM model were validated against in-house measurements on the AM lattice samples with the same unit cell topologies. Based on the simulation results, a novel hybrid model is proposed to accurately predict the volume averaged flow properties (permeability and inertial coefficients) of the four structures. Specifically, the linear LBM (neglecting inertial forces) is first implemented to obtain the intrinsic permeability, and then the standard LBM is applied to obtain the inertial coefficient. Convenient correlations for those flow properties as a function of porosity and fiber diameter are constructed. The effects of the AM print qualities on the flow properties are also discussed. The advantages of the hybrid model compared to the polynomial fitting approach for determining flow properties are discussed and compared quantitatively. The hybrid model and presented results are valuable for flow and thermal transport evaluation when designing new metal foams for specific applications and with different materials and topologies. Finally, the presented correlations based on pore-scale simulations can also be conveniently used in volume-averaged models to predict the macroscale flow behavior in such complex structures.

42 ENGINEERING↗
DOE OSTI2025

Microstructure Scale Lithium-Ion Battery Modeling: Part III. When and Where Lithium Plating Occurs and its Correlation with the Electrode Microstructure

Li-ion battery performance and degradation are closely related to the cell’s underlying electrode microstructure. Electrode microstructures are typically characterized with volume-averaged properties that neglect the impact of local heterogeneities. However, local heterogeneities create hot spots that can trigger degradation onset. Herein, a microstructure scale electrochemical model is used to investigate the impact of microstructure heterogeneity on lithium plating. The model predicts lithium plating is not uniform, even when considering a relatively small portion of the electrode (a cross-sectional area of 154×144 µm 2 ), preferring to plate on larger particles as compared to smaller particles. While local heterogeneities control where plating occurs, the model predicts that volume-averaged properties control when plating occurs. Additionally, the model predicts that the active material specific surface area has a linear relationship with the plating onset. However, the linear relationship between increased active material surface area and delayed plating response appears to be sensitive to the microstructure feature used to increase the active interface area. Here, a comparative case-study is explored where the specific surface area is increased by either reducing the active material particle diameter, adding open-porosity cracks, or increasing the active material surface roughness. The model predicts that increasing the specific surface area by reducing the active material particle diameter is the most effective strategy for delaying lithium plating. At 6C, reducing particle size is shown to be 3 and 20 times more effective than, respectively, adding open-porosity cracks and increasing surface roughness. A dual-layer electrode architecture combining gradations both for average properties and uniformities is eventually proposed to improve homogeneous material utilization and reduce degradation at high charge rates.

25 ENERGY STORAGE↗
NASA NTRS1971

Design of optical mirror structures

The structural requirements for large optical telescope mirrors was studied with a particular emphasis placed on the three-meter Large Space Telescope primary mirror. Analysis approaches through finite element methods were evaluated with the testing and verification of a number of element types suitable for particular mirror loadings and configurations. The environmental conditions that a mirror will experience were defined and a candidate list of suitable mirror materials with their properties compiled. The relation of the mirror mechanical behavior to the optical performance is discussed and a number of suitable design criteria are proposed and implemented. A general outline of a systematic method to obtain the best structure for the three-meter diffraction-limited system is outlined. Finite element programs, using the STRUDL 2 analysis system, were written for specific mirror structures encompassing all types of active and passive mirror designs. Parametric studies on support locations, effects of shear deformation, diameter to thickness ratios, lightweight and sandwich mirror configurations, and thin shell active mirror needs were performed.

Soosaar, K.↗
NASA NTRS1972

Analog simulation of a gas pressure regulator.

The behavior characteristics of direct-acting gas pressure regulators are discussed in terms of spring force, flow force, and friction force. The dynamics of the metering valve and bellows assembly are described by equating all forces on the valve to zero. Continuity equations for the regulator are derived. Simulations are carried out to determine effects of sensing orifice diameter, poppet stem friction, output volume, and supply pressure on regulator behavior. Several regulator configurations are studied.

Dustin, M. O.↗
NASA NTRS1973

Fatigue of boron-aluminum composites bonds and joints

Study examines effects of boron filament diameter on bonds and joints in boron-aluminum composite. Data include static strength, fatigue, and dynamic moduli of elasticity. Manson-Coffin analyses and metallurgical and fracture surface evaluation were also performed.

Hersh, M. S.↗
NASA NTRS1975

Apparatus for production, measurement and reaction studies of dissociated gases at elevated temperatures

An apparatus is described which is used for the controlled production, characterization, and study of dissociated gases in a microwave discharge at elevated temperatures. A unique feature is the ability to produce and study a microwave discharge plasma in the heated zone. This allows elevated temperature reactions to be studied in high concentrations of dissociated gases. Further, the system permits weight change measurements of specimens in the plasma, thus facilitating reaction rate determinations. Included is a description of a cavity for use on a 50-mm diameter cylindrical reactor. The effects of flow rate, pressure, temperature, power, metal sample, and sampling position on dissociation percentage of oxygen in the apparatus are described as well as a technique for sample temperature measurements in the plasma which permits determination of high temperature recombination coefficients and reaction rates.

Christian, J. D.↗
NASA NTRS1976

Applications of the Ultrasonic Serial Number Restoration Technique to Guns and Typical Stolen Articles

An ultrasonic cavitation method for restoring obliterated serial numbers has been further explored by application to articles involved in police cases. The method was applied successfully to gun parts. In one case portions of numbers were restored after prior failure by other laboratories using chemical etching techniques. The ultrasonic method was not successful on a heavily obliterated and restamped automobile engine block, but it was partially successful on a motorcycle gear-case housing. Additional studies were made on the effect of a larger diameter ultrasonic probe, and on the method's ability to restore numbers obliterated by peening.

Young, S. G.↗