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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 307 records · Page 17

Mixed-Material Scintillators (MMSS Quarterly Report FY20Q2)

This project aims to invent, model, and prototype mixed-material scintillator systems (MMSSs), a new class of radiation detectors that use heterogenous internal structures of different scintillating materials to detect additional properties of radiation. These internal structures can be produced using additive manufacture (3D printing) of scintillator, a currently emerging application of additive manufacture technology. MMSSs combine the low cost and complexity of conventional scintillation detectors with capabilities currently only available in more expensive and complex detectors. By identifying promising MMSS designs, this project will enable a new class of detectors to meet DNN’s mission needs for SNM detection. This quarter, we delivered one the MMSS Particle-ID Modeling report, a major deliverable of this project. This report describes our results on simulations of the particle-ID (PID) class of detectors. We found that these detectors outperform competing approaches for neutron-gamma discrimination, neutron source pointing, and neutron spectroscopy. Further highlights of the report are described below. During this quarter, We alerted HQ to a change in schedule for the remaining simulations planned for this project: we plan to put off further simulation and reporting of the position-resolving (PR) detector class until July. This change in schedule has allowed us to go into additional detail in the PID work that is both very promising and motivates our upcoming proposal. The other active task in this project is prototyping 3D-printed scintillators with the aim of realizing the designs we’ve simulated. On that front, we had three focuses: measuring the light output, increasing the size of printed parts, and combining blue and green scintillators. We succeeded in measuring the light output, showing an output of 30% of commercial standard. This result leaves room for improvement but is within striking distance of where we need to be. We were on track to demonstrate a key requirement for increasing the size of parts and also to show combined green/blue prints before the laboratory moved to a Minimum Safe (MinSafe) Operations posture as a result of local Shelter In Place orders due to Covid-19.

42 ENGINEERING↗

Development of an In-Situ Method for Cable Condition Monitoring in Nuclear Power Plants (SBIR Phase IIB Final Report)

This is the final report of a Small Business Innovation Research (SBIR) project that Analysis and Measurement Services Corporation (AMS) has conducted for the U.S. Department of Energy (DOE) over a seven-and-a-half year period (February 2013 through April 2020 with the awards of Phase I, Phase II and Phase IIB projects). The goal of the project was to design, develop, validate, and demonstrate a technique for in-situ testing of cable insulation polymers that will identify, locate, and provide the degree of aging for cables commonly used in nuclear power plants. During the Phase I project, AMS established that the frequency domain reflectometry (FDR) technique can successfully identify and measure cable insulation degradation that can be trended with aging. In Phase II, AMS performed extensive cable aging studies to correlate FDR measurements with other laboratory condition monitoring techniques and developed aging condition categories to quantify the severity of insulation degradation. In Phase IIB, the project expanded the research to include a wider variety of cable polymers that are used in the commercial nuclear power industry. This work also involved developing acceptance criteria to objectively assess age-related cable degradation while sharing the results of this research with industry, academia, and national laboratories to advance the state of the art in cable aging management technologies. The products developed under this research project provide the nuclear industry with an effective condition monitoring tool to support safe and long-term plant operation. Throughout the project, collaborations and support were received from a variety of industry organizations and individuals including DOE National Laboratories as well as nuclear plant utilities and several other industry experts and cable manufacturers. Contributions from these organizations included the donation of new cables, naturally aged cables, and research collaboration. The validation and commercialization of the products of this project were achieved through opportunities to test and demonstrate the technologies’ capabilities on-site at nuclear power generation and research facilities as well as in the laboratory alongside industry peers and cable testing service companies. The research resulted in a technology that can be used to identify, locate, and quantify age-related degradation in several types of cable polymers. This included developing software and hardware as well as the methodology for using the FDR technique to assess age-related degradation of installed cables. The technology developed under this project can provide nuclear plant management, engineers, and technicians with an in-situ electrical test method to determine if in-service cables need to be replaced, monitored on a periodic basis, or show no evidence of significant age-related degradation that may require action. Near the end of this Phase IIB project, the FDR product was sold to a nuclear power utility in South Korea. This sale of a dedicated aging assessment tool is the beginning of a comprehensive contract with the expectation of twelve (12) units sold to that country. Additionally, the FDR technology has been sold to several industry organizations including a nuclear research institute and the Diablo Canyon nuclear power plant. This technology is also being leased by other nuclear industry service companies for incorporation into aging management programs. The cable testing technology that was developed under this project was also integrated into a comprehensive cable aging assessment service that is being offered to the nuclear industry at the request of U.S. nuclear utilities and is currently part of onsite testing services provided by AMS.

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗

Magnetic Microcalorimeter Gamma Detectors with Ultra-High Energy Resolution. Final Report

The goal of this project was to build a commercially viable metallic microcalorimeter (MMC) g-spectrometer with an ultra-high energy resolution <50 eV for accurate non-destructive assay (NDA) of nuclear materials. Improved NDA simplifies and accelerates safeguards analyses in the nuclear fuel cycle and enhances capabilities to detect the diversion of nuclear materials for illicit purposes. High-resolution MMC g-spectrometers can also improve the accuracy of nuclear data that NDA is based on.

38 RADIATION CHEMISTRY, RADIOCHEMISTRY, AND NUCLEA↗

MagMicro with Ultra-High Energy Resolution (FY20 Q3 Report)

Progress this quarter: All technical work on this project had been completed in Q2. In Q3, we only worked on summarizing the results of this 4-year project for the final report. It will be submitted separately.

38 RADIATION CHEMISTRY, RADIOCHEMISTRY, AND NUCLEA↗

Discrete Element Method Analysis for Metal Powders Used in Additive Manufacturing, and DEM Simulation Tutorial Using LIGGGHTS-PUBLIC [PowerPoint and paper]

Discrete Element Method (DEM) is a method of analysis to evaluate the dynamic interactions between granular particles. This method has been used in the pharmaceutical industry to improve the powder compaction process for tablet manufacturing. There are also applications in agriculture, food industry, and manufacturing. Direct energy deposition is an additive manufacturing technique which uses metallic powders fed through a nozzle, melted using a directed laser, and transformed into a solid object layer by layer. One way of feeding metal particles into the system involves the use of a vibrating hopper. Given a specified amplitude and frequency input, the hopper will enable the powder to travel up a path, and inject through the system with assistance from a stream of gas. The mechanical properties of a printed object can vary, depending on the characteristics of the powder flow and the particles’ as-received properties. Improved understanding of dynamic interactions of flowing powders could enable additive manufacturing components with 2D or 3D variations in mechanical properties, e.g., density. This work uses DEM simulation software to investigate the effects of particle cohesion, friction, and density on the quality of the flow by performing an angle of repose simulation, which is often used as a metric to evaluate the flowability of powders.

36 MATERIALS SCIENCE↗

CryoTARPOS Vibration Mitigation System for Layered Experiments

The goal of this project is to implement a system that can eliminate or mitigate vibration so that clear images can be taken without bypassing the cryocooler. By allowing for layer characterization and cryocooler operation at the same time, cooling capacity and thermal stability of the target would be improved, and more layer characterization data could be taken. Increased cooling capacity and thermal stability could allow for layering during occasional off normal conditions that would typically result in a loss of temperature control and NIF operational delays ranging from several hours to several days per month. The increased cooling capacity and thermal stability could also allow for layering of new target platforms that have less cooling margin. Additional layer images could be used for better characterization of defects and non-uniformities in the layer and would reduce the likelihood of layer seed loss, which typically adds ~12 hours per week in layering time. Motion blur from vibration due to off normal activity in the NIF Target Bay could also be mitigated that would usually result in NIF operational delays of several hours every month.

42 ENGINEERING↗

Assessing the Vulnerability of Unmanned Aircraft Systems to Directed Acoustic Energy

The increasingly large payloads of Unmanned Aircraft Systems (UASs) are exponentially increasing the threat to the nuclear enterprise. Current mitigation using RF interference is effective, but not feasible for fully autonomous systems and is prohibited in many areas. A new approach to UAS threat mitigation is needed that does not create radio interference but is effective against any type of vehicle. At the present time there is no commercial counter-UAS system that directly assaults the mems gyros and accelerometers in the Inertial Measurement Unit on the aircraft. But lab testing has revealed resonances in some IMUs that make them susceptible to moderate amplitude acoustic monotones. Sandia's energetic materials facility has enabled a quick and thorough exploration of UAS vulnerability to directed acoustic energy by using intense acoustic impulses to destabilize or down a UAS. We have: 1) detonated/deflagrated explosive charges of various sizes; 2) accurately measured impulse pressure and pulse duration; 3) determined what magnitude of acoustic insult to the IMU disrupts flight and for how long and; 4) determined if the air blast/shock wave on aircraft/propellers disrupts flight.

42 ENGINEERING↗

Replacing photomultiplier tubes with silicon photomultipliers for nuclear safeguards applications

Photomultiplier tubes (PMTs) have been used for decades as the default light detection technology for scintillator-based radiation monitors. PMTs come with a handful of disadvantages, however, including large volume usage, fragility, high-voltage requirements, and susceptibility to magnetic fields. Arrays of silicon photomultipliers (SiPMs) are a possible alternative to PMTs providing similar performance while offering improvements in the areas listed. We focus on straightforward “drop-in replacement” evaluations by imposing a single channel output of the SiPM signal and a backend electronics data acquisition and analysis routine identical to that used for PMTs. In the realm of nuclear safeguards, the primary performance metric for gamma spectroscopy is detector resolution, and for neutron detection it is pulse shape discrimination (PSD) to separate neutron and gamma signals. In this work we present the results of replacing a PMT with a 2” x 2” SiPM array mounted, in turn, to the same 2” x 2” cylindrical sodium iodide (NaI) crystal. The ultimate comparison for this gamma spectrometry is confirmation of uranium enrichment standards, ranging from depleted uranium to 93% highly enriched uranium (HEU), by analyzing the resulting spectra with both a simple integral scaling in key energy regions of the spectrum, as well as with the NaIGEM software package. In addition to the gamma spectroscopy work, we will present the latest results on comparing the PSD capabilities of a 4” x 4” SiPM array to a 5” PMT. As with the gamma spectroscopy evaluations, the light detectors are mounted in turn to the same liter-scale organic scintillators. This neutron-focused work includes evaluation of prototype SiPM readout boards with a single output signal summed over 256 individual SiPM pixels, and evident tradeoffs between PSD capability and fast response.

42 ENGINEERING↗

Gear Test Assembly - Report on Experimental Testing (FY2020)

The Gear Test Assembly (GTA) has completed Campaign #2 of in-sodium testing at the Mechanisms Engineering Test Loop (METL). Campaign #1 was conducted in 2019 and completed 19,600 cycles, correlating to 9,800 fuel assembly maneuvers. Campaign #1 was terminated following a shaft seizure caused by a failed bearing in the sodium gearbox. Campaign #2 was conducted in the spring of 2020 and completed 2,768 cycles, correlating to 1,384 fuel assembly maneuvers. Campaign #2 was terminated following elevated vibration measurements coming from the sodium gearbox. Following cleaning and disassembly, a bearing was found to have failed in the sodium gearbox. Campaign #1 used tapered roller bearings made of 52100 steel with a heat treatment from the manufacturer that allows for operation to 350°C. Campaign #2 used the same tapered roller bearings, but with no heat treatment. A new dynamic shaft seal design was used in Campaign #2 that led to significant reductions in argon consumption and graphite debris generation. A modified external gearbox system led to no external bearing failures and allowed for higher torque output. Finally, modifications to the Carbonation System led to a more effective carbonation process and all-around reduction in turnaround time.

42 ENGINEERING↗

Microcalorimeters for IAEA NML (Annual Report FY2020)

Based on input from Andrey Bosko (IAEA NML) during a visit to LLNL October 17-18, 2019, the project focused on adapting magnetic microcalorimeters (MMCs) for high-resolution decay energy (Q) spectroscopy of actinides. This included fabricating an MMC detector suitable for MeV signals, testing different approaches on how to embed an alpha source inside an absorber, and demonstrating Q-spectroscopy with MMCs.

42 ENGINEERING↗

Verification of Spent Fuel Inside Dry Storage Casks by Fast/Epi-thermal Neutron Mapping: FY2020 Annual Report to NA241 (Annual Report)

Lawrence Livermore National Laboratory has embarked upon development of a novel methodology for verification of spent fuel inside dry storage casks. The issue of verification of the integrity of spent fuel inside dry storage has been one of the most challenging technical problems facing IAEA for many decades. The difficulty arises because of the massive amount of shielding between the inner spent fuel and the outer surface where measurements can be performed. Despite many efforts, detection of useful gamma rays or neutrons from the outer surface has so far proven unsuccessful.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Focused Ion Beam analysis of non radioactive samples [PowerPoint]

The presentation includes various images to illustrate the analysis. Helios G4 Plasma FIB: Xe ion columns mills material 30 times faster than Ga; Options include: Energy Dispersive Spectroscopy (EDS), Wavelength Dispersive spectroscopy (WDS) Electron backscattered Diffraction (EBSD), Time of Flight Sims (ToF SIMS), Inert gas/vacuum sample transfer system; Excels at micromachining and collecting 3D datasets using various detection systems.

42 ENGINEERING↗

Steady-State Ultrasonic Non-Destructive Evaluation for Aerospace & Additive Manufacturing Applications [Slides]

How does ultrasonic inspection work? Rich phenomenology of interactions between ultrasonic waves and features in plate-like structures. Hidden defects/discontinuities create measurable changes in the surface wavefield. Based on these measurements, we can build tools that detect the presence of different kinds of defects and estimate structural/material properties (e.g. local thickness).

42 ENGINEERING↗

National Ignition Facility 192 beam 3w power sensor

NIF requires additional laser diagnostic capabilities to support existing missions and drive performance of the laser to higher powers and energies. There exists a current gap in laser power data on the facility due to the subset of beamlines that are measurement capable. Additionally, as NIF increases the radiation yield on target experiments, the performance of the current laser diagnostic 3w power sensor system has been steadily decreasing. The degradation of the current system is not well understood and needs to be characterized to facilitate any new system design.

42 ENGINEERING↗