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DOE OSTI2024

A Novel Dew Point Meter: Application to the Measurement of the Sulfuric Acid Dew Point for Combustion Flue Gas

Accurate knowledge of acid dew point is essential for industrial and applied combustion applications. Sulfur in the fuel or raw materials is converted to sulfur dioxide (SO2) during combustion, and a portion of the SO2 is oxidized to sulfur trioxide (SO3). The SO3 will react to form H2SO4 vapor when in the presence of water vapor. Even with just trace levels of H2SO4 vapor in the gas phase (1-10 ppm), the dew point can reach 100°C and higher. To avoid acid condensation and the resulting corrosion on heat recovery equipment, plant engineers must ensure that surface temperatures are above the acid dew point, but this decreases the efficiency of thermal energy recovery. Thus, there is a trade-off between minimizing equipment corrosion and maximizing thermal energy recovery, and the acid dew point is a key parameter for this optimization. Commercially available acid dew point meters use electric conductivity sensors. These sensors are known to greatly underestimate the dew point due to their low sensitivity. In addition, no validation testing has been reported for these units and they are often expensive. In this work, we analyze the theory of the sulfuric acid condensation and develop a novel dew point meter based on this analysis. The meter consists of a novel optical instrument that is designed to monitor the slightest appearance of condensation on a hydrophobic window surface as the surface temperature of the window is slowly decreased. In this way, an accurate measurement of the dew point is obtained under a wide range of concentrations. The basis of the instrument is that a collimated beam from a diode laser will generate forward scattered light when the beam encounters surface condensate, and a sophisticated array detector is used to sensitively monitor the onset of light scattering. The measurement procedures are established to rapidly find the acid dew point, while minimizing error. Further, to calibrate the dew point meter we developed a calibration system based on a liquid bubbler that can generate a stable gas flow with a known sulfuric acid dew point. Test results show that the dew point meter can accurately measure acid dew point over a wide range. For H2SO4 vapor concentrations as low as 6 ppm the acid dew point is measured with an error of only ~1°C. To demonstrate the versatility of this instrument, the dew point meter was adapted for use with a high-pressure flow cell to allow for measurements of the dew point of flue gas from pressurized oxy-fuel combustion in a 100 kWth pressurized reactor.

Cheng, Mao↗

NASA NTRS1978

Studies of satellite and planetary surfaces and atmospheres

Completed or published research supported by NASA is summarized. Topics cover limb darkening and the structure of the Jovian atmosphere; the application of generalized inverse theory to the recovery of temperature profiles; models for the reflection spectrum of Jupiter's North Equatorial Belt; isotropic scattering layer models for the red chromosphore on Titan; radiative-convective equilibrium models of the Titan atmosphere; temperature structure and emergent flux of the Jovian planets; occultation of epsilon Geminorum by Mars and the structure and extinction of the Martian upper atmosphere; lunar occultation of Saturn; astrometric results and the normal reflectances of Rhea, Titan, and Iapetus; near limb darkening of solids of planetary interest; scattering light scattering from particulate surfaces; comparing the surface of 10 to laboratory samples; and matching the spectrum of 10: variations in the photometric properties of sulfur-containing mixtures.

Sagan, C.↗

NASA NTRS1984

Phase/doppler spray analyzer for simultaneous measurements of drop size and velocity distributions

Research was conducted on a laser light scatter detection method for measuring the size and velocity of spherical particles. The method is based upon the measurement of the interference fringe pattern produced by spheres passing through the intersection of two laser beams. A theoretical analysis of the method was carried out using the geometrical optics theory. The instrument response function was determined to be linear with drop size. Experimental verification of the theory was obtained by using monodisperse droplet streams. Several optical configurations were tested to identify all of the parametric effects upon the size measurements. Both off-axis forward-scatter and back-scatter light detection were utilized. Simulated spray environments and fuel spray nozzles were used in the evaluation of the method. The measurements of the monodisperse drops showed complete agreement with the theoretical predictions. The method was demonstrated to be independent of the beam intensity and extinction resulting from the surrounding drops. An instrument based on the concept has been developed.

Bachalo, W. D.↗

NASA NTRS1986

Lidar mapping of a mixture of aerosol concentrations in a varying atmosphere

In several recent applications dealing with lidar measurement of atmospheric pollution, two basic assumptions are made: (1)The investigated aerosol layer is the only particulate material within the scattering volume; and (2)The contribution of the gaseous atmosphere to the lidar backscattering signals can be estimated and deducted from the total backscattering measurements. In the method discussed a generalized method which allows the elimination of the above mentioned assumptions was developed using multiparameter lidar measurements. The different parameters can be several wavelengths, polarization of the scattered light, scattering angles, or any combination of these parameters. The basic requirements are given. The detailed derivations are presented and discussed.

Kleiman, M.↗

NASA NTRS1986

Prospecting for planets in circumstellar dust - Sifting the evidence from Beta Pictoris

IRAS and near-IR coronographic data for the A5V star Beta Pic are analyzed for evidence of planetary formation. The light scattered from the central star in the system is integrated along the distance to the star to determine the disk magnitude at various distances from the star. A modified gamma distribution is applied to evaluate the scattering coefficient to test a hypothesis that the inner 30 AU of the disk has been swept out by planets. The scattering from the region around Beta Pic is compared with scattering around other A5V stars. Finally, the IR data at 0.89 micron is compared with scattering at the coronograph wavelengths. No evidence is found to support the hypothesis of clearing in the inner disk, although large particle densities can be found very close to Beta Pic. The study illustrates the effectiveness of using scattered light and IR data to discover and characterize matter distributions circumstellar disks.

Diner, D. J.↗

NASA NTRS1989

Surface roughness of flat and curved optical surfaces

Surface roughness measurement has several applications. Even a few A roughness will cause scattered light in optical systems. Smooth surfaces are required in a wide variety of instruments. For example, the outputs of the high power lasers are limited by the surface roughness of mirrors and windows. Similarly, the information storage capacity of magnetic media is limited by the roughness of the surface. Roughness reduces the resolving power of optics and distorts images. The performance of certain thin film components in electronic industries is affected by the roughness on the film surface. X-ray astronomical telescopes require smooth curved surfaces. To improve the surface quality, super sensitive detection methods are required. Wide ranging measurement techniques are developed based on interferometry, electron microscopy, C-rays, ellipsometry, light scattering, and using mechanical stylus, etc. Though there are several techniques available for measurement and evaluation of the surfaces, no single technique is fully adequate. Also, the technique used should be nondestructive and highly sensitive. So, an optical heterodyne profilometer was fabricated. Its current sensitivity is much better than 10A rms. It is a noncontact and nondestructive technique. The instrument can be operated even by unskilled personnel for routine measurements.

George, M. C.↗

NASA NTRS1991

Planar imaging of the mixing characteristics of a multi-element triplet injector

Planar light scattering has been used to investigate the turbulent mixing in a multi-element triplet injector at mixture ratio conditions typical of liquid rocket engine gas generators. Experiments were conducted at atmospheric pressure using air seeded with smoke particles to simulate the oxidizer flow and unseeded air to simulate the fuel. Data sets of 200 images (containing 122,000 simultaneous measurements each) of the instantaneous distribution of the scattered light were acquired at several positions throughout the flow. These images have been processed digitally to produce local distributions of the average and rms fluctuation of the mixture fraction. In addition, the spatial autocorrelation of the images has been calculated and analyzed to determine a mean length scale related to the large scale structures in the flow.

Makel, D. B.↗

NASA NTRS1990

Contamination study

The time dependence of the angular reflectance from molecularly contaminated optical surfaces in the Vacuum Ultraviolet (VUV) is measured. The light scattering measurements are accomplished in situ on optical surfaces in real time during deposition of molecular contaminants. The measurements are taken using non-coherent VUV sources with the predominant wavelengths being the Krypton resonance lines at 1236 and 1600 A. Detection of the scattered light is accomplished using a set of three solar blind VUV photomultipliers. An in-plane VUV BRDF (Bidirectional Reflectance Distribution Functions) experiment is described and details of the ongoing program to characterize optical materials exposed to the space environment is reported.

Johnson, R. Barry↗

NASA NTRS1991

A fiber-optic probe for particle sizing in concentrated suspensions

A fiber-optic probe employing two monomode optical fibers, one for transmitting a Gaussian laser beam to the scattering volume and the second, positioned at some backscatter angle, for receiving the scattered light is described. Performance and suitability of the system for a process control environment is assessed by studying a suspension of polystyrene latex particles over a wide range of sizes and concentrations. The results show that the probe is ideal for a process control environment in industrial and laboratory applications. Particle size is recovered, without any additional corrections for multiple light scattering, in concentrations containing up to 10 percent solids of 39-nm polystyrene latex spheres.

Dhadwal, Harbans S.↗

NASA NTRS1992

Wind tunnel seeding particles for laser velocimeter

The design of an optimal air foil has been a major challenge for aerospace industries. The main objective is to reduce the drag force while increasing the lift force in various environmental air conditions. Experimental verification of theoretical and computational results is a crucial part of the analysis because of errors buried in the solutions, due to the assumptions made in theoretical work. Experimental studies are an integral part of a good design procedure; however, empirical data are not always error free due to environmental obstacles or poor execution, etc. The reduction of errors in empirical data is a major challenge in wind tunnel testing. One of the recent advances of particular interest is the use of a non-intrusive measurement technique known as laser velocimetry (LV) which allows for obtaining quantitative flow data without introducing flow disturbing probes. The laser velocimeter technique is based on measurement of scattered light by the particles present in the flow but not the velocity of the flow. Therefore, for an accurate flow velocity measurement with laser velocimeters, two criterion are investigated: (1) how well the particles track the local flow field, and (2) the requirement of light scattering efficiency to obtain signals with the LV. In order to demonstrate the concept of predicting the flow velocity by velocity measurement of particle seeding, the theoretical velocity of the gas flow is computed and compared with experimentally obtained velocity of particle seeding.

Ghorieshi, Anthony↗

NASA NTRS1994

A new technique for the measurement of surface shear stress vectors using liquid crystal coatings

Research has recently shown that liquid crystal coating (LCC) color-change response to shear depends on both shear stress magnitude and direction. Additional research was thus conducted to extend the LCC method from a flow-visualization tool to a surface shear stress vector measurement technique. A shear-sensitive LCC was applied to a planar test surface and illuminated by white light from the normal direction. A fiber optic probe was used to capture light scattered by the LCC from a point on the centerline of a turbulent, tangential-jet flow. Both the relative shear stress magnitude and the relative in-plane view angle between the sensor and the centerline shear vector were systematically varied. A spectrophotometer was used to obtain scattered-light spectra which were used to quantify the LCC color (dominant wavelength) as a function of shear stress magnitude and direction. At any fixed shear stress magnitude, the minimum dominant wavelength was measured when the shear vector was aligned with and directed away from the observer; changes in the relative in-plane view angle to either side of this vector/observer aligned position resulted in symmetric Gaussian increases in measured dominant wavelength. Based on these results, a vector measurement methodology, involving multiple oblique-view observations of the test surface, was formulated. Under present test conditions, the measurement resolution of this technique was found to be +/- 1 deg for vector orientations and +/- 5% for vector magnitudes. An approach t o extend the present methodology to full-surface applications is proposed.

Reda, Daniel C.↗

NASA NTRS2001

Transport of Photoelectrons in the Nightside Magnetosphere

Kinetic modeling results are analyzed to examine the transport of photoelectrons through the nightside inner magnetosphere. Two sources are considered, those on the dayside from direct solar illumination, and those at all local times from light scattered by the upper atmosphere and geocorona. For the dayside photoelectrons, a natural filter exists oil the nightside for these particles, with Coulomb collisions eroding the distribution at low energies and low L shells, and magnetospheric convection compressing the flux tubes as they corotate towards dawn. It is shown that, for low activity levels, a band of photoelectrons forms between L=4 and 6 that extends throughout the nightside local times and into the morning sector. For the scattered light photoelectrons, the trapped zone throughout the nightside is filled for energies less than 30 eV. Convective compression on the nightside and expansion on the dayside yields an accelerated population up to 50 eV at high L shells around dawn. Modeled energy and pitch angle distributions are presented to show the development and features of these populations. Such distinctive features should be observable in satellite spectrometer measurements.

Khazanov, G. V.↗

NASA NTRS2006

Development of Point Doppler Velocimetry for Flow Field Investigations

A Point Doppler Velocimeter (pDv) has been developed using a vapor-limited iodine cell as the sensing medium. The iodine cell is utilized to directly measure the Doppler shift frequency of laser light scattered from submicron particles suspended within a fluid flow. The measured Doppler shift can then be used to compute the velocity of the particles, and hence the fluid. Since this approach does not require resolution of scattered light from individual particles, the potential exists to obtain temporally continuous signals that could be uniformly sampled in the manner as a hot wire anemometer. This leads to the possibility of obtaining flow turbulence power spectra without the limitations of fringe-type laser velocimetry. The development program consisted of a methodical investigation of the technology coupled with the solution of practical engineering problems to produce a usable measurement system. The paper outlines this development along with the evaluation of the resulting system as compared to primary standards and other measurement technologies.

Cavone, Angelo A.↗

NASA NTRS2007

Development of a Rayleigh Scattering Diagnostic for Time-Resolved Gas Flow Velocity, Temperature, and Density Measurements in Aerodynamic Test Facilities

A molecular Rayleigh scattering technique is developed to measure time-resolved gas velocity, temperature, and density in unseeded turbulent flows at sampling rates up to 32 kHz. A high power continuous-wave laser beam is focused at a point in an air flow field and Rayleigh scattered light is collected and fiber-optically transmitted to the spectral analysis and detection equipment. The spectrum of the light, which contains information about the temperature and velocity of the flow, is analyzed using a Fabry-Perot interferometer. Photomultiplier tubes operated in the photon counting mode allow high frequency sampling of the circular interference pattern to provide time-resolved flow property measurements. An acoustically driven nozzle flow is studied to validate velocity fluctuation measurements, and an asymmetric oscillating counterflow with unequal enthalpies is studied to validate the measurement of temperature fluctuations. Velocity fluctuations are compared with constant temperature anemometry measurements and temperature fluctuations are compared with constant current anemometry measurements at the same locations. Time-series and power spectra of the temperature and velocity measurements are presented. A numerical simulation of the light scattering and detection process was developed and compared with experimental data for future use as an experiment design tool.

Mielke, Amy F.↗

NASA NTRS2008

Gold Nanoparticle Labels Amplify Ellipsometric Signals

The ellipsometric method reported in the immediately preceding article was developed in conjunction with a method of using gold nanoparticles as labels on biomolecules that one seeks to detect. The purpose of the labeling is to exploit the optical properties of the gold nanoparticles in order to amplify the measurable ellipsometric effects and thereby to enable ultrasensitive detection of the labeled biomolecules without need to develop more-complex ellipsometric instrumentation. The colorimetric, polarization, light-scattering, and other optical properties of nanoparticles depend on their sizes and shapes. In the present method, these size-and-shape-dependent properties are used to magnify the polarization of scattered light and the diattenuation and retardance of signals derived from ellipsometry. The size-and-shape-dependent optical properties of the nanoparticles make it possible to interrogate the nanoparticles by use of light of various wavelengths, as appropriate, to optimally detect particles of a specific type at high sensitivity. Hence, by incorporating gold nanoparticles bound to biomolecules as primary or secondary labels, the performance of ellipsometry as a means of detecting the biomolecules can be improved. The use of gold nanoparticles as labels in ellipsometry has been found to afford sensitivity that equals or exceeds the sensitivity achieved by use of fluorescence-based methods. Potential applications for ellipsometric detection of gold nanoparticle-labeled biomolecules include monitoring molecules of interest in biological samples, in-vitro diagnostics, process monitoring, general environmental monitoring, and detection of biohazards.

Venkatasubbarao, Srivatsa↗

NASA NTRS2005

Simultaneous Conoscopic Holography and Raman Spectroscopy

A new instrument was developed for chemical characterization of surfaces that combines the analytical power of Raman spectroscopy with the three-dimensional topographic information provided by conoscopic holography. The figure schematically depicts the proposed hybrid instrument. The output of the conoscopic holographic portion of the instrument is a topographical map of the surface; the output of the Raman portion of the instrument is hyperspectral Raman data, from which the chemical and/or biological composition of the surface would be deduced. By virtue of the basic principles of design and operation of the instrument, the hyperspectral image data would be inherently spatially registered with the topographical data. In conoscopic holography, the object and reference beams of classical holography are replaced by the ordinary and extraordinary components generated by a single beam traveling through a birefringent, uniaxial crystal. In the basic conoscopic configuration, a laser light is projected onto a specimen and the resulting illuminated spot becomes a point source of diffuse light that propagates in every direction. The laser beam is rasterscanned in two dimensions (x and y) perpendicular to the beam axis (z), and at each x,y location, the pattern of interference between the ordinary and extraordinary rays is recorded. The recorded interferogram constitutes the conoscopic hologram. Of particular significance for the proposed instrument is that the conoscopic hologram contains information on the z coordinate (height) of the illuminated surface spot. Hence, a topographical map of the specimen is constructed point-by-point by rastering the laser beam in the x and y directions and correlating the x and y coordinates with the z information obtained from the interferograms. Conoscopic imaging is an established method, and conoscopic laboratory instruments for surface metrology are commercially available. In Raman spectroscopy of a surface, one measures the spectrum of laser light scattered inelastically from a laser-illuminated spot on the surface. The wavelengths of the inelastically scattered light differ from that of the incident laser beam by amounts that correspond to the energies of molecular vibrations. The resulting vibrational spectrum can be used to identify the molecules. Raman spectroscopy is a standard laboratory technique for identifying mineralogical, biological, and other specific chemical compositions.

Schramm, Harry F.↗

NASA NTRS2011

In Situ Aerosol Detector

An affordable technology designed to facilitate extensive global atmospheric aerosol measurements has been developed. This lightweight instrument is compatible with newly developed platforms such as tethered balloons, blimps, kites, and even disposable instruments such as dropsondes. This technology is based on detection of light scattered by aerosol particles where an optical layout is used to enhance the performance of the laboratory prototype instrument, which allows detection of smaller aerosol particles and improves the accuracy of aerosol particle size measurement. It has been determined that using focused illumination geometry without any apertures is advantageous over using the originally proposed collimated beam/slit geometry (that is supposed to produce uniform illumination over the beam cross-section). The illumination source is used more efficiently, which allows detection of smaller aerosol particles. Second, the obtained integral scattered light intensity measured for the particle can be corrected for the beam intensity profile inhomogeneity based on the measured beam intensity profile and measured particle location. The particle location (coordinates) in the illuminated sample volume is determined based on the information contained in the image frame. The procedure considerably improves the accuracy of determination of the aerosol particle size.

Vakhtin, Andrei↗

NASA NTRS2012

Mercury's Na Exosphere from MESSENGER Data

MESSENGER entered orbit about Mercury on March 18, 2011. Since then, the Ultraviolet and Visible Spectrometer (UWS) channel of MESSENGER's Mercury Atmospheric and Surface Composition Spectrometer (MASCS) has been observing Mercury's exosphere nearly continuously. Daily measurements of Na brightness were fitted with non-uniform exospheric models. With Monte Carlo sampling we traced the trajectories of a representative number of test particles, generally one million per run per source process, until photoionization, escape from the gravitational well, or permanent sticking at the surface removed the atom from the simulation. Atoms were assumed to partially thermally accommodate on each encounter with the surface with accommodation coefficient 0.25. Runs for different assumed source processes are run separately, scaled and co-added. Once these model results were saved onto a 3D grid, we ran lines of sight from the MESSENGER spacecraft :0 infinity using the SPICE kernels and we computed brightness integrals. Note that only particles that contribute to the measurement can be constrained with our method. Atoms and molecules produced on the nightside must escape the shadow in order to scatter light if the excitation process is resonant-light scattering, as assumed here. The aggregate distribution of Na atoms fits a 1200 K gas, with a PSD distribution, along with a hotter component. Our models constrain the hot component, assumed to be impact vaporization, to be emitted with a 2500 K Maxwellian. Most orbits show a dawnside enhancement in the hot component broadly spread over the leading hemisphere. However, on some dates there is no dawn/dusk asymmetry. The portion of the hot/cold source appears to be highly variable.

Killen, Rosemary M.↗